Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “grazing incidence”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 217 records · Page 12
All sourcesNASA NTRSDOE OSTI
NASA NTRS2016

Performance of NICER Flight X-Ray Concentrator

Neutron star Interior Composition ExploreR (NICER) is a NASA instrument to be onboard International Space Station, which is equipped with 56 pairs of an X-ray concentrator (XRC) and a silicon drift detector for high timing observations. The XRC is based on an epoxy replicated thin aluminum foil X-ray mirror, similar to those of Suzaku and ASTRO-H (Hitomi), but only a single stage parabolic grazing incidence optic. Each has a focal length of 1.085 m and a diameter of 105 mm, with 24 confocally aligned parabolic shells. Grazing incident angles to individual shells range from 0.4 to 1.4 deg. The flight 56 XRCs have been completed and successfully delivered to the payload integration. All the XRC was characterized at the NASA/GSFC 100-m X-ray beamline using 1.5 keV X-rays (some of them are also at 4.5 keV). The XRC performance, effective area and point spread function, was measured by a CCD camera and a proportional counter. The average effective area is about 44 sq cm at 1.5 keV and about 18 sq cm at 4.5 keV, which is consistent with a micro-roughness of 0.5 nm from individual shell reflectivity measurements. The XRC focuses about 91% of X-rays into a 2mm aperture at the focal plane, which is the NICER detector window size. Each XRC weighs only 325 g. These performance met the project requirement. In this paper, we will present summary of the flight XRC performance as well as co-alignment results of the 56 XRCs on the flight payload as it is important to estimate the total effective for astronomical observations.

X-ray concentrator↗
DOE OSTI2020

Use of in Situ Synchrotron Techniques to Probe the Oxidized Surface of Molybdenum Nitride Oxygen Reduction Electrocatalysis

The development of active and stable earth-abundant catalysts for the oxygen reduction reaction (ORR) is needed for widespread, economic development of fuel cell technologies. Designing and optimizing these non-platinum group metals is challenging, however, because they are susceptible to composition and structure changes, including dissolution, oxidation, and corrosion, both in air and under reaction conditions. To identify the active surface, and thus understand the properties that affect activity, the catalyst surface must be characterized in situ. Herein, we utilize a grazing incidence electrochemical cell to investigate in situ composition and morphology changes of a molybdenum nitride (Mo-N) thin film catalyst using grazing incidence x-ray absorption spectroscopy (GI-XAS) and x-ray reflectivity (XRR). In rotating ring disk electrode measurements, we find that the activity, selectivity, stability, and capacitance of the Mo-N catalyst is dependent on the maximum potential to which it has been exposed. Specifically, the overpotential required to reach -2 mA cm-2geo decreases by over 90 mV when the maximum potential is increased from 0.3 to 0.8 V vs RHE (Figure 1). Because the Mo-N oxidizes rapidly in air, ex situ characterization methods including x-ray photoelectron spectroscopy and time-of-flight secondary ion mass spectrometry can provide only limited insight into these in situ catalyst changes. Using in situ GI-XAS measurements at applied potentials between 0.3 and 0.9 V vs RHE, however, we are able to determine that the surface of the film oxidizes and becomes more amorphous when exposed to increasingly higher potentials (Figure 1). Furthermore, the surface remains oxidized on the order of several hours when returned to "ORR relevant potentials" (< 0.6 V vs RHE), indicating that this surface-oxidized nitride is the active surface for ORR. Using in situ XRR measurements, we find that there is no change in surface roughness at potentials below 0.7 V vs RHE, but the film roughens significantly at 0.8 V vs RHE, correlating with ex situ measurements of Mo dissolution at this potential (Figure 1). We therefore conclude that the intrinsic activity of the Mo-N catalyst increases when exposed to potentials up to 0.7 V vs RHE, while above that potential activity enhancements are due to the exposure of more active sites through dissolution. The in situ electrochemical surface-sensitive x-ray characterization as used here is a promising methodology for understanding and leveraging surface dynamics to improve the performance of non-traditional catalysts.

Kreider, Melissa↗
NASA NTRS2015

SuperHERO: Design of a New Hard X-Ray Focusing Telescope

SuperHERO is a hard x-ray (20-75 keV) balloon-borne telescope, currently in its proposal phase, that will utilize high angular-resolution grazing-incidence optics, coupled to novel CdTe multi-pixel, fine-pitch (250 micrometers) detectors. The high-resolution electroformed-nickel, grazing-incidence optics were developed at MSFC, and the detectors were developed at the Rutherford Appleton Laboratory in the UK, and are being readied for flight at GSFC. SuperHERO will use two active pointing systems; one for carrying out astronomical observations and another for solar observations during the same flight. The telescope will reside on a light-weight, carbon-composite structure that will integrate the Wallops Arc Second Pointer into its frame, for arcsecond or better pointing. This configuration will allow for Long Duration Balloon flights that can last up to 4 weeks. This next generation design, which is based on the High Energy Replicated Optics (HERO) and HERO to Explore the Sun (HEROES) payloads, will be discussed, with emphasis on the core telescope components.

