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At least 235 records · Page 13

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DOE OSTI2025

Measuring the Interfacial Chemistry of Micro- and Nano-Plastics Using Matrix Assisted Laser Desorption Ionization

Micro- and nano-plastics (MNPs) pose a significant hazard to both environmental and human health due to their complex interfacial interactions with their surroundings, however there is a lack of techniques available to study the composition of MNPs at their surface. To fill this gap, representative MNPs were coated with matrix that enabled detection via matrix-assisted laser desorption ionization mass spectrometry (MALDI), a technique that has been shown to be surface specific but had not been applied to MNPs previously. Three different coating techniques were tested; evaporation and condensation, drop-casting, and mixed nebulization. Mixed nebulization provided the best balance of results, which was a strong MALDI signal in combination with even coating on the MNP surface from MNPs ≥20 µm. This work provides a new technique for the measurement of MNP surface composition that will help advance the field and enable more thorough studies of the chemical transformations that MNPs undergo in the environment.

36 MATERIALS SCIENCE↗

DOE OSTI2025

Development of High-Temperature Bonding Techniques to Enable High-Temperature Static or Dynamic Strain Measurements

Current light-water nuclear reactors rely on a variety of different sensors and sensor applications to meet their structural health monitoring needs throughout the entirety of the reactor primary, secondary, and containment systems. Optical fiber–based sensor technologies could provide solutions to reduce the sensor system footprint while enhancing the measurement fidelity and spatial resolution by leveraging distributed monitoring techniques. Moreover, advanced reactors may require optical fiber–based sensors for structural health monitoring because their operating temperatures will exceed the limits of conventional transducers used to acquire dynamic strain or acoustic data in nuclear power plants. Therefore, this report describes experiments targeting the development of high-temperature bonding techniques that would allow for potentially long lengths of fibers to be bonded to metallic reactor components in advanced reactor systems. The high temperatures experienced within target application, next-generation nuclear reactors, necessitate a high-temperature resistant bond to limit the amount of tension on the fiber at the target application temperature. The primary bonding method investigated in this work is brazing; hot-rolling has also been investigated to a lesser extent. Both techniques are well-suited to bonding optical fibers to large reactor components such as primary coolant piping, pressure vessels, or heat exchangers. Optical frequency domain reflectometry was used to monitor the strain in metal-coated optical fibers before, during, and after the high-temperature bonding process. On select optical fibers that were successfully bonded, additional thermal cycling was performed to assess the extent to which the fiber remained bonded based on the expected thermal expansion of the test specimen material. The results of the various experiments yielded the following general conclusions: (1) brazing is a viable technique for bonding and allows significant compressive strain to be applied to the fiber at room temperature; (2) hot-rolling is a viable technique as well, which has been more optimized than the brazing technique for bonding, but less residual compressive strain has been observed with this technique; and (3) both techniques will need further development and optimization to demonstrate bonding of a long length of fiber that can provably operate at relevant temperatures for an advanced nuclear reactor application.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

NASA NTRS1985

Satellite geodynamics

The application of space technology to the study of solid-earth geophysics are reviewed. Attention is given to the major experiments in the field of space-based geodynamics research including early satellite laser ranging (SLR) measurements, the GEOS-3 satellite observations, and the installation of corner cube reflectors on the moon. The contribution of VLBI techniques to terrestriral positioning measurements is also discussed. Prospects for future advances with the development of the Global Positioning System (GPS) and observations from on board the Space Station are also assessed.

Walter, L. S.↗

NASA NTRS1992

Long-baseline optical and infrared stellar interferometry

The history and the current status of optical and infrared long-baseline interferometry are reviewed. In particular, attention is given to Michelson interferometry; the Mark III stellar interferometer and its applications to astrometry, measurement of stellar diameters, and observations of binary stars; and advanced techniques. The discussion then focuses on astrometry and imaging with space interferometers. Finally, the future of long-baseline interferometry is briefly discussed with particular reference to the interferometry of the moon.

