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At least 217 records · Page 12

Five experiments in materials science for less than $10.00

Diffusion, twinning, fatigue, acoustic emission, and aging can be studied using readily available materials and the household oven. Each experiment can be expanded to a more extensive investigation of the properties of the material investigated, as well as other materials, and offers an opportunity for the student to learn about the relationship between engineering, science, society, and politics.

Spiegel, F. Xavier↗

Investigations on atomic-vapor-filter high-spectral-resolution lidar for temperature measurements

The temperature measurement by the analysis of Rayleigh scattered laser radiation with atomic vapor filters is investigated in both theory and laboratory experiments. Synthetic air is irradiated with a cw dye laser at 283 nano-meters, and the backscattered spectrum is analyzed with two lead vapor cells in one oven. Temperature measurements are carried out, and the effect of different parameters on the accuracy is investigated. Important aspects for the realization of a lidar are given.

Voss, E.↗

Huygens/ACP: An instrument for aerosols chemical composition measurements

The Aerosol Collector Pyrolyzer (ACP) which will be used aboard the Huygens probe is introduced. The scientific objectives, scientific rationale, and a technical description of the ACP are given. The ACP will sample the aerosols of the Titan's atmosphere in two regions, 160 to 60 and 60 to 25 km, respectively. In the first region, it will collect aerosol particles absorbed by a complex core (organic polymers) coated with absorbed or condensed molecules. The second collect will sample larger aerosols and the N2-CH4 droplets. In each sampling, the particles are collected on a metallic filter through which the atmospheric gas is pumped. The filter is then inserted into an oven connected to the Gas Chromatograph Mass Spectrometer (GCMS) Experiment which analyzes the gases produced during the heating of the samples. For each sample it will be possible to bring information on the nature and abundance of the volatile components contained in the particles and/or the composition of the photochemical core.

Israel, Guy↗

Experimental radiation cooled magnetrons for space

The heat disposal problem that occurs in the microwave generator of the Solar Power Satellite when it converts dc power from solar photovoltaic arrays into microwave power for transmission to earth is examined. A theoretical study is made of the radiation cooling of a magnetron directional amplifier, and some experimental data obtained from the QKH 2244 magnetron are presented. This instrument is an unpackaged microwave oven magnetron to which an anodized aluminum radiator has been attached and whose magnetic field is supplied by special samarium cobalt magnets.

Brown, W. C.↗

The development of an alternative thermoplastic powder prepregging technique

An alternative powder prepregging technique is discussed that is based on the deposition of powder onto carbon fibers that have been moistened using an ultrasonic humidifier. The dry fiber tow is initially spread to allow a greater amount of the fiber surface to be exposed to the powder, thus ensuring a significant amount of intimate contact between the fiber and the matrix. Moisture in the form of ultrafine water droplets is then deposited onto the spread fiber tow. The moisture promotes adhesion to the fiber until the powder can be tacked to the fibers by melting. Powdered resin is then sieved onto the fibers and then tacked onto the fibers by quick heating in a convective oven. This study focuses on the production of prepregs and laminates made with LaRC-TPI (thermoplastic polyimide) using this process. Although the process appears to be successful, early evaluation was hampered by poor interfacial adhesion. The adhesion problem, however, seems to be the result of a material system incompatibility, rather than being influenced by the process.

Ogden, A. L.↗

Adjustable-Pressure Mandrel For Making Composite Tubes

Inflatable inner mandrel enables application of any desired pressure (within reasonable limits) during curing stage in fabrication of fiber/matrix composite tube. Consists mainly of sheath of silicone rubber sealed on aluminum tube. Composite material laid up on mandrel and enclosed in rigid outer die. Sheath on inner mandrel inflated to requisite pressure and regulated during curing. Assembly then placed in oven and cured at specified temperature.

Jacoy, Paul J.↗

CONCAP 4: A Complex Autonomous Payload (CAP) for growing organic thin films in microgravity

A GAS facility has been developed for carrying out low temperature experiments. The arrangement being used on CONCAP IV-01 is designed for thin film growth in microgravity and can process up to twelve samples per mission. The nonlinear optical oven hardware can also be made suitable for other low temperature applications, such as gradient freeze and solution growth of crystals.