SuperHERO↗
NASA NTRS1986

An extreme ultraviolet telescope with no soft X-ray response

While EUV grazing incidence telescopes of conventional design exhibit a substantial X-ray response as well as an extreme UV response, and existing bandpass filters for the transmission of radiation longward of 400 A also transmit soft X-rays, the grazing incidence telescope presented suppresses this soft X-ray throughput through the incorporation of a Wolter Schwarzschild Type II mirror with large graze angles. The desirable features of an EUV photometric survey telescope are retained. An instrument of this design will be flown on the EUE mission, in order to make a survey of the sky at wavelengths longer than 400 A.

Finley, David S.↗
NASA NTRS1990

Reflected Sunlight Reduction and Characterization for a Deep-Space Optical Receiver Antenna (DSORA)

A baffle system for the elimination of first-order specular and diffuse reflection of sunlight from the sunshade of a deep-space optical receiver telescope is presented. This baffle system consists of rings of 0.5cm blades spaced 2.5 cm apart on the walls of GO hexagonal sunshade tubes that combine to form the telescope sunshade. The shadow cast by the blades, walls, and rims of the tubes prevent all first-order reflections of direct sunlight from reaching the primary mirror of the telescope. A reflection model of the sunshade without baffles is also presented for comparison. Since manufacturers of absorbing surfaces do not measure data near grazing incidence, the reflection properties at anticipated angles of incidence must be characterized. A description of reflection from matte surfaces in term of bidirectional reflection distribution function (BRDF) is presented along with a discussion of measuring BRDF near grazing incidence.

Clymer, B. D.↗
NASA NTRS2000

Astronomical X-Ray Optics

Over the past two decades, grazing incidence optics have transformed observational x-ray astronomy into a major scientific discipline at the cutting edge of research in astrophysics and cosmology. This review summarizes the fundamental design principles of grazing incidence optics for astronomical applications, describes the capabilities of the current generation of x-ray telescopes, and explores several avenues of future development.

Joy, M. K.↗
NASA NTRS2008

HERO: A Balloon-Borne Hard-X-Ray Focusing Telescope

HERO, for High Energy Replicated Optics, is an evolutionary balloon payload featuring hard-x-ray grazing-incidence nickel optics. The HERO payload is designed to perform high-sensitivity, fine spatial resolution observations of galactic and extragalactic sources in an energy range that is as yet unexplored with grazing-incidence optics. A proof-of-concept flight with just 6 x-ray mirrors was completed in 2001 and captured the first focused hard-x-ray images galactic sources. Since that time, the payload has been greatly expanded and now features 100, in-house-fabricated mirror shells with an attendant large increase in sensitivity. In its current form, HERO was flown in 2007, from Fort Sumner, NM, and is schedules to fly again in September 2009, from Alice Springs, NT. Full details of the HERO payload will be provided in this presentation together with a discussion of the challenges of flying moderate resolution x-ray optics from a balloon platform.

Ramsey, Brian↗
NASA NTRS1988

Electromagnetic scattering by pyramidal and wedge absorber

Electromagnetic scattering from pyramidal and wedge absorbers used to line the walls of modern anechoic chambers is measured and compared with theoretically predicted values. The theoretical performance for various angles of incidence is studied. It is shown that a pyramidal absorber scatters electromagnetic energy more as a random rough surface does. The apparent reflection coefficient from an absorber wall illuminated by a plane wave can be much less than the normal absorber specifications quoted by the manufacturer. For angles near grazing incidence, pyramidal absorbers give a large backscattered field from the pyramid side-faces or edges. The wedge absorber was found to give small backscattered fields for near-grazing incidence. Based on this study, some new guidelines for the design of anechoic chambers are advocated because the specular scattering models used at present do not appear valid for pyramids that are large compared to the wavelength.

Dewitt, Brian T.↗
NASA NTRS2015

Nested Focusing Optics for Compact Neutron Sources

NASA's Marshall Space Flight Center, the Massachusetts Institute of Technology (MIT), and the University of Alabama Huntsville (UAH) have developed novel neutron grazing incidence optics for use with small-scale portable neutron generators. The technology was developed to enable the use of commercially available neutron generators for applications requiring high flux densities, including high performance imaging and analysis. Nested grazing incidence mirror optics, with high collection efficiency, are used to produce divergent, parallel, or convergent neutron beams. Ray tracing simulations of the system (with source-object separation of 10m for 5 meV neutrons) show nearly an order of magnitude neutron flux increase on a 1-mm diameter object. The technology is a result of joint development efforts between NASA and MIT researchers seeking to maximize neutron flux from diffuse sources for imaging and testing applications.