Shao, M.↗

NASA NTRS2004

NASA Programs in Advanced Sensors and Measurement Technology for Aeronautical Applications

There are many challenges facing designers and operators of our next-generation aircraft in meeting the demands for efficiency, safety, and reliability which are will be imposed. This paper discusses aeronautical sensor requirements for a number of research and applications areas pertinent to the demands listed above. A brief overview will be given of aeronautical research measurements, along with a discussion of requirements for advanced technology. Also included will be descriptions of emerging sensors and instrumentation technology which may be exploited for enhanced research and operational capabilities. Finally, renewed emphasis of the National Aeronautics and Space Administration in advanced sensor and instrumentation technology development will be discussed, including project of technology advances over the next 5 years. Emphasis on NASA efforts to more actively advance the state-of-the-art in sensors and measurement techniques is timely in light of exciting new opportunities in airspace development and operation. An up-to-date summary of the measurement technology programs being established to respond to these opportunities is provided.

Conway, Bruce A.↗

NASA NTRS2005

Experimental Investigation of the Differences Between Reynolds-Averaged and Favre-Averaged Velocity in Supersonic Jets

Recent advancement in the molecular Rayleigh scattering based technique allowed for simultaneous measurement of velocity and density fluctuations with high sampling rates. The technique was used to investigate unheated high subsonic and supersonic fully expanded free jets in the Mach number range of 0.8 to 1.8. The difference between the Favre averaged and Reynolds averaged axial velocity and axial component of the turbulent kinetic energy is found to be small. Estimates based on the Morkovin's "Strong Reynolds Analogy" were found to provide lower values of turbulent density fluctuations than the measured data.

Panda, J.↗

NASA NTRS2017

Measured Boundary Layer Transition and Rotor Hover Performance at Model Scale

An experiment involving a Mach-scaled, 11:08 f t: diameter rotor was performed in hover during the summer of 2016 at NASA Langley Research Center. The experiment investigated the hover performance as a function of the laminar to turbulent transition state of the boundary layer, including both natural and fixed transition cases. The boundary layer transition locations were measured on both the upper and lower aerodynamic surfaces simultaneously. The measurements were enabled by recent advances in infrared sensor sensitivity and stability. The infrared thermography measurement technique was enhanced by a paintable blade surface heater, as well as a new high-sensitivity long wave infrared camera. The measured transition locations showed extensive amounts, x=c>0:90, of laminar flow on the lower surface at moderate to high thrust (CT=s > 0:068) for the full blade radius. The upper surface showed large amounts, x=c > 0:50, of laminar flow at the blade tip for low thrust (CT=s < 0:045). The objective of this paper is to provide an experimental data set for comparisons to newly developed and implemented rotor boundary layer transition models in CFD and rotor design tools. The data is expected to be used as part of the AIAA Rotorcraft SimulationWorking Group

Overmeyer, Austin D.↗

DOE OSTI2023

SonicPy: a suite of programs for ultrasound pulse-echo data acquisition and analysis

Sound speed and elastic constants measurements in solids and liquids are commonly performed using the ultrasound pulse-echo technique. Recent advances have expanded the use of this technique at numerous high pressure synchrotron beamlines and offline laboratories. However, the increased experimental throughput has revealed many limitations in existing software for handling the rapid measurement and the subsequent data-reduction. Here, we report the development of a collection of computer programs for sound speed measurements using the ultrasound pulse-echo technique, compatible with stepped multi-frequency, as well as broadband-pulse, couplant-corrected methods. The programs provide a highly interactive graphical interface, enable efficient measurement, exploration and near real-time analysis of the ultrasound data, and contain features useful for working with samples under high pressure and/or high temperature. The included analysis programs can alleviate the time required for data reduction from hours to less than a minute, allowing users to make timely and informed decisions regarding the appropriate experimental parameters.

