Experiments to measure material and mechanism damping at cryogenic temperatures
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Tests performed at Langley Research Center to find connectors, cables, and other electrical components suitable for use in cryogenic environment described. In addition, several electrical cables have to flex under cryogenic conditions. Tests necessary to qualify materials for use in National Transonic Facility (NTF), which operates at temperature range from 175 degrees to - 300 degrees F (353 to 89 K).
Adhesive, which bonds a metal liner to a filament wound composite structure used for cryogenic pressure vessels, prevents the metal liner from buckling under depressurization. The adhesive consists of adducts of urethane and epoxy resins.
Cold working and aging prepares nickel alloys for coiling into springs with properties acceptable in a cryogenic environment.
Cryogenic properties of polymers - NASA/Case Conference, Cleveland, April 1967
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New metal-oxide-semiconductor field-effect transistors designed for source-follower preamplifiers operating at liquid-helium temperatures in conjunction with infrared detectors. Lower thresholds and offset give CryoFET's greater dynamic range and linearity than conventional MOSFET's at low temperatures and facilitates pair balancing to reduce offsets in output. Reduces heat loading of cryogenic system, extending life, reliability, and performance of cryogenic infrared instruments.
Film boiling occurs in the quenching of metals, the chilling of biological species, the regenerative cooling of rockets, and the cooling down of a cryogenic fuel tank. Occasionally film boiling is also found in a nuclear reactor or in a cryomagnet. Aspects of film boiling involving an unconstrained liquid mass are considered, giving attention to the evaporation time, the Leidenfrost temperature, solid-liquid contacts, the thermal properties of the solid, effects of coating or scale, wettability, the metastable condition, and the velocity effect on drops. Developments discussed with regard to pool boiling are related to vertical surfaces, film boiling from horizontal surfaces, film boiling from a horizontal cylinder, film boiling from a sphere, and film boiling of helium. Processes of film boiling in a channel are also analyzed.
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Pressure and temperature characteristics were measured for a number of multichannel electronically scanned pressure sensors. The tests were made on commercially available units designed to operate in a controlled temperature environment. Measurements of zero shift, sensitivity, and nonlinearity for each transducer were taken over a temperature range from 100 K to 340 K using a computer controlled data acquisition system. The units tested failed to meet accuracy specifications over the complete temperature range, which was expected. However, the sensors showed acceptable and predictable behavior over the temperature range from approximately -40 C (233 K) to 70 C (343 K). It was determined that a combination of local heating and accurate temperature monitoring can result in a device that can be compensated for temperature as well as its other physical properties. The design of a prototype for operation in a cryogenic environment is proposed, and a method for compensation is developed.
Low temperature chemical reactivity and synthesis research and applications
An investigation was conducted to study the concept of thermal control by means of physical or chemical reaction heats for applications involving the storage of cryogens during long-term space voyages. The investigation included some preliminary experimental tests of energy storage material (ESM) effectiveness. The materials considered can store and liberate large amounts of thermal energy by means of mechanisms such as sensible heat, heat of fusion, and physical or chemical reaction heat. A differential thermal analysis was utilized in the laboratory tests. Attention is given to the evaluation of cryogenic ESM thermal control concepts, the experimental determination of phase change materials characteristics, and adsorption ESMs. It is found that an ESM shield surrounded by multiple layer insulation provides the best protection for a cryogen store.
We present the current state of development in passive gas-gap heat switches. This type of switch does not require a separate heater to activate heat transfer but, instead, relies upon the warming of one end due to an intrinsic step in a thermodynamic cycle to raise a getter above a threshold temperature. Above this temperature sequestered gas is released to couple both sides of the switch. This enhances the thermodynamic efficiency of the system and reduces the complexity of the control system. Various gas mixtures and getter configurations will be presented.
We present the current state of development in passive gas-gap heat switches. This type of switch does not require a separate heater to activate heat transfer but, instead, relies upon the warming of one end due to an intrinsic step in a thermodynamic cycle to raise a getter above a threshold temperature. Above this temperature sequestered gas is released to couple both sides of the switch. This enhances the thermodynamic efficiency of the system and reduces the complexity of the control system. Various gas mixtures and getter configurations will be presented.
The following summarizes the activities performed under NASA grant NAG10-323 from September 1, 2002 through September 30, 2004 at the. Univ ersity of Central Florida. A version of this has already been submitt ed for publication in the international journal Swart Materials and S tructures in December 2004. Additionally, a version of this has alrea dy appeared in print in Advances in Cryogenic Engineering, American Institute of Physics, (2004) 50A 26-3; in an article entitled "A Shape Memory Alloy Based Cryogenic Thermal Conduction Switch" by V.B. Krish nan. J.D. Singh. T.R. Woodruff. W.U. Notardonato and R. Vaidyanathan (article is attached at the end of this report).
This report describes the Mirror Transport Mechanism (MTM), which supports a pair of dihedral mirrors and moves them in a very smooth and uniform scanning motion normal to a beamsplitter. Each scan is followed by a quick flyback and repeat. Included in the report will be material selection, design, and testing of all major components of the MTM in order to meet the stringent performance requirements under cryogenic conditions and survive the launch environment of the shuttle. Areas to be discussed in detail will be those in which failures or performance anomalies occurred and their solutions. Typically, this will include (but not to be limited to) flex pivot failures during vibration testing, excessive dihedral platform sag under one "g" operation, electronic and fiber optic characteristics, and tolerancing considerations. As of this writing, development of the mechanism has reached the final phase of thermal and vibration qualification. Environmental testing of the complete FIRAS (Far Infrared Absolute Spectrophotometer) experiment is just beginning.
The Space Shuttle External Tank (ET) contains the liquid H2 fuel and liquid oxygen oxidizer and supplies them under pressure to the three space shuttle main engines (SSME) in the orbiter during lift-off and ascent. The ET thermal protection system consists of sprayed-on foam insulation and pre-molded ablator materials. The closed-cell foams are the external coating on the ET and are responsible for minimizing the amount of moisture that condenses out and freezes on the tank from the humid air in Florida while it is on the pad with cryogenic propellant awaiting launch. This effort was part of the overall drive to understand the behavior of these materials under use-conditions. There are four specially-engineered closed-cell foams used on the tank. The thermal expansion (contraction) of three of the polyurethane and polyisocyanurate foams were measured from -423 F (the temperature of liquid hydrogen) to 125 F under atmospheric conditions and under vacuum. One of them, NCFI 24-124, is a mechanically-applied material and covers the main acreage of the tank, accounting for 77 percent of the total foam used. Another, BX-265, is also a mechanically-applied and hand-sprayed material used on the tank's "closeout" areas. PDL 1034 is a hand-poured foam used for filling odd-shaped cavities in the tank, Measurements were made in triplicate in the three primary material directions in the case of the first two materials and the two primary material directions in the case of the last. Task 1 was developing the techniques for getting a uniform heating rate and minimizing axial and radial thermal gradients in the specimens. Temperature measurements were made at four locations in the specimens during this initial development phase of testing. Major challenges that were overcome include developing techniques for transferring the coolant, liquid helium (-452 F), from its storage container to the test facility with a minimal transfer of heat to the coolant and control of the heating rate at the lowest temperatures.