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At least 235 records · Page 13

All sources NASA NTRS DOE OSTI

DOE OSTI2016

Radiation Tolerance of Silicon Carbide Joints at LWR Relevant Temperature

The development of reliable joints in reactor service conditions is a critical requirement for SiC based accident tolerant fuels and core structures for light water reactor (LWR) applications. The effects of neutron irradiation on the mechanical properties is an important consideration under normal operation. Though various SiC joints retained the strength following neutron irradiation at ∼500 and ∼800 deg. C to ∼3 dpa, the irradiation tolerance of the joints at the LWR relevant temperature is still an unknown. This study presents the strengths of the candidate SiC joints following irradiation at ∼300 deg. C. The bonding strength was investigated using torsional shear testing which was developed for miniature irradiation specimens in previous work. Torsional shear strengths of various SiC joints were evaluated following irradiation at 270-310 deg. C to 8.7 dpa. Strength degradation by the irradiation likely occurred in the Mo diffusion bond. No obvious strength degradation was found in the MAX phase and hybrid polymer/CVD joints. The irradiation caused large deviation of the strength of Ti diffusion bond, TEP slurry and tape joints. The cause of this deviation will be investigated based on microstructural analysis in future work. (authors)

36 MATERIALS SCIENCE↗

DOE OSTI2023

THE ROLE OF FRACTURE PROPERTIES ON LAP JOINT STRENGTH OF FRICTION STIR WELDED AA7055-T6 SHEETS

Friction stir lap welded (FSLW) joints have weight-saving potential in aluminum-intensive automotive assembly. However, FSLW also modifies the material microstructure close to the joint. Optimizing the FSLW process requires understanding the relationship between the strength and the joint's microstructure. In previous studies, efforts have been dedicated to determining the effects of local softening, the shape of the oxide line, and porosity. However, the impact of changes to the fracture properties on the joint's strength has not been studied. In this work, strength testing, and simulations, aided by material characterization, were used to determine the role of fracture properties on the shear strength of a 3-sheet (aluminum alloys 7055-7055-6022) lap joint. Characterization involved testing for fracture properties in the weld region. This data was then implemented into finite element simulations. As a result, the joint strength was predicted with a deviation of less than 6% from the experimental value. Comparison with strength prediction using only the base metal properties indicates that fracture property in the nugget region determines the strength of AA7055 FSLW.

Finite element analysis, Friction stir welding, ma↗

DOE OSTI2017

Study on the Reliability of Carbon Nanotube-Reinforced Sn-58Bi Lead-Free Solder Joints

The wettability, microstructure and mechanical properties of multi-walled carbon nanotube (CNT)-reinforced Sn-58Bi composite solder joints were investigated. The results indicate that the wettability of the Sn-58Bi solder is improved and the growth of interfacial intermetallic (IMC) compounds for solder joints is restrained by CNTs. The thickness of the IMC layers is decreased with increasing CNTs concentration. The microstructure of the Sn-58Bi composite solders is refined, the maximum tensile strength and shear strength are obtained by adding the optimum CNTs content about 0.01 wt.%. However, excessive content of CNTs addition can deteriorate the properties. The creep rupture life of Sn-58Bi solder joint and Sn-58Bi-0.01CNTs solder joint is decreased with increasing load, temperature and current density. The average creep rupture life of Sn-58Bi-0.01CNTs composite solder joint is 60% higher than that of the plain solder joint.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

DOE OSTI2018

Microstructure and Strain Rate-Dependent Tensile Deformation Behavior of Fiber Laser-Welded Butt Joints of Dual-Phase Steels