97 MATHEMATICS AND COMPUTING↗

NASA NTRS2016

Exploiting Measurement Uncertainty Estimation in Evaluation of GOES-R ABI Image Navigation Accuracy Using Image Registration Techniques

In evaluating GOES-R Advanced Baseline Imager (ABI) image navigation quality, upsampled sub-images of ABI images are translated against downsampled Landsat 8 images of localized, high contrast earth scenes to determine the translations in the East-West and North-South directions that provide maximum correlation. The native Landsat resolution is much finer than that of ABI, and Landsat navigation accuracy is much better than ABI required navigation accuracy and expected performance. Therefore, Landsat images are considered to provide ground truth for comparison with ABI images, and the translations of ABI sub-images that produce maximum correlation with Landsat localized images are interpreted as ABI navigation errors. The measured local navigation errors from registration of numerous sub-images with the Landsat images are averaged to provide a statistically reliable measurement of the overall navigation error of the ABI image. The dispersion of the local navigation errors is also of great interest, since ABI navigation requirements are specified as bounds on the 99.73rd percentile of the magnitudes of per pixel navigation errors. However, the measurement uncertainty inherent in the use of image registration techniques tends to broaden the dispersion in measured local navigation errors, masking the true navigation performance of the ABI system. We have devised a novel and simple method for estimating the magnitude of the measurement uncertainty in registration error for any pair of images of the same earth scene. We use these measurement uncertainty estimates to filter out the higher quality measurements of local navigation error for inclusion in statistics. In so doing, we substantially reduce the dispersion in measured local navigation errors, thereby better approximating the true navigation performance of the ABI system.

navigation performance↗

NASA NTRS2005

Nighttime Cirrus Detection using Atmospheric Infrared Sounder Window Channels and Total Column Water Vapor

A method of cirrus detection at nighttime is presented that utilizes 3.8 and 10.4 (micro)m infrared (IR) window brightness temperature differences (dBT) and total column precipitable water (PW) measurements. This technique is applied to the Atmospheric Infrared Sounder (AIRS) and Advanced Microwave Sounding Unit A (AMSU-A) instrument suite on board EOS-Aqua, where dBT is determined from sets of carefully selected AIRS window channels, while PW is derived from the synergistic AIRS and AMSU-A water vapor retrievals. Simulated and observed dBT for a particular value of PW are not constant; several physical factors impact dBT, including the variability in temperature and relative humidity profiles, surface emissivity, instrument noise, and skin/ near-surface air temperature differences. We simulate clear-sky dBT over a realistic range of PWs using 8350 radiosondes that have varying temperature and relative humidity profiles. Thresholds between cloudy and uncertain sky conditions are derived once the scatter in the clear-sky dBT is determined. Simulations of optically thin cirrus indicate that this technique is most sensitive to cirrus optical depth in the 10 (micro)m window of 0.1-0.15 or greater over the tropical and subtropical oceans, where surface emissivity and skin/near-surface air temperature impacts on the IR radiances are minimal. The method at present is generally valid over oceanic regions only, specifically, the tropics and subtropics. The detection of thin cirrus, and other cloud types, is validated using observations at the Atmospheric Radiation Measurement (ARM) program site located at Manus Island in the tropical western Pacific for 89 coincident EOS-Aqua overpasses. Even though the emphasis of this work is on the detection of thin cirrus at nighttime, this technique is sensitive to a broad cloud morphology. The cloud detection technique agrees with ARM-detected clouds 82-84% of the time, which include thin cirrus, as well as other cloud types. Most of the disagreements are well explained by AIRS footprint-scale heterogeneity compared to ARM point measurements, cirrus overlying lower-layer water clouds, possible mixed phase microphysics in midlevel clouds, and significant IR channel noise for cold BT scenes over deep convective towers.

Atmospheric Radiation Measurement (RAM)↗

NASA NTRS1993

Acoustic mode measurements in the inlet of a model turbofan using a continuously rotating rake: Data collection/analysis techniques

The rotating microphone measurement technique and data analysis procedures are documented which are used to determine circumferential and radial acoustic mode content in the inlet of the Advanced Ducted Propeller (ADP) model. Circumferential acoustic mode levels were measured at a series of radial locations using the Doppler frequency shift produced by a rotating inlet microphone probe. Radial mode content was then computed using a least squares curve fit with the measured radial distribution for each circumferential mode. The rotating microphone technique is superior to fixed-probe techniques because it results in minimal interference with the acoustic modes generated by rotor-stator interaction. This effort represents the first experimental implementation of a measuring technique developed by T. G. Sofrin. Testing was performed in the NASA Lewis Low Speed Anechoic Wind Tunnel at a simulated takeoff condition of Mach 0.2. The design is included of the data analysis software and the performance of the rotating rake apparatus. The effect of experiment errors is also discussed.