Carswell, W. E.↗

The millimeter-wave spectrum of CaH (X 2Sigma(+))

The millimeter-wave spectrum of the CaH and CaD radicals (X 2Sigma(+)) has been observed in the laboratory via direct absorption spectroscopy. The species were generated by the reaction of calcium vapor, produced in a Broida-type oven, with hydrogen atoms created in a microwave discharge. The six hyperfine components of the N = 0 yields 1 rotational transition of CaH near 254 GHz were resolved and their frequencies determined to an accuracy of +/- 100 kHz. The main hyperfine lines originating in the N = 0 yields 1, 1 yields 2, and 2 yields 3 rotational transitions of CaD were also detected. Spectroscopic constants were determined for both radicals from a nonlinear least squares fit to the data, using a 2Sigma Hamiltonian. These measurements constitute the first laboratory observation of CaH at high spectral resolution, and are essential to the detection of this radical in interstellar space.

Barclay, W. L., Jr.↗

Space Station Freedom food management

This paper summarizes the specification requirements for the Space Station Food System, and describes the system that is being designed and developed to meet those requirements. Space Station Freedom will provide a mix of frozen, refrigerated, rehydratable, and shelf stable foods. The crew will pre-select preferred foods from an approved list, to the extent that proper nutrition balance is maintained. A galley with freezers, refrigerators, trash compactor, and combination microwave and convection ovens will improve crew efficiency and productivity during the long Space Station Freedom (SSF) missions.

Whitehurst, Troy N., Jr.↗

The millimeter-wave spectrum of AlOH

The pure rotational spectrum of the AlOH and AlOD molecules in their X 1Sigma(+) (v = 0) ground electric states has been measured in the laboratory using direct absorption millimeter/submillimeter spectroscopy. The species were produced by the reaction of aluminum vapor, created in a Broida-type oven, with hydrogen peroxide or D2O2. Eight rotational transitions of AlOH and five transitions for AlOD were measured in the frequency range of 157-378 GHz to an accuracy better than +/- 75 kHz. Electric quadrupole interactions, arising from the aluminum nuclear spin of 5/2, were observed in the J = 4 - 5 and the J = 5 - 6 transitions of AlOH. The rotational constants of these molecules have been determined from a nonlinear least-squares fit to the data. The electric quadrupole coupling constant, eqQ, has been measured as well, and was found to have a value of -42.4 +/- 4.3 MHz. The spectra are consistent with quasi-linear ground states for AlOH and AlOD, as predicted by theory. AlOH is of astrophysical interest because of the relatively high cosmic abundance of aluminum.

Apponi, A. J.↗

Development of an advanced spacecraft tandem mass spectrometer

The purpose of this research was to apply current advanced technology in electronics and materials to the development of a miniaturized Tandem Mass Spectrometer that would have the potential for future development into a package suitable for spacecraft use. The mass spectrometer to be used as a basis for the tandem instrument would be a magnetic sector instrument, of Nier-Johnson configuration, as used on the Viking Mars Lander mission. This instrument configuration would then be matched with a suitable second stage MS to provide the benefits of tandem MS operation for rapid identification of unknown organic compounds. This tandem instrument is configured with a newly designed GC system to aid in separation of complex mixtures prior to MS analysis. A number of important results were achieved in the course of this project. Among them were the development of a miniaturized GC subsystem, with a unique desorber-injector, fully temperature feedback controlled oven with powered cooling for rapid reset to ambient conditions, a unique combination inlet system to the MS that provides for both membrane sampling and direct capillary column sample transfer, a compact and ruggedized alignment configuration for the MS, an improved ion source design for increased sensitivity, and a simple, rugged tandem MS configuration that is particularly adaptable to spacecraft use because of its low power and low vacuum pumping requirements. The potential applications of this research include use in manned spacecraft like the space station as a real-time detection and warning device for the presence of potentially harmful trace contaminants of the spacecraft atmosphere, use as an analytical device for evaluating samples collected on the Moon or a planetary surface, or even use in connection with monitoring potentially hazardous conditions that may exist in terrestrial locations such as launch pads, environmental test chambers or other sensitive areas. Commercial development of the technology could lead to a new family of environmental test instruments that would be small and portable, yet would give quick analyses of complex samples.