The microstructure and tensile deformation behavior of the fiber laser-welded similar and dissimilar dual-phase (DP) steel joints over a wide range of strain rates from 10{sup −3} to 10{sup 3} s{sup −1} were investigated for the further applications on the lightweight design of vehicles. The high strain rate dynamic tensile deformation process and full-field strain distribution of the base metals and welded joints were examined using the digital image correlation method and high-speed photography. The strain rate effects on the stress–strain responses, tensile properties, deformation, and fracture behavior of the investigated materials were analyzed. The yield stress (YS) and ultimate tensile strength (UTS) of the dissimilar DP780/DP980 welded joints were lying in-between those of the DP780 and DP980 base metals, and all materials exhibited positive strain rate dependence on the YS and UTS. Owing to the microstructure heterogeneity, the welded joints showed relatively lower ductility in terms of total elongation (TE) than those of the corresponding base metals. The strain localization started before the maximum load was reached, and the strain localization occurred earlier during the whole deformation process with increasing strain rate. As for the dissimilar welded joint, the strain localization tended to occur in the vicinity of the lowest hardness value across the welded joint, which was in the subcritical HAZ at the DP780 side. As the strain rate increased, the typical ductile failure characteristic of the investigated materials did not change.

36 MATERIALS SCIENCE↗

DOE OSTI2018

Microstructures and Mechanical Properties of Resistance Spot-Welded Steel/Aluminum Alloy Joints with Process Tapes

The microstructure and mechanical property of resistance spot-welded joints of steel and aluminum were studied by using process tapes. The steel/aluminum joint consists mainly of aluminum nugget and interface zone. The liquid nugget solidification has an epitaxial growth characteristic, and the interface zone displays a double-layer structure, Fe{sub 2}Al{sub 5} layer at steel side and Fe{sub 4}Al{sub 13} layer at aluminum nugget side. Compared with joints without process tape, the joint nugget diameter and tensile shear load increased by 35.45 and 10.98%, respectively, and its indentation ratio decreased by 56.25% due to the process tapes increasing heat input, producing larger nugget diameter and continuous interface layer, and protecting against deep indentation. The joining area of intermetallic layer and aluminum nugget is weak link in the joint. It is favorable to use the process tapes for improving welding quality, raising joint strength, and energy saving.

36 MATERIALS SCIENCE↗

DOE OSTI2019

Microstructure and Mechanical Properties of a SiO{sub 2} Ceramic and TC4 Alloy Joint Brazed with a Nanocomposite Filler

Vacuum brazing of TC4 alloy and SiO{sub 2} ceramic was achieved using a nano-AgCuNi braze alloy. The melting temperature of nano-AgCu powders was analyzed by differential scanning calorimeter. Furthermore, the effects of the Ni content on the microstructure and mechanical properties of the joints were studied. The results showed that the melting temperature of the nano-AgCu filler was 774 °C. A decrease in the melting temperature of 6 °C was observed, compared with the general AgCu filler, and this decrease enabled the interfacial reaction of the joint to begin earlier. The typical interfacial microstructure of the TC4/nano-AgCuNi/SiO{sub 2} ceramic joint brazed at 950 °C for 10 min was TC4/α-Ti + Ti{sub 2}(Cu,Ni) + Ti{sub 2}(Ni,Cu) hypereutectoid structure/Ti{sub 2}(Cu,Ni) compound with α-Ti + Ti{sub 2}(Cu,Ni) + Ti{sub 2}(Ni,Cu) hypereutectic structure/Ti{sub 4}O{sub 7} + TiSi{sub 2}/SiO{sub 2} ceramics. The homogeneous microstructure of α-Ti + Ti{sub 2}(Cu,Ni) + Ti{sub 2}(Ni,Cu) hypereutectoid structure primarily existed in the diffusion layer. Additionally, the refined α-Ti + Ti{sub 2}(Cu,Ni) + Ti{sub 2}(Ni,Cu) hypereutectic structure created via a eutectic reaction and Ti{sub 2}(Cu,Ni) compound was distributed in the brazing seam. The Ni content could influence the formation of Ti-Cu-Ni ternary intermetallic compounds (IMCs). An increase in Ni led to an increase in the α-Ti + Ti{sub 2}(Cu,Ni) + Ti{sub 2}(Ni,Cu) hypereutectic structure in the brazing seam. The shear strength of the brazed joints first increased and then decreased with the increase in the nano-Ni content, and the optimal shear strength of 30.1 MPa was achieved at 10 wt.% Ni. The increase in the α-Ti + Ti{sub 2}(Cu,Ni) + Ti{sub 2}(Ni,Cu) hypereutectic structure and the decrease in brittle compounds enhanced the shear strength of the joint. Fracture analysis of the joints brazed at 950 °C for 10 min indicated that the cracks mainly occurred in SiO{sub 2} ceramic.