Hall, David G.↗

NASA NTRS1993

Acoustic mode measurements in the inlet of a model turbofan using a continuously rotating rake - Data collection/analysis techniques

Hall, David G.↗

NASA NTRS2013

Advanced Optical Diagnostics for Ice Crystal Cloud Measurements in the NASA Glenn Propulsion Systems Laboratory

A light extinction tomography technique has been developed to monitor ice water clouds upstream of a direct connected engine in the Propulsion Systems Laboratory (PSL) at NASA Glenn Research Center (GRC). The system consists of 60 laser diodes with sheet generating optics and 120 detectors mounted around a 36-inch diameter ring. The sources are pulsed sequentially while the detectors acquire line-of-sight extinction data for each laser pulse. Using computed tomography algorithms, the extinction data are analyzed to produce a plot of the relative water content in the measurement plane. To target the low-spatial-frequency nature of ice water clouds, unique tomography algorithms were developed using filtered back-projection methods and direct inversion methods that use Gaussian basis functions. With the availability of a priori knowledge of the mean droplet size and the total water content at some point in the measurement plane, the tomography system can provide near real-time in-situ quantitative full-field total water content data at a measurement plane approximately 5 feet upstream of the engine inlet. Results from ice crystal clouds in the PSL are presented. In addition to the optical tomography technique, laser sheet imaging has also been applied in the PSL to provide planar ice cloud uniformity and relative water content data during facility calibration before the tomography system was available and also as validation data for the tomography system. A comparison between the laser sheet system and light extinction tomography resulting data are also presented. Very good agreement of imaged intensity and water content is demonstrated for both techniques. Also, comparative studies between the two techniques show excellent agreement in calculation of bulk total water content averaged over the center of the pipe.

Bencic, Timothy J.↗

DOE OSTI2024

Metadynamics investigation of lanthanide solvation free energy landscapes and insights into separations energetics

Lanthanide ion solvation chemistry in nonaqueous phases is key to understanding and developing effective separation processes for these critical materials. Due to the complexity and inherent disorder of the solution phase, a comprehensive picture of the solvated metal ion is often difficult to generate solely from conventional spectroscopic approaches and electronic structure calculations, particularly in the extractant phase. In this work, we use classical molecular dynamics (MD) simulation with an advanced sampling technique, metadynamics, supplemented by experimental spectroscopy and speciation analysis, to measure lanthanide solvation free energy landscapes. We define coordination-based collective variables to probe the entire range of solvation configurations in the organic phase of lanthanum (La), europium (Eu), and lutetium (Lu) nitrate salts bound with a commonly used extractant, N,N′-dimethyl, N,N′-dioctylhexylethoxymalonamide (DMDOHEMA). The known lanthanide extraction trend of La ≈ Eu > Lu is readily explained by the measured free energy surfaces, which show consistent DMDOHEMA coordination from La to Eu, followed by loss of DMDOHEMA coordination from Eu to Lu. These simulations suggest how ligand crowding at the metal center can control selectivity, in this case resulting in the opposite extraction trend as observed with other conventional extractants, where the enthalpic contribution from increasing lanthanide charge density across the series dominates the extraction energetics. We also find that the presence of inner-sphere water, verified by time-resolved fluorescence, diversifies the accessible solvation structures. As a result, understanding solvation requires consideration of an entire thermodynamic ensemble, rather than the single dominant lowest-energy structure, as is often considered out of necessity in interpretation of spectroscopic data or in electronic structure-based ligand design approaches. In general, we demonstrate how metadynamics uniquely enables investigation of complex, multidimensional solvation energetic landscapes, and how it can explain selectivity trends where extraction is controlled by more complex mechanisms than simple charge density-based selectivity.