Drew, Russell C.↗

A new NASA LaRC Multi-Purpose Prepregging Unit

A multi-purpose prepregging machine has been designed and built for NASA Langley Research Center. The machine has numerous advantages over existing units due to its various modular components. Each of these can be used individually or simultaneously depending on the required prepregging method. A reverse roll coater provides the ability to prepare thin films from typical hot-melt thermoset formulations. Also, if necessary, the design allows direct fiber impregnation within the reverse roll coater gap. Included in the impregnation module is a solution dip tank allowing the fabrication of thermoplastic prepregs from solution. The proceeding modules within the unit consist of four nip stations, two hot-plates, a hot-sled option and a high temperature oven. This paper describes the advantages of such a modular construction and discusses the various processing combinations available to the prepregger. A variety of high performance prepreg material systems were produced on IM7 (Hercules) carbon fiber. These included LaRC RP46, a PMR-type resin processed from methanol and two polyamide acids, LaRC IA and LaRC ITPI, prpregged from N-methyl pyrrolidinone (NMP). Parameters involved in the production of these prepreg materials are presented as are the mechanical properties of the resulting good quality laminates. A brief introduction into the existing prepregging science is presented. Topics relating to solution prepregging are identified with a focus on the current research effort and its future development.

Wilkinson, S. P.↗

Helium in interplanetary dust particles

Helium and neon were extracted from fragments of individual stratosphere-collected interplanetary dust particles (IDP's) by subjecting them to increasing temperature by applying short-duration pulses of power in increasing amounts to the ovens containing the fragments. The experiment was designed to see whether differences in release temperatures could be observed which might provide clues as to the asteroidal or cometary origin of the particles. Variations were observed which show promise for elucidating the problem.

Nier, A. O.↗

A solar photovoltaic power system for use in Antarctica

A solar photovoltaic power system was designed and built at the NASA Lewis Research Center as part of the NASA/NSF Antarctic Space Analog Program. The system was installed at a remote field camp at Lake Hoare in the Dry Valleys, and provided a six-person field team with electrical power for personal computers and printers, lab equipment, lighting, and a small microwave oven. The system consists of three silicon photovoltaic sub-arrays delivering a total of 1.5 kWe peak power, three lead-acid gel battery modules supplying 2.4 kWh, and an electrical distribution system which delivers 120 Vac and 12 Vdc to the user. The system was modularized for ease of deployment and operation. Previously the camp has been powered by diesel generators, which have proven to be both noisy and polluting. The NSF, in an effort to reduce their dependence on diesel fuel from both an environmental and cost standpoint, is interested in the use of alternate forms of energy, such as solar power. Such a power system also will provide NASA with important data on system level deployment and operation in a remote location by a minimally trained crew, as well as validate initial integration concepts.

Kohout, Lisa L.↗

A solar photovoltaic power system for use in Antarctica

A solar photovoltaic power system was designed and built at the NASA Lewis Research Center as part of the NASA/NSF Antarctic Space Analog Program. The system was installed at a remote field camp at Lake Hoare in the Dry Valleys and provided a six-person field team with the power to run personal computers and printers, lab equipment, lightning, and a small microwave oven. The system consists of three silicon photovoltaic sub-arrays delivering 1.5 kW peak power, three lead-acid gel battery modules supplying 2.4 kWh, and electrical distribution system which delivers 120 Vac and 12 Vdc to the user. The system was modularized for each of deployment and operation. Previously the camp has been powered by diesel generators, which have proven to be both noisy and polluting. The NSF, in an effort to reduce their dependence on diesel fuel from both and environmental and cost standpoint is interested in the use of alternate forms of energy, such as solar power. Such a power system will also provide NASA with important data on system level deployment and operation in a remote location by a minimally trained crew, as well as validate initial integration concepts.