Nabors, Sammy A.↗
NASA NTRS1982

High resolution X-ray scattering measurements

The results of high angular resolution grazing incidence scattering measurements of highly polished, coated optical flats in the X-ray spectral range of 1.5 to 6.4 keV are reported. The interpretation of these results in terms of surface microtopography is presented and the implications for grazing incidence X-ray imaging are discussed.

Zombeck, M. V.↗
NASA NTRS2012

Toward Active X-ray Telescopes II

In the half century since the initial discovery of an astronomical (non-solar) x-ray source, the sensitivity for detection of cosmic x-ray sources has improved by ten orders of magnitude. Largely responsible for this dramatic progress has been the refinement of the (grazing-incidence) focusing x-ray telescope. The future of x-ray astronomy relies upon the development of x-ray telescopes with larger aperture areas (greater than 1 m2) and finer angular resolution (less than 1.). Combined with the special requirements of grazing-incidence optics, the mass and envelope constraints of space-borne telescopes render such advances technologically challenging.requiring precision fabrication, alignment, and assembly of large areas (greater than 100 m2) of lightweight (approximately 1 kg m2 areal density) mirrors. Achieving precise and stable alignment and figure control may entail active (in-space adjustable) x-ray optics. This paper discusses relevant programmatic and technological issues and summarizes progress toward active x-ray telescopes.

O'Dell, Stephen L.↗
NASA NTRS1983

High efficiency spectrographs for the EUV and soft X-rays

The use of grazing incidence optics and reflection grating designs is shown to be a method that improves the performance of spectrographs at wavelengths shorter than 1200 A. Emphasis is laid on spectroscopic designs for X ray and EUV astronomy, with sample designs for an objective reflection grating spectrograph (ORGS) and an echelle spectrograph for wavelengths longer than 100 A. Conical diffraction allows operations at grazing incidence in the echelle spectrograph. In ORGS, the extreme distance of X ray objects aids in collimating the source radiation, which encounters conical diffraction within the instrument, proceeds parallel to the optical axis, and arrives at the detector. A series of gratings is used to achieve the effect. A grazing echelle is employed for EUV observations, and offers a resolution of 20,000 over a 300 A bandpass.

Cash, W.↗
NASA NTRS1979

Space optics: Imaging X-ray optics workshop; Proceedings of the Seminar, Huntsville, Ala., May 22-24, 1979

The papers in this volume are broadly based and represent a comprehensive summary of past achievements, new designs, techniques and future plans in space optics. The design, construction, testing and use of grazing incidence optics have played an integral role in the advance of X-ray astronomy. Topics of interest include a cosmic X-ray telescope for ARIES rocket observations, quest for ultrahigh resolution in X-ray optics, optical coating techniques for Wolter-type substrates, astronomical applications of grazing incidence telescopes with polynomial surfaces, and a paraboloidal X-ray telescope mirror for solar coronal spectroscopy.

Weisskopf, M.↗
DOE OSTI2020

Towards isolated attosecond electron bunches using ultrashort-pulse laser-solid interactions

We investigate MeV-level attosecond electron bunches from ultrashort-pulse laser-solid interactions through similarities between experimental and simulated electron energy spectra. We show measurements of the bunch duration and temporal structure from particle-in-cell simulations. The experimental observation of such bunches favors specular reflection direction when focusing the laser pulse onto a subwavelength boundary of thick overdense plasmas at grazing incidence. Particle-in-cell simulation further reveals that the attosecond duration is a result of ultra-thin (~tenth of a micron) gaps of zero electromagnetic energy density in the modulated reflected radiation, while the bunching (locally peaked electron concentration) comes from the highly-directional electron angular distribution acquired by the electrons in a grazing incidence setup. To isolate a single electron bunch, we perform simulations using 1-cycle laser pulses and analyze the effect of carrier-envelop phase with particle tracking. The duration of the electron bunch can be further decreased by increasing the laser intensity and the focal spot size, while its direction can be changed by tuning the preplasma density gradient.

High-harmonic generation↗
NASA NTRS1986

FUSE/Lyman grant

A variety of options for a short wavelength spectrometer for the Lyman telescope has been studied, and the optimum configuration for this instrument identified. In this spectrometer option study it is assumed (consistent with performance goals outlined by the project) that the instrument, whose prime spectral domain is 900-12000A, will incorporate a grazing incidence telescope which will maintain good collecting efficiency down to 100A. In particular it is assumed that the telescope will have an effective focal length of 10 meters, an image quality of 1.5", and will provide a diverging f/10 beam. Designs compatible with this telescope are analyzed, and it is determined that a two-element grazing incidence spectrometer using as its first optic an ellipsoid to re-focus the beam and a varied line-space plane diffraction grating to disperse the light is the best overall design. This spectrometer could be fed by a small pick-off mirror located just behind the prime focus of the telescope and would clear the light path when not in use. A test of the diffraction efficiency of a low blaze angle grating is undertaken, which is the only technical uncertainty in the spectrometer design.