36 MATERIALS SCIENCE↗

DOE OSTI2019

Solderability of AZ31B Magnesium Alloy Coated by Copper and Strength of the Solder Joints

Magnesium alloys are promising as light materials, while their high chemical reactivity makes them difficult to be soldered. In this study, the AZ31B alloy was pretreated by zincification and coated by an electrodeposited Cu layer, and then soldered with Sn-58Bi solder in air furnace. The microstructure and properties of the AZ31B/Cu(Zn)/SnBi solder joints were characterized to evaluate the solderability of the Cu-coated Mg alloy and the influence of soldering on the Cu coating. It was found that the Cu coating is dense, and little defect exists along the Cu(Zn)/AZ31B interface. The soldering process has little negative effect on the bonding between the Cu coating and the AZ31B substrate, and the AZ31B/Cu(Zn)/SnBi solder joints of high metallurgical quality were obtained. Tensile fracture of the solder joint occurs mainly in the solder, with no peeling of the Cu coating. Under shear loading, cracks initiate inside the SnBi solder and the final fracture of the joint occurs around the Cu{sub 6}Sn{sub 5}/solder interface or along the Cu(Zn)/AZ31B interface. The tensile and shear strength of the AZ31B/Cu(Zn)/SnBi solder joints are close to that of the SnBi/Cu solder joints. It is demonstrated that the Cu-coated Mg alloy shows superior solderability and can be soldered by the Sn-based low-melting solder in air.

36 MATERIALS SCIENCE↗

DOE OSTI2014

Comparison of Cu, Ti and Ta interlayer explosively fabricated aluminum to stainless steel transition joints for cryogenic pressurized hydrogen storage

Fabrication of a bimetallic joint to facilitate a material transition from a 6061-T651 aluminum pressure vessel liner to stainless steel tubing in cryogenic pressure vessels is explored using three different dissimilar metal interlayers with an explosive welding (EXW) process. Due to difficulties in directly EXW joining aluminum (Al) 6061 to 304 stainless steel, interlayers are used to prevent interaction of the aluminum and stainless steel, thus minimizing brittle intermetallic phase formation. Titanium (Ti), copper (Cu), and tantalum (Ta) were selected as the dissimilar metal interlayer materials; each having advantages and disadvantages. Further, titanium is a commonly used interlayer for this joint, but can microcrack during EXW if the bonding parameters are not correct. Copper has the advantage that it is compatible with hydrogen, but is also known to form brittle intermetallics with aluminum. Tantalum is ductile and bonds well to both Al and stainless steel, and is a high temperature metal that does well to prevent interdiffusion and intermetallic phase formation. However Ta is the most expensive metal of the three. Results of the characterization of the three interlayer bonds showed that Ti produced the highest strength joints, Ta produced the most ductile joints, and Cu produced a joint that failed with low ductility at the Al/Cu interface. Based on these results, the Cu-interlayer joint is not recommended for this application, while the Ti and Ta interlayer bonds both appear to have sufficient strength and ductility for the intended use.