Kohout, Lisa L.↗

Skin exposure: Assessing the hazard in the workplace

An outline of the Occupational Safety and Health Agency's concerns of skin exposure to hazardous chemicals is presented, followed by the corresponding slide narrations. Specifically, dermatitis and skin absorption as compared to lung absorption are addressed. Lung versus skin exposure is examined for glycol ethers and acrylamide. Examples of skin exposure include PBC's in transformers, toluene and xylene from autobody work, polynuclear aromatics (PNA's) among Coke oven workers, toluene diisocyanate (TDI), and occupational chemical exposures in an academic medical center. Permeation through gloves in the semiconductor industry is addressed as evidence for the need to assess the effectiveness of PPE (Personal Protective Equipment). This leads to the revisions of the PPE standard and the Safety and Health Program standard.

Cummins, Kevin↗

An NMR study of microvoids in polymers

An understanding of polymer defect structures, like microvoids in polymeric matrices, is crucial to their fabrication and application potential. In this project guest atoms are introduced into the microvoids in PMR-15 and NMR is used to determine microvoid sizes and locations. Xenon is a relatively inert probe that would normally be found naturally in polymer or in NMR probe materials. There are two NMR active xenon isotopes, Xe-129 and Xe-131. The Xe atom has a very high polarizability, which makes it sensitive to the intracrystalline environment of polymers. Interactions between the Xe atoms and the host matrix perturb the Xe electron cloud, deshielding the nuclei, and thereby expanding the range of the observed NMR chemical shifts. This chemical shift range which may be as large as 5000 ppm, permits subtle structural and chemical effects to be studied with high sensitivity. The Xe(129)-NMR line shape has been found to vary in response to changes in the pore symmetry of the framework hosts line Zeolites and Clathrasil compounds. Before exposure to Xe gas, the PMR-15 samples were dried in a vacuum oven at 150 C for 48 hours. The samples were then exposed to Xe gas at 30 psi for 72 hours and sealed in glass tubes with 1 atmosphere of xenon gas. Xenon gas at 1 atmosphere was used to tune up the spectrometer and to set up the appropriate NMR parameters. A single Xe-129 line at 83.003498 Mhz (with protons at 300 Mhz) was observed for the gas. With the xenon charged PMR-15 samples, a second broader line is observed 190 ppm downfield from the gas line (also observed). The width of the NMR line from the Xe-129 absorbed in the polymer is at least partially due to the distribution of microvoid sizes. From the chemical shift (relative to the gas line) and the line width, we estimate the average void sizes to be 2.74 +/- 0.20 angstroms. Since Xe-129 has such a large chemical shift range (approximately 5000 ppm), we expect the chemical shift anisotropy to contribute to the line width (delta upsilon = 2.5 kHz).

Toy, James↗

Static measurement of the thickness of the ablative coating of the solid rocket boosters

The Solid Rocket Boosters (SRB's) used to launch the Space Shuttle are coated with a layer of ablative material to prevent thermal damage when they reenter the earth's atmosphere. The coating consists of a mixture of cork, glass, and resin. A new coating (Marshall Convergent Coating, MCC-2) was recently developed that is environmentally complaint. The coating must meet certain minimum thickness standards in order to protect the SRB. The coating is applied by a robot controlled nozzle that moves from the bottom to top, as the rocket part rotates on a table. Several coats are applied, building up to the desired thickness. Inspectors do a limited amount of destructive 'wet' testing. This involves an inspector inserting a rod in the wet coating and removing the rod. This results in a hole that, of course, must be patched later. The material is cured and the thickness is measured. There is no real-time feedback as the coating is being applied. Although this might seem like the best way to control thickness, the problems with 'blowback' (reflected material covering the sensor) are formidable, and have not been solved. After the thermal coating is applied, a protective top coat is applied. The SRB part is then placed in a oven and baked to harden the surface. The operations personnel then measure the thickness of the layer using the Kaman 7200 Displacement Measuring System. The probe is placed on the surface. One person (the inspector) reads the instrument, while another(the technician) records the thickness. Measurements are taken at one foot intervals. After the measurements are taken, the number of low readings is tabulated. If more than 10 percent of the points fall below the minimum value, there is a design review, and the part may be stripped of coating, and a new coating is applied. There is no other analysis.

Harrison, Harry C.↗