Hurwitz, M.↗
NASA NTRS2011

The Focusing Optics X-Ray Solar Imager: FOXSI

The Focusing Optics x-ray Solar Imager (FOXSI) is a sounding rocket payload funded under the NASA Low Cost Access to Space program to test hard x-ray (HXR) focusing optics and position-sensitive solid state detectors for solar observations. Today's leading solar HXR instrument, the Reuven Ramaty High Energy Solar Spectroscopic Imager (RHESSI) provides excellent spatial (2 arcseconds) and spectral (1 keV) resolution. Yet, due to its use of an indirect imaging system, the derived images have a low dynamic range (typically <10) and sensitivity. These limitations make it difficult to study faint x-ray sources in the solar corona which are crucial for understanding the particle acceleration processes which occur there. Grazing-incidence x-ray focusing optics combined with position-sensitive solid state detectors can overcome both of these limitations enabling the next breakthrough in understanding impulsive energy release on the Sun. The FOXSI project is led by the Space Sciences Laboratory at the University of California, Berkeley. The NASA Marshall Space Flight Center is responsible for the grazing-incidence optics, while the Astro-H team at JAXA/ISAS has provided double-sided silicon strip detectors. FOXSI is a pathfinder for the next generation of solar hard x-ray spectroscopic imagers. Such observatories will be able to image the non-thermal electrons within the solar flare acceleration region, trace their paths through the corona, and provide essential quantitative measurements such as energy spectra, density, and energy content in accelerated electrons.

Krucker, Saem↗
NASA NTRS2004

Improved Inlet Noise Attenuation by Alteration of Boundary Layer Profiles

Acoustic liners are an essential component of technology used to reduce aircraft engine noise. Flow affects attenuation due to the liner in several ways, one of which is that boundary layers adjacent to the liner refract the sound. In the case of inlet noise, the boundary layer causes sound to be refracted away from the liner, thus degrading attenuation. A concept to improve attenuation by the liner by alteration of inlet boundary layer profiles is presented. The alteration of profiles is achieved by inlet blowing. Computational fluid dynamics and duct mode propagation theory for ducts carrying a parallel sheared flow have been used to design experiments to explore such a possibility in the NASA Langley Research Center Grazing Incidence Tube using an inlet blowing scheme developed at General Electric Global Research. The effects of inlet blowing on two liner configurations were evaluated. Calculated results will be shown for blowing ratios (injected flow/duct flow) of approximately 12% and frequencies up to 3 kHz. These results emphasize changes of attenuation achieved by blowing for the two liners. Experimental results of measured flow profiles (with and without blowing) in the Grazing Incidence Tube, and of corresponding changes in attenuation by the liner due to blowing will be presented.

Mani, Ramani↗
DOE OSTI2026

Suppressing Phase Segregation and Improving Stability in Mixed-Halide Perovskites through Spinel Oxide-Directed Epitaxy

Mixed-cation mixed-halide perovskite compositions are essential for achieving the required bandgaps for high-efficiency multijunction photovoltaics, yet their stability remains limited by interfacial defects, phase segregation, and degradation. Here, we introduce spinel oxides as a new family of lattice-matched substrates that enable crystalline, phase-pure, compositionally-uniform, bromide-rich perovskite film growth. The effect of spinel oxides is two-fold: reducing defects at the bottom interface by templating film growth and inducing beneficial compressive strain through mismatch-dependent substrate-perovskite lattice coupling. Spinel oxide substrates facilitate growth of highly crystalline films and eliminate detrimental secondary phases across thicknesses. Using grazing incidence X-ray diffraction, X-ray fluorescence, cathodoluminescence–scanning electron microscopy, cryogenic photoluminescence, and density functional theory, we reveal that Mg-halide bonds at the bottom interface induce lattice mismatch-dependent compressive strain that suppresses halide segregation and further reduces defect formation. In addition, films grown on spinel oxides maintain over 87% of the perovskite phase after 12 h under 100% relative humidity, as monitored by in situ grazing incidence wide-angle X-ray scattering (GIWAXS), compared to less than 70% for control samples. This work extends lattice matching from vapor-deposited epitaxial semiconductors to solution-processed halide perovskites to establish a broadly applicable strategy for defect suppression, phase homogenization, and long-term stability. Based on the fundamental science explored here, we set the stage for the development of lattice-matched spinel oxide charge transport layers to be integrated into perovskite solar cells and other optoelectronic devices.

36 MATERIALS SCIENCE↗