08 HYDROGEN↗

DOE OSTI2023

Corrosion of Al-Fe self-pierce riveting joints with multiphysics-based modeling and experiments

Self-piercing riveting (SPR) is an extensively used joining technique to assemble dissimilar materials. However, this joining of the dissimilar materials can generate galvanic/crevice corrosion, which can drastically impact the mechanical properties and the service life of the joint. In this study, a multiphysics-based hybrid modeling approach is developed for the galvanic corrosion of the Al-Fe SPR joints, which can consider the corrosion initiation and corrosion evaluation jointly. Experimental studies are first performed to extract information regarding the corrosion initiation sites, corrosion evolution and overall corrosion induced material loss in SPR joints. The initiation information is then passed onto the multiphysics FE model thus making it a hybrid model. This model can help understand the influences of metal microstructure on the corrosion propagation while the morphology changes can also be analyzed. Using the developed hybrid modeling approach, thorough parametric studies can be performed to explore the coupled impacts of multiple corrosion factors on the corrosion behavior of the joints. The developed hybrid model is validated on the prediction of galvanic corrosion for the SPR joints by comparing with experimental observations.

36 MATERIALS SCIENCE↗

DOE OSTI2018

Interfacial structure and properties of Cu/Al joints brazed with Zn-Al filler metals

Highlights: • The formation mechanism of Cu side interfacial compounds of Cu/Al joints with Zn-Al filler metals are revealed accurately. • The Cu side interfacial structure is uncertain and dependent on brazing parameters, especially cooling rate after brazing. • The close relation among composition, brazing parameters, interfacial structure and mechanical properties is discovered. - Abstract: Seeing that opinions vary, no unanimous conclusion has been drawn on Cu side interfacial structure and its relationship with the mechanical properties of Cu/Al joints brazed with Zn-Al filler metals, XRD, SEM and HAADF-STEM were used to accurately reveal the Cu side interfacial structure and the mechanism concerned. The relationship among the brazing process, interfacial structure and mechanical properties of the joints was systematically studied. The following phenomena and principles were newly found and clarified. The Cu side interfacial structure are uncertain and dependent on brazing parameters, especially cooling rate after brazing, in addition to the composition of Zn-Al filler metal. High cooling rate promotes the formation of CuZn and Al{sub 4.2}Cu{sub 3.2}Zn{sub 0.7} compounds, while slow cooling rate is beneficial for the formation of Cu-Al interfacial compounds at the Cu side interface. Increasing brazing temperature or lengthening holding time enhances the dissolution of base metals, which results in the increase of Al and Cu contents at the Cu side interface, thus promoting the formation of CuAl{sub 2} compound. Besides, increasing Al content in Zn-Al filler metal also promotes the formation of CuAl{sub 2} compound by directly increasing Al content at the Cu side interface. The significant differences in joint strength are caused by the differences of Cu side interfacial compounds essentially. When the thin CuZn and Al{sub 4.2}Cu{sub 3.2}Zn{sub 0.7} layers exist at the Cu side interface, the brazed joint possesses high shear strength. On the contrary, the formation of Cu-Al compound layers at the Cu side interface, especially CuAl{sub 2}, will severely degrade the joint strength.

36 MATERIALS SCIENCE↗

DOE OSTI2016

M3FT-16OR020202112 - Report on viability of hydrothermal corrosion resistant SiC/SiC Joint development

Hydrothermal corrosion of four types of the silicon carbide (SiC) to SiC plate joints were investigated under PWR and BWR relevant chemical conditions without irradiation. The joints were formed by metal diffusion bonding using molybdenum or titanium interlayer, reaction sintering using Ti-Si-C system, and SiC nanopowder sintering. Most of the formed joints withstood the corrosion tests for five weeks. The recession of the SiC substrates was limited. Based on the recession rate of the bonding layers, it was concluded that all the joints except for the molybdenum diffusion bond are promising under the reducing activity environments. The SiC nanopowder sintered joint was the most corrosion tolerant under the oxidizing activity environment among the four joints.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