Wang, Xiaoyu↗

DOE OSTI2021

Direct double ionization of the Ar + M shell by a single photon

Direct double ionization of the Ar + (3p –1 ) ion by a single photon is investigated both experimentally and theoretically. The photon-ion merged-beams technique was employed at the Advanced Light Source in Berkeley, USA, to measure absolute cross sections in the energy range from 60 to 150 eV. In this range, three contributions to the double ionization of Ar + are to be expected: the removal of two 3p electrons, of a 3s and a 3p electron, and of two 3s electrons. Among the possible mechanisms leading to double ionization, the TS1 (two-step one) process dominates in the near-threshold region. In TS1, a photoelectron is ejected and, on its way out, knocks out a secondary electron. Here, this two-step mechanism is treated theoretically by multiplying the calculated cross section for direct single photoionization of a given subshell with the calculated (e, 2e) ionization probability for the ejected photoelectron to knock off a secondary electron. The calculated cross section is in very good agreement with the experiment.

74 ATOMIC AND MOLECULAR PHYSICS↗

NASA NTRS1975

Carbon dioxide sensor

Analytical techniques for measuring CO2 were evaluated and rated for use with the advanced extravehicular mobility unit. An infrared absorption concept using a dual-wavelength monochromator was selected for investigation. A breadboard carbon dioxide sensor (CDS) was assembled and tested. The CDS performance showed the capability of measuring CO2 over the range of 0 to 4.0 kPa (0 to 30 mmHg) P sub (CO2). The volume and weight of a flight configured CDS should be acceptable. It is recommended that development continue to complete the design of a flight prototype.

Source record↗

NASA NTRS1985

Laser Doppler velocimetry primer

Advanced research in experimental fluid dynamics required a familiarity with sophisticated measurement techniques. In some cases, the development and application of new techniques is required for difficult measurements. Optical methods and in particular, the laser Doppler velocimeter (LDV) are now recognized as the most reliable means for performing measurements in complex turbulent flows. And such, the experimental fluid dynamicist should be familiar with the principles of operation of the method and the details associated with its application. Thus, the goals of this primer are to efficiently transmit the basic concepts of the LDV method to potential users and to provide references that describe the specific areas in greater detail.

Bachalo, William D.↗

NASA NTRS1995

Development of advanced diagnostics for characterization of burning droplets in microgravity

Diagnostic techniques currently used for microgravity research are generally not as advanced as those used in earth based gravity experiments. Diagnostic techniques for measuring the instantaneous radial temperature profile (or temperature gradients) within the burning droplet do not exist. Over the past few years, Aerometrics has been researching and developing a rainbow thermometric technique for measuring the droplet temperatures of burning droplets. This technique has recently been integrated with the phase Doppler interferometric technique to yield a diagnostic instrument that can be used to simultaneously measure the size, velocity, and temperature of burning droplets in complex spray flames. Also, the rainbow thermometric technique has been recently integrated with a point-diffraction interferometric technique for measuring the instantaneous gas phase temperature field surrounding a burning droplet. These research programs, apart from being very successful, have also helped us identify other innovative techniques for the characterization of burning droplets. For example, new techniques have been identified for measuring the instantaneous regression rate of burning droplets. Also, there is the possibility of extracting the instantaneous radial temperature distribution or the temperature gradients within a droplet during transient heating. What is important is that these diagnostic techniques have the potential for making use of inexpensive, light-weight, and rugged devices such as diode lasers and linear CCD arrays. As a result, they can be easily packaged for incorporation into microgravity drop-test and flight-test facilities. Furthermore, with the use of linear CCD arrays, data rates as high as 10-100 kHz can be easily achieved. This data rate is orders of magnitude higher than what is currently achievable. In this research and development program, a compact and rugged diagnostic system will be developed that can be used to measure instantaneous fuel droplet diameter, droplet regression rate, and the droplet internal temperature profiles or gradients at very high data rates in microgravity experiments.

Sankar, Subramanian↗