Synopsis of cesium compatibility studies
Compatibility of metallic and ceramic materials with gaseous and liquid cesium for ion engines
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Results for “Ceramic materials”
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
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Laser processing
Progress in the Progress ceramic materials is reported. Experiments and models for sintering and microstructure evolution are described. Models and data for