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NASA NTRS2000

Long Term Degradation of Resin for High Temperature Composites

The durability of polymer matrix composites exposed to harsh environments is a major concern. Surface degradation and damage are observed in polyimide composites used in air at 125 to 300 C. It is believed that diffusion of oxygen into the material and oxidative chemical reactions in the matrix are responsible. Previous work has characterized and modeled diffusion behavior, and thermogravimetric analyses (TGAs) have been carried out in nitrogen, air, and oxygen to provide quantitative information on thermal and oxidative reactions. However, the model developed using these data was not able to capture behavior seen in isothermal tests, especially those of long duration. A test program that focuses on lower temperatures and makes use of isothermal tests was undertaken to achieve a better understanding of the degradation reactions under use conditions. A new low-cost technique was developed to collect chemical degradation data for isothermal tests lasting over 200 hr in the temperature range 125 to 300 C. Results indicate complex behavior not captured by the previous TGA tests, including the presence of weight-adding reactions. Weight gain reactions dominated in the 125 to 225 C temperature range, while weight loss reactions dominated beyond 225 C. The data obtained from isothermal tests was used to develop a new model of the material behavior. This model was able to fully capture the behavior seen in the tests up to 275 C. Correlation of the current model with both isothermal data at 300 C and high rate TGA test data is mediocre. At 300 C and above, the reaction mechanisms appear to change. Attempts (which failed) to measure non-oxidative degradation indicate that oxidative reactions dominate the degradation at low temperatures. Based on this work, long term isothermal testing in an oxidative atmosphere is recommended for studying the degradation behavior of this class of materials.

Patekar, Kaustubh A.↗

NASA NTRS1986

Translucent molecular clouds: Theory and observations

Few suitable stars behind molecular clouds have been identified. A limited survey was performed of interstellar lines toward highly reddened stars in the southern sky, using the ESO 1.4 m CAT telescope with a Reticon detector, and the Cerro Tololo 4 m telescope equipped with a GEC charge coupled device (CCD) detector. Because of the reduced extinction at longer wavelengths, molecules were searched for with transitions in the red part of the spectrum such as C2 and CN. For some lines-of-sight for which C2 was detected, the 4300 A line of CH was also observed. Absorption lines of interstellar C2 around 8750 A were detected in the spectra of about 1/4 of the 36 observed stars. The inferred C2 column densities range between 10 to the 13th power and 10 to the 14th power sq. cm., and are up to an order of magnitude larger than those found for diffuse clouds. The observed column densities of CH correlate very well with those of C2 over this range. In contrast, the measured column densities of CN vary by orders of magnitude between the various regions, and they do not correlate with those of C2 and CH. The observed rotational population distribution of C2 also provides information about the physical conditions in the clouds. Models of translucent molecular clouds have been constructed along the lines described by van Dishoeck and Black (1986) for diffuse clouds. The models compute accurately the fractions of atomic and molecular hydrogen as functions of depth into the clouds, as well as the excitation of H2 by ultraviolet pumping. They also incorporate a detailed treatment of the photodissociation processes of the molecules (cf. van Dishoeck 1986), which play an important role in the chemistry up to depths of about 3 mag.

Vandishoeck, E. F.↗

NASA NTRS1996

NASA/DOD Aerospace Knowledge Diffusion Research Project. Paper 56: Technical Communications in Engineering and Science: The Practices Within a Government Defense Laboratory

Research in recent decades has identified the varied information needs of engineers versus scientists. While most of that research looked at the differences among organizations, we surveyed engineers and scientists within a single Air Force research and development laboratory about their information gathering, usage, and production practices. The results of the Phillips Laboratory survey confirm prior assumptions about distinctions between engineering and science. Because military employees responded at a much higher rate than civilian staff, the survey also became an opportunity to profile a little-known segment of the engineer/scientist population. In addition to the effect Phillips Laboratory's stated mission may have on member engineers and scientists, other factors causing variations in technical communication and information-related activities are identified.

VonSeggern, Marilyn↗

NASA NTRS1991

NASA/DOD Aerospace Knowledge Diffusion Research Project. Report 4: Summary report to phase 1 respondents

Phase 1 of a 4 part study was undertaken studying the use of scientific and technical information (STI) by U.S. aerospace engineers and scientists. Specific attention was paid to institutional and socioeconomic variables and to the step-by-step process of information gathering used by the respondents. Data were collected by means of three self administered mail-back questionnaires. The approximately 34,000 members of the American Institute of Aeronautics and Astronautics (AIAA) served as the study population. More than 65 percent of the randomly selected respondents returned the questionnaires in each of the three groups. Respondents relied more heavily upon informal sources of information than formal sources and turned to librarians and other technical information specialists only when they did not obtain results via informal means or their own formal searches.