NASA NTRS2024

Out of Plane Stresses Using a Beam-Based Elastic Foundation Bonded Joint Model

Efficient, semi-analytical models of bonded joints are utilized for initial joint design and sizing due to their convenience and speed. Many of these models are based on beam and plate theories, which are most applicable when in-plane stresses/strains dominate. While this can be a sensible assumption for obtaining the deformations of the joint, out of plane (transverse) stresses are often of critical importance for failure in bonded joints composed of fiber reinforced composite materials. Since through-thickness strains are neglected in these semi-analytical theories, the present study shows a method to back-calculate the out of plane stresses based on stress balance equations, which use the in-plane stresses and displacements that have already been obtained. The method was implemented within the Joint Element Designer (JED) software, and verification and validation examples have been shown. As is typical for these types of models, corner stress singularities are not captured by the JED model, but the general trends of the stress and deformation fields agreed with a higher fidelity finite element model. As such, this method for obtaining out of plane stresses, when coupled with the JED code, is very useful for the complete stress analysis of bonded composite joints.

composites↗

NASA NTRSDate not supplied

Structural Analysis, Modeling, and Testing of Multi-nut Joint for TriTruss Structure

The Multi-nut joint, developed at NASA Langley Research Center (LaRC), was designed to assemble TriTruss modules for a doubly curved 65.6-feet telescope support structure. Axial and bending tests for a multi-nut joint in the TriTruss structure were conducted to characterize the structural performance of the multi-nut joint and to obtain the installation torque value of the attachment fastener. This paper describes the summary of the axial and bending tests of the multi-nut joint, along with the test results. The equivalent axial stiffness (EA) and equivalent bending stiffness (EI) of the multi-nut joint were characterized based on these test results and are presented in this report. Additionally, finite element models (FEMs) of the axial and bending test specimens were developed, and the predicted axial and bending responses of the multi-nut joint were compared with the test results. Test-analysis comparison results show that the predicted axial load-displacement response of the test specimen was within 5 percent of the test results, while the predicted load-bending response of the test specimen exhibited a consistent trend with the test data.

TriTruss↗

NASA NTRSDate not supplied

Structural Analysis, Modeling, and Testing of Multi-nut Joint for TriTruss Structure

Structural analysis↗

DOE OSTI2019

Microstructure and Mechanical Property Improvement in Laser-Welded TC4 Titanium Alloy and 301L Stainless Steel Joints Without Filler Metal

Pulsed laser welding of Ti alloy to stainless steel (SS) has been applied without filler metal. When the laser beam was focused on the Ti alloy–SS interface, large volumes of Ti-Fe intermetallics were formed in the joint. These Ti-Fe intermetallics were highly brittle, causing the joint to crack spontaneously after welding. The brittle coarse Ti-Fe intermetallics seriously deteriorates the joint strength of Ti alloy and SS; therefore, it is necessary to control the quantities and distributions of brittle Ti-Fe intermetallics in the joint. The amount of melted base materials was controlled by changing laser offset to control the melted proportion and thus control the quantity and distribution of brittle Ti-Fe intermetallics in weld. When laser beam was on the SS side, melting amount of Ti alloy in weld was decreased. When laser beam was on the Ti alloy side, melting amount of SS in weld was decreased. When the laser offset was 0.35 mm away from SS side, the sample realizes the effective connection between Ti alloy and SS. A compound layer was formed at the SS side with the main microstructure of β-Ti and TiFe{sub 2}. The joint fractured at the compound layer with the maximum tensile strength of 182 MPa. Microstructures and mechanical properties of joints were improved by changing laser offset.

