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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 217 records · Page 12
All sourcesNASA NTRSDOE OSTI
DOE OSTI2021

Reinforced Ammo Can Validation Test Report for Lawrence Livermore National Laboratory

A research effort was conducted to investigate the effects of an unintentional internal detonation of energetic materials on a small transportation container called the “Reinforced Ammo Can” (RAC), which is currently approved for the transport of energetic materials up to 2 grams net explosive weight (NEW) onsite at Lawrence Livermore National Laboratory (LLNL). The project used experimental testing of the containers based on simulated results conducted by a Missouri S & T explosives engineering graduate student while on an internship working in explosives safety at LLNL. The proposed experimental testing consisted of 20 central detonation tests in separate Reinforced Ammo Can containers to verify their high explosive (HE) containment capability. RAC containers are required for transporting secondary explosives on site at LLNL Site 200 in quantities between 300 mg and 2 grams of Trinitrotoluene (TNT) equivalent NEW. Currently, the LLNL Environmental Safety and Health (ES&H) Manual states that the RAC containers are permissible for on-site transportation of secondary explosives up to 2 grams NEW by approved HE handlers with the approval of an Explosives Safety Expert (ESE). Simulated results indicated that tensile failure of the closure mechanism on the container is the most likely failure mode, and showed potential occurrence at the 2 gram NEW threshold. Experimental validation tests were conducted indicating failure/rupture of the containers lid with venting of the detonation products at the 2 gram NEW test threshold with an explosive mass safety factor of 1.3. Failure consisted of impact opening the container latch mechanism resulting in potential ejection of the lid depending on the orientation of the charge within the confinement. This analysis solely is an evaluation of the response of the containment if a detonation were to occur, it does NOT consider the probability of such an event.

42 ENGINEERING↗
DOE OSTI2021

Alternative Liquid DSA Containers for Sludge Slurry Storage in the SRNL Shielded Cells

A pending revision of the Documented Safety Analysis (DSA) for the Savannah River National Laboratory (SRNL) defines “DSA containers” for liquid sludge slurries as containers not susceptible to a flashing spray release in a fire and requires that a list of DSA containers be maintained. High Level Waste (HLW) samples are typically received from the Savannah River Site (SRS) tank farm after retrieval from the storage tanks. Glass bottles are preferred for long-term storage of radioactive liquid sludge slurry samples but are not on the DSA container list. An evaluation has been conducted to identify vessel lids for the glass bottles that would vent prior to pressurization and liquid superheating in a fire event. Low melting Field’s Metal eutectic alloy with a melting point of 62 °C has been identified as a preferred material of construction for vessel lids for this application because the material is resistant to puncture and is expected to have good chemical compatibility and radiation stability in the shielded cells environment. A test vessel was designed to evaluate the alloy and confirm that it would melt before the water in the vessel reaches the boiling point. The tests confirmed: 1) that the reported melting point of the alloy was accurate, 2) that a top fashioned from this material will melt creating an open atmosphere in the vessel headspace prior to sample boiling under moderate and fast heating rates, and 3) that nonuniform heating of the bottle from the bottom also results in melting of the alloy prior to boiling. Based on the results, neither an engulfing fire with standing or toppled bottles or a fire producing localized heat at the vessel bottom would result in flashing spray conditions.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2021

FY 2021 Filter Test for TRU Waste Drum POC Proof-of-Concept Unit

Continuing last year’s (fiscal year 2020) work, a Proof-of-Concept (POC) instrument was developed to assess the functionality of filters on transuranic waste containers (commonly called 55 Gallon ring-top drums) without requiring removal of the drum lid. The purpose of this work is to determine the air flow and pressure characteristics associated with filter clogging, filter pressure drop, headspace volume, leakage around the lid seal and influence of the additional filter on a bag-out bag.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2021

A Solution to Asymmetric Marangoni GTA Weld Behavior in a Dissimilar Chemistry Stainless Steel Joint [Slides]

Asymmetric and irregular weld morphology is an issue with the 9516 shipping container GTA weld. Observation of the weld puddle and cross sections showed the weld was biased toward the body side of the joint. This issue is attributed to a difference in the sulfur content and Marangoni fluid flow characteristics of the lid (150 ppm) and body (10 ppm) components of the weld joint. An additional contributing factor in this issue is the large difference in mass between the ½” thick lid and 1/8” thick body. A solution was developed comprised of a preliminary partial penetration weave pass across the joint intended to homogenize the sulfur content prior to the full penetration pass.