Pinelli, Thomas E.↗

NASA NTRS1976

Flow and heat transfer measurements in a pseudo-shock region with surface cooling

An experimental investigation was conducted to acquire information on the flow structure, mean flowfield, and temperature distributions in a pseudo-shock region in a supersonic diffuser with surface cooling. The Mach number upstream was 2.9, and the wall to stagnation temperature ratio was 0.44. A Mach-disk-like shock wave emanated from the thin separated flow region near the beginning of the compression region, and reattachment occurred one diameter downstream so that the flow was not separated over most of the pseudo-shock region. The flow compression was a shock-free, predominantly viscous process. Along the pseudo-shock region the measured heat-transfer coefficient increased approximately as the 0.8 power of the measured wall static pressure. The estimated wall shear stress increased downstream of flow attachment, but was still considerably less than the upstream value.

Cuffel, R. F.↗

NASA NTRS1986

Planetary optical and infrared imaging

Images were acquired of a circumstellar disk of orbiting material around the nearby star beta Pictoris. This material is believed to be associated with the formation of planets and provides a first look at a planetary system much younger than our own. Preliminary work was also done to acquire multicolor photometric data and polarimetry on the beta Pictoris disk as well. A coronagraphic search for other proto-planetary systems is also underway. Coronagraphic imaging provided the first clear images and a determination of the geometric albedo of the rings of Uranus. A search for material around the asteroid Amphitrite showed that the region around the asteroid was free of particles larger than 500 meters in radius or diffuse material with an optical depth larger than .000001. NASA IRTF infrared images of Jupiter and Saturn are providing information on the relative heights and cloud top temperatures of atmospheric features.

Terrile, R. J.↗

NASA NTRS2002

Organic Synthesis in Space

This talk will review our current understanding of the synthesis of organic molecules in space, with particular emphasis on the synthesis of those compounds that may be of prebiotic interest. The talk will address the possibility that molecules created in the interstellar medium may play a role in the origin and evolution of life on planetary surfaces. The various organic and volatile compounds that are now known or suspected to exist in a variety of space environments (stellar outflows, the diffuse interstellar medium, dense molecular clouds, protostellar nebulae, and planetesimal parent bodies in planetary systems) will be reviewed. This information comes largely from the combined applications of observational infrared and radio spectroscopy, laboratory astrophysical simulations, and theoretical astrochemistry. This will be followed by a discussion of the evidence, largely gathered from the laboratory isotopic study of extraterrestrial materials (meteorites and cosmic dust), that interstellar materials, including organics, can and do survive the transition from the interstellar space into forming stellar systems. Once there, some of this material can be delivered largely unaltered to planetary surfaces where it can play key roles in the origin and subsequent evolution of life.

Sandford, Scott A.↗

NASA NTRS1985

Fourier transform-infrared spectroscopic methods for microbial ecology: analysis of bacteria, bacteria-polymer mixtures and biofilms

Fourier transform-infrared (FT-IR) spectroscopy has been used to rapidly and nondestructively analyze bacteria, bacteria-polymer mixtures, digester samples and microbial biofilms. Diffuse reflectance FT-IR (DRIFT) analysis of freeze-dried, powdered samples offered a means of obtaining structural information. The bacteria examined were divided into two groups. The first group was characterized by a dominant amide I band and the second group of organisms displayed an additional strong carbonyl stretch at approximately 1740 cm-1. The differences illustrated by the subtraction spectra obtained for microbes of the two groups suggest that FT-IR spectroscopy can be utilized to recognize differences in microbial community structure. Calculation of specific band ratios has enabled the composition of bacteria and extracellular or intracellular storage product polymer mixtures to be determined for bacteria-gum arabic (amide I/carbohydrate C-O approximately 1150 cm-1) and bacteria-poly-beta-hydroxybutyrate (amide I/carbonyl approximately 1740 cm-1). The key band ratios correlate with the compositions of the material and provide useful information for the application of FT-IR spectroscopy to environmental biofilm samples and for distinguishing bacteria grown under differing nutrient conditions. DRIFT spectra have been obtained for biofilms produced by Vibrio natriegens on stainless steel disks. Between 48 and 144 h, an increase in bands at approximately 1440 and 1090 cm-1 was seen in FT-IR spectra of the V. natriegens biofilm. DRIFT spectra of mixed culture effluents of anaerobic digesters show differences induced by shifts in input feedstocks. The use of flow-through attenuated total reflectance has permitted in situ real-time changes in biofilm formation to be monitored and provides a powerful tool for understanding the interactions within adherent microbial consortia.