36 MATERIALS SCIENCE↗

DOE OSTI2019

Creep Deformation and Rupture Behavior of P92 Steel Weld Joint Fabricated by NG-TIG Welding Process

The creep deformation and rupture behavior of P92 steel weld joint fabricated by narrow-gap TIG (NG-TIG) welding process have been investigated at 923 K over a stress range of 80-140 MPa. The prior-austenite grain size, M{sub 23}C{sub 6} precipitate size and hardness have been found to vary significantly in the weld joint. The reduction in hardness from weld metal to base metal with a trough at the outer edge of heat-affected zone (HAZ) has been observed. Coarsening of M{sub 23}C{sub 6} precipitate, recovery of martensite lath dislocation structure and formation of subgrain structure led to lower hardness in the intercritical HAZ. The creep rupture life of NG-TIG weld joint was lower than the base metal, the difference in creep rupture life between base metal and weld joint has been increased significantly with decrease in applied stress. The fracture location in the joint changed from base metal at high-stress regime to the fine grain (FG) HAZ (Type IV cracking) under lower stress level. Fracture in the FGHAZ evidenced the significant reduction in ductility, localized deformation and extensive localized cavitation. Extensive Laves phase formation with significant loss of solution strengthening contribution from tungsten and coarsening of M{sub 23}C{sub 6} precipitate with prolonged creep exposure led to reduction in hardness and more extensive cavitation in the FGHAZ resulting in premature Type IV failure of the weld joint. Weld strength reduction factor about 0.59 has been evaluated for 10{sup 5} h at 923 K.

36 MATERIALS SCIENCE↗

DOE OSTI2019

Effect of Welding Parameters on Junction Structure and Fracture Behavior of Friction-Stir-Welded Joints of 2024 Aluminum Alloys

In this paper, the effect of welding speed and tool rotation speed on the junction structure and fracture behavior of friction-stir-welded joints was investigated with use of 2024 aluminum alloys of 3.2 mm thick. Results show that the formation of junction structure is more affected by tool rotation speed than by welding speed due to the differences of heat input levels. When welding speed is at 100 mm/min and tool rotation speed is in the range of 400-600 r/min, the joint junction structure causes complete bonding with no welding defects. While under improper welding parameters, the junction structure causes the precipitate aggregation on the bonding line and the partial bonding with the appearance of both tunnel defects and kissing bond defects. Meanwhile, the results of tensile tests show that the tensile fracture of all FSW joints occur at the weld center. The failure mode of joints with defects-free junction structure characterized by shear fracture is ductile. While the failure mode of joints with defects-existent junction structure characterized by layered fracture surface is brittle. Furthermore, that heterogeneous microstructure, precipitate aggregation and welding defects converge inside the junction structure is the main factor affecting the tensile properties and fracture behavior of the friction-stir-welded joint.

36 MATERIALS SCIENCE↗

DOE OSTI2019

Flow Patterns, Microstructure and Mechanical Properties of AZ31/Al6061 Dissimilar Friction Stir-Welded Joints

Dissimilar joints between die-cast AZ31 and extruded Al6061-T6 were joined using friction stir welding technology at a constant transverse speed (50 mm/min) and rotation rate of 800 or 1000 rpm. The flow patterns, microstructure evolution and intermetallic compounds in dissimilar joints were studied by optical and scanning electron microscopy. The relationship between microstructure and tensile properties was analyzed. The microhardness distribution along the horizontal centerline in cross section was investigated. Local flow without obvious mixing existed between Mg and Al metals in the tool shoulder-affected zone. For the tool-pin-affected zone, two typical zones, namely, the “extrusion zone” and “flow zone” existed because of the different flow modes of the plastic metals. The phase analysis showed that intermetallic compounds, including Al{sub 12}Mg{sub 17} and Al{sub 3}Mg{sub 2} formed in banded structures. Phase analysis showed that a joint with welding parameters of 800 rpm and 50 mm/min (Joint-500) had good mechanical properties because of the more uniform microstructure distribution and fewer intermetallic compounds. Fracture analysis indicated some microvoids and lamellate intermetallic compounds in the fracture surface of the joint with welding parameters of 1000 rpm and 50 mm/min (Joint-1000), which deteriorated its tensile strength significantly.

36 MATERIALS SCIENCE↗