42 ENGINEERING↗
DOE OSTI2022

Test Report for DPP-1 Regulatory Compliance Testing. Volume 1 - Main Report

Consolidated Nuclear Security, LLC (CNS), the management and operating contractor for the Y-12 National Security Complex (Y-12) for the National Nuclear Security Administration (NNSA), is currently responsible for the regulatory testing of a new Type B fissile material shipping package called the Defense Programs Package (DPP)-1. The DPP-1 is a drum packaging with an inner liner and a removable lid. Both the drum body and the lid are filled with an impact-limiting, thermal-insulating material that protects the inner containment vessel (CV) during normal conditions of transport (NCT) and hypothetical accident conditions (HAC) as defined by 10 US code of Federal Regulations (CFR) 71. In fiscal year 2021, the Oak Ridge National Laboratory (ORNL) Package Testing Program (PTP), located at the National Transportation Research Center (NTRC), conducted Type B performance tests as prescribed in Title 10 Code of Federal Regulations Part 71 (10 CFR 71) on seven DPP-1 prototype units. This test report documents test unit (TU) preparation, pretest condition, conditioning of each TU, NCT and HAC testing, and posttest measurements and observations made of the damage resulting from these tests.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2022

FY2022 Filter Test for TRU Waste Drum Prototype Unit

Continuing last year’s (fiscal year 2021) work, a prototype instrument and an NPI-6 Integrated Work Document (IWD) were developed to assess the functionality of filters on transuranic waste containers (commonly called 55 Gallon ring-top drums) without requiring the removal of the drum lid. The purpose of this work is to determine the air flow and pressure characteristics associated with filter clogging, filter pressure drop at a fixed flow rate, and leakage around the lid seal. The FY22 objectives included: (A) Development of prototype device, (B) Drafting an IWD document, (C) Defining a filter clogging parameter, (D) Assessing filter damage due to over-pressure events, and (E) A path forward to obtain approval of the system safety filters in compliance with P101-16 Industrial Ventilation – non HVACR (LANL 2022).

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2025

Full Submersion Water Testing of SAVY-4000 Nuclear Material Storage Containers

SAVY-4000 (SAVY) containers are the primary container used at Technical Area (TA) TA-55 plutonium facility for the prevention of water ingress to mitigate against a criticality event. The basis for water resistance of these containers has long been attributed to the Polytetrafluoroethylene (PTFE) membrane that is assembled on the outermost surface of the filter assembly. On August 22nd a test of a container used inside of a glovebox was performed that brought into question this long-standing-basis. This test was performed by inverting a SAVY-lid onto a specialized piece of equipment for evaluating the integrity of the PTFE membrane. During the test water was observed passing through the filter indicating that the filter membrane was no longer preventing the ingress of water through the filter. The assumption after making this observation was that alpha-particles were rapidly degrading the membrane creating a leak path through the underlying aluminosilicate media (Fiberfrax®). The apparatus used was designed to only test the lid rather than the entire SAVY assembly. A test plan, PA-PLAN-01921, was developed to investigate whether a fully assembled container with a fully degraded PTFE membrane would be capable of meeting the criteria defined in PA-RD-1009 of not allowing more than 200 ml of water to enter the container with a water column of 6-inches applied over a 2-hour period. This report provides the results of the testing performed against PA-PLAN-01921.

36 MATERIALS SCIENCE↗
DOE OSTI2026

Water-Resistant Container Testing: A426-7, A426-25, and A426-50 Container Designs

The purpose of this report is to detail the results of water ingress testing conducted on the A426-7, A426-25, and A426-50 Mini-Pot container designs and discuss these results against the water-resistant container requirements of TA55-AP-522 and PA-RD-01009. The A426 design series is a proposed commercially off the shelf inner container option for material storage inside of a glovebox and/or as an approved nonhermetically sealed inner of an approved packaging configuration inside of an approved outer container as listed in PA-RD-01022. The A426-25 and A426-50 are shaped similar to an ointment jar, made of 316L stainless steel, and utilize a threaded lid for closure and containment. The A426-7 container is shaped similar to a vial, made of 316L stainless steel, and utilizes a threaded lid for closure and containment. See Figure 1 and Table 1-3 for a summary of the container specifications. For more details on the container design, see Section 1.4.

42 ENGINEERING↗
DOE OSTI2026

Degradation Mode Identification by Photocarrier Lifetime Spectroscopy on Devices and Test Structures

In this presentation, I examine the basic concepts of the device physics that can be used to distinguish various degradation and recovery modes on a cell level. The known degradation modes (bulk LeTID and LID, UVID, etc.) are due to defects and impurities that cause the photocarrier recombination according to Shockley-Reed-Hall (SRH) statistics. The SRH recombination rate strongly depends on the balance of electron and hole capture rates into the defects, which in turn, are governed by their local concentrations. The strongest recombination takes place at approximately equal concentrations of electrons and holes, while at low injection conditions (when one type of carrier dominates) the SRH recombination is suppressed. For cell degradation modes that affect the passivated interface (UVID, H-induced TOPCon contact degradation) the defects are at the interface under low-injection conditions due to either high local doping or the adjacent built-in charge in the dielectric. This mode is characterized by changes in the "diode prefactor" J01 slope in the inverse lifetime-injection level curve. In contrast, bulk degradation (LeTID, LID) affects bulk lifetime, with J01 slope unchanged. Carrier lifetime - injection level plots therefore serve as clear indicators of different degradation modes and are shown by experimental examples.

14 SOLAR ENERGY↗
DOE OSTI2026

SAVY-4000 Finite-Element Drop Test Analysis

PFE Auxiliary Systems conducted drop testing on SAVY-4000 containers to evaluate structural response under 12-foot drop conditions. In support of that effort, a finite-element modeling capability was developed to simulate drop response across multiple container sizes and impact orientations. The purpose of this work was to provide a consistent analysis framework that could support interpretation of testing, compare response trends across multiple configurations, and generate quantities of interest for later comparison with experimental data. More broadly, the analysis and testing were intended to assess whether the containers continued to perform their primary function after a 12-foot drop, namely maintaining structural integrity and containment of the contents. The modeling approach combined an implicit preload analysis with an explicit drop simulation so that each drop event began from a mechanically realistic assembled condition, including compression of the silicone O-ring. Separate models were developed for 2-quart, 5-quart, 12-quart, and 10-gallon containers. The results were evaluated in terms of strain-gauge response, collar-lid gap behavior, and accumulated plastic strain. In addition, parametric studies were performed on the 2-quart container to assess sensitivity to O-ring stiffness, friction, canister thickness, geometry tolerance, and mesh density. The simulations showed that predicted drop responses depended strongly on both container size and drop orientation. Gap metrics identified cases in which the predicted collar-lid opening exceeded the nominal O-ring cross-section threshold, while plastic strain metrics identified localized regions of elevated permanent deformation. Parametric studies showed that the predicted response was especially sensitive to the assumed O-ring stiffness and contact friction, while the geometry tolerance study produced smaller changes in the cases examined. The main value of this work was that it established a repeatable modeling and simulation workflow to support drop-test implementation, evaluate effects of future configuration changes, and understand modeling assumptions that most influenced predicted response. At the current stage, the results were viewed as preliminary model predictions rather than validated predictions. The next step would be to compare drop-test data to the model so that predictive values of the workflow could be refined and used with greater confidence to assess whether the containers maintained structural integrity and containment of the contents after a 12-foot drop.

42 ENGINEERING↗
DOE OSTI2021

Reducing Sample Loss in Measurement of Heat of Vaporization of Ethanol/Gasoline Blends by Differential Scanning Calorimetry/Thermogravimetric Analysis

Higher gasoline Heat of Vaporization (HOV) can enable higher compression-ratio direct injection spark ignition engines by providing evaporative cooling that effectively increases fuel knock resistance. Methods to directly measure this fuel property in complex gasoline samples are not well developed. The objective of the present study was to further improve a Differential Scanning Calorimetry/Thermogravimetric Analyzer (DSC/TGA) method to measure the total and partial HOV of gasoline. Ten market gasoline samples were chosen to have a wide range of properties to assess the method's capability across the entire volatility range with an emphasis on understanding how well the method captures the initial 10 percent (%) of sample evaporation and how much sample is left unevaporated at the end of the experiment. Modifications to the sample preparation/introduction method as well as to the instrument itself were made to reduce initial sample losses which included measurements of the HOV at 10 degrees C and 5 degrees C (in a cold chamber) as well as under (uncontrolled) ambient conditions. Experimental results from the DSC/TGA were compared to calculated total HOV results based on Detailed Hydrocarbon Analysis (DHA). Results from the two methods agreed very well with the difference being 5% or less in almost every case. In addition, the repeatability of the method was investigated by analyzing samples in triplicate at the three temperatures investigated. One valuable conclusion from the study was that the lower temperatures of 10 degrees C and 5 degrees C enabled more reproducible measurements for both total and partial HOV. This improved precision may be caused by the fact that temperature control in the cold chamber was more reliable than the ambient laboratory temperature control. Additionally, cold chamber experiments, due to ergonomic limitations, did not allow for the use of a lid on the sample pan. The reproducibility of the evaporation rate was found to be highly dependent on the pan/lid fit which can vary significantly such that elimination of the lid improved measurement precision while operation at sub-ambient temperature slowed the evaporation rate. Results detailing sample preparation and instrument modifications as well as a detailed comparison of total and partial HOV results are presented.

ADVANCED PROPULSION SYSTEMS,BIOMASS FUELS↗
NASA NTRS1980

Three-dimensional time-dependent simulations of hydro-thermal behaviour of Biscayne Bay

The purpose of the paper is to evaluate the performance of rigid-lid formulations in predicting velocity and temperature fields in domains where the applicability of rigid-lid formulations is not immediately obvious. A test was conducted to determine whether local depth scaled vertical exchange coefficients yield better simulations compared to constant vertical coefficient formulations. Extensive infrared imagery was used to evaluate the model's ability to predict temperature yields in Biscayne Bay, Fla. Two cases, one with constant vertical eddy transport coefficient, and the other with vertical transport coefficient scaled with local depth are discussed.

Sengupta, S.↗
NASA NTRS1982

Experimental study of time-dependent flows in laboratory atmospheric flow models

Baroclinic waves in a rotating, differentially-heated annulus of liquid were studied in support of the Atmospheric General Circulation Experiment. Specific objectives were to determine: (1) the nature of the flow at shallow depths, (2) the effect of a rigid lid vs. free surface, and (3) the nature of fluctuations in the waves as a function of rotation rate, depth, and type of surface. It is found that flows with a rigid lid are basically the same as those with a free surface, except for a decrease in flow rate. At shallow depths steady flows are found in essentially the same form, but the incidence of unsteady flows is greatly diminished.

Rush, J. E.↗
NASA NTRS1983

Uppermantle anisotropy and the oceanic lithosphere

Published Rayleigh and Love wave phase and group velocity data have been inverted taking into account sphericity, anelastic dispersion, and transverse isotropy. For a PREM-type modular parameterization, the thickness of the high velocity mantle seismic lithosphere (LID) varies in thickness from about 30 km for young ocean to about 50 km for old ocean, much less than previous estimates based on isotropic inversion of similar data. This LID thickness is comparable to the elastic or flexural thickness found from studies of seamount loading and flexure at trenches, suggesting that the thickness of the lithosphere may be controlled by mineralogy, composition, or crystal orientation rather than by temperature alone.

Anderson, D. L.↗
NASA NTRS1987

The effect of a shallow low viscosity zone on the apparent compensation of midplate swells

A model for midplate swells is assumed where the swell topography is dynamically maintained by convection beneath a conducting lid. Using an idealized viscosity structure consisting of a low viscosity layer underneath the lid and overlying a constant viscosity region, the effect of the low viscosities, the layer thickness, and the Rayleigh number on the flow and on the inference of a compensation mechanism from the associated gravity, geoid, and topography anomalies is investigated. The calculations show that a simple plume model with stratified viscosity variations of less than two orders of magnitude near the surface can produce the range of depths of compensation seen at midplate swells. Shallow depths of compensation, therefore, cannot be used to argue against dynamic models for the formation of hot spot swells.

Robinson, Elizabeth M.↗
NASA NTRS1988

Device Maintains Water At The Triple Point

Inexpensive device maintains water at 0.01 degree C for 10 weeks or longer. New device consists of four basic assemblies; small, commercial chest freezer containing insulated water tank; insulated copper cell holder; "ice switch" for cycling freezer compressor and externally-mounted air pump for circulation. Access hole in freezer lid allows triple point measurements without opening lid. Modified freezer used to calibrate standard platinum resistance thermomenters.

West, J. W.↗
NASA NTRS1989

Reduction Of Stresses In Growing Silicon Webs

New trenched lid intercepts less radiation from edges of growing silicon ribbon, giving rise to faster growth and temperature distribution resulting in lower residual stress. Cutting trench in susceptor lid allows edges of growing ribbon of silicon to cool more rapidly. Edges cool and solidify nearly same rate as center of ribbon, and thermal stress in ribbon reduced. Because of more-effective edge cooling, wider ribbon grown, and withdrawn at faster rate. Productivity of dendritic-web growth furnace increased.

Duncan, C. S.↗
NASA NTRS1988

The delineation and interpretation of the earth's gravity field

A series of fluid dynamical experiments in variable viscosity fluid have been made and are in progress to study: (1) the onset of small scale convection relative to lithosphere growth rate; (2) the influence of paired fracture zones in modulating the horizontal scale of small scale convection; (3) the influence of the mantle vertical viscosity structure on determing the mode of small scale convection; and (4) the 3-D and temporal evolution of flows beneath a high viscosity lid. These experiments extend and amplify the present experimental work that has produced small scale convection beneath a downward-moving solidification front. Rapid growth of a high viscosity lid stifles the early onset of convection such that convection only begins once the lithosphere is older than a certain minimum age. The interplay of this convection with both the structure of the lithosphere and mantle provide a fertile field of investigation into the origin of geoid, gravity, and topographic anomalies in the central Pacific. These highly correlated fields of intermediate wavelength (approximately 200 to 2000 km), but not the larger wavelengths. It is the ultimate, dynamic origin of this class of anomalies that is sought in this investigation.

Marsh, Bruce D.↗