NASA Discipline Number 61-10↗

NASA NTRS1991

Evaluating some computer enhancement algorithms that improve the visibility of cometary morphology

The observed morphology of cometary comae is determined by ejection circumstances and the interaction of the ejected material with the local environment. Anisotropic emission can provide useful information on such things as orientation of the nucleus, location of active areas on the nucleus, and the formation of ion structure near the nucleus. However, discrete coma features are usually diffuse, of low amplitude, and superimposed on a steep intensity gradient radial to the nucleus. To improve the visibility of these features, a variety of digital enhancement algorithms were employed with varying degrees of success. They usually produce some degree of spatial filtering, and are chosen to optimize visibility of certain detail. Since information in the image is altered, it is important to understand the effects of parameter selection and processing artifacts can have on subsequent interpretation. Using the criteria that the ideal algorithm must enhance low contrast features while not introducing misleading artifacts (or features that cannot be seen in the stretched, unprocessed image), the suitability of various algorithms that aid cometary studies were assessed. The strong and weak points of each are identified in the context of maintaining positional integrity of features at the expense of photometric information.

Larson, S. M.↗

NASA NTRS1994

NASA/DOD Aerospace Knowledge Diffusion Research Project. Report 23: The communications practices of US aerospace engineering faculty and students: Results of the phase 3 survey

The U.S. government technical report is a primary means by which the results of federally funded research and development (R&D) are transferred to the U.S. aerospace industry. However, little is known about this information product in terms of its actual use, importance, and value in the transfer of federally funded R&D. To help establish a body of knowledge, the U.S. government technical report is being investigated as part of the NASA/DOD Aerospace Knowledge Diffusion Research Project. In this report, we summarize the literature on technical reports and provide a model that depicts the transfer of federally funded aerospace R&D via the U.S. government technical report. We present results from our investigation of aerospace knowledge diffusion vis-a-vis the U.S. government technical report, and present the results of research that investigated aerospace knowledge diffusion vis-a-vis U.S. aerospace engineering faculty and students.

Pinelli, Thomas E.↗

NASA NTRS1972

Techniques in balloon X-ray astronomy.

Since the first balloon observation of the Crab Nebula balloon data have provided much information on the positions, spectra, time variability and pulsed nature of localized sources, and on the spectrum and isotropy of diffuse galactic and universal components. Measurements are limited to energies above about 20 keV by atmospheric attenuation at 2 to 3 g/sq cm depth and to below several hundred keV by detector sensitivity. Detectors usually consist of large-area Na I or Cs I scintillation counters with anticoincidence collimators for rejection of charged particles and scattered X-rays. Proportional counters are occasionally used at lower energies and solid-state detectors are used where extreme energy resolution is important. The instruments require a pointing capability on the order of 1.0 to 0.1 deg, depending on the collimator aperture. Digital data is either recorded on board or telemetered using a PCM technique.

Peterson, L. E.↗

NASA NTRS1980

The diffuse UV background

The diffuse radiation field in the UV (900-3,000 A) affects the structure of galactic molecular clouds and conveys important information concerning the physical characteristics and spatial distribution of gas and dust in the universe. Continuum emission in this range is probably dominated by interstellar dust scattering in our galaxy. For view directions and angular resolutions allowing observations in the rifts between galactic dust clouds, the background due to the integrated light of spiral galaxies may be detected, providing important information on their structure and evolution. The redshifted emission from an intergalactic medium may be observable in the regions between nearby bright galaxies. Present observations provide weak constraints on the radiation field required to ionize the intergalactic medium at the level required by the Gunn-Peterson test.

Paresce, F.↗

NASA NTRS1981

Transport properties associated with entry into the atmosphere of Titan

In this paper the transport properties in the atmosphere of Titan and at the shock front and the probe surface for non-ablative entry into Titan's atmosphere are calculated, using the kinetic theory of gases. The species N2, H2, CH4, HCN, N, and H contribute to the transport properties under these conditions. The transport properties were calculated by using accurate potential energy curves for each of the thirteen two-body interactions which occur between these species. Results are given for the binary diffusion coefficients, the non-reactive and reactive thermal conductivity, and the viscosity from 1000 K to 8000 K. This information is needed for calculating flowfield properties and surface heating rates. The most important conclusions are that the non-reactive thermal conductivity is much larger behind the shock layer than it is in the ambient atmosphere and that the nonreactive thermal conductivity appears to be nearly constant in the shock layer.

Flori, B.↗

NASA NTRS2004

Reduced Gravity Studies of Soret Transport Effects in Liquid Fuel Combustion

Soret transport, which is mass transport driven by thermal gradients, can be important in practical flames as well as laboratory flames by influencing transport of low molecular weight species (e.g., monatomic and diatomic hydrogen). In addition, gas-phase Soret transport of high molecular weight fuel species that are present in practical liquid fuels (e.g., octane or methanol) can be significant in practical flames (Rosner et al., 2000; Dakhlia et al., 2002) and in high pressure droplet evaporation (Curtis and Farrell, 1992), and it has also been shown that Soret transport effects can be important in determining oxygen diffusion rates in certain classes of microgravity droplet combustion experiments (Aharon and Shaw, 1998). It is thus useful to obtain information on flames under conditions where Soret effects can be clearly observed. This research is concerned with investigating effects of Soret transport on combustion of liquid fuels, in particular liquid fuel droplets. Reduced-gravity is employed to provide an ideal (spherically-symmetrical) experimental model with which to investigate effects of Soret transport on combustion. The research will involve performing reduced-gravity experiments on combustion of liquid fuel droplets in environments where Soret effects significantly influence transport of fuel and oxygen to flame zones. Experiments will also be performed where Soret effects are not expected to be important. Droplets initially in the 0.5 to 1 mm size range will be burned. Data will be obtained on influences of Soret transport on combustion characteristics (e.g., droplet burning rates, droplet lifetimes, gas-phase extinction, and transient flame behaviors) under simplified geometrical conditions that are most amenable to theoretical modeling (i.e., spherical symmetry). The experiments will be compared with existing theoretical models as well as new models that will be developed. Normal gravity experiments will also be performed.

Shaw, Benjamin D.↗

NASA NTRS1994

NADA/DOD Aerospace Knowledge Diffusion Research Project. Report number 19: The US government technical report and the transfer of federally funded aerospace R/D: An analysis of five studies

The U.S. government technical report is a primary means by which the results of federally funded research and development are transferred to the U.S. aerospace industry. However, little is known about this information product in terms of its actual use, importance, and value in the transfer of federally funded R&D. To help establish a body of knowledge, the U.S. government technical report is being investigated as part of the 'NASA/DoD Aerospace Knowledge Diffusion Research Project'. In this report, we summarize the literature on technical reprts and provide a model that depicts the transfer of federally funded aerospace R&D via the U.S. government technical report. We present results from five studies of our investigation of aerospace knowledge diffusion vis-a-vis the U.S. government technical report and close with a brief overview of on-going research into the use of the U.S. government technical report as a rhetorical device for transferring federally funded aerospace R&D.

Pinelli, Thomas E.↗

NASA NTRS1994

NASA/DOD Aerospace Knowledge Diffusion Research Project. Report 25: The technical communications practices of British aerospace engineers and scientists: Results of the phase 4 RAeS mail survey

Pinelli, Thomas E.↗

NASA NTRS1994

NASA/DOD Aerospace Knowledge Diffusion Research Project. Report 24: The technical communications practices of US aerospace engineers and scientists: Results of the phase 1 SAE mail survey

Pinelli, Thomas E.↗

NASA NTRS1994

NASA/DOD Aerospace Knowledge Diffusion Research Project. Report 31: The technical communications practices of US aerospace engineers and scientists: Results of the phase 1 SME mail survey

The U.S. government technical report is a primary means by which the results of federally funded research and development (R&D) are transferred to the U.S. aerospace industry. However, little is known about this information product in terms of its actual use, importance, and value in the transfer of federally funded R&D. To help establish a body of knowledge, the U.S. government technical report is being investigated as part of the NASA/DOD Aerospace Knowledge Diffusion Research Project. In this report, we summarize the literature on technical reports and provide a model that depicts the transfer of federally funded aerospace R&D via the U.S. government technical report. We present results from our investigation of aerospace knowledge diffusion vis-a-vis the U.S. government technical communications practices of U.S. aerospace engineers and scientists affiliated with, not necessarily belonging to, the Society of Manufacturing Engineers (SME).

Pinelli, Thomas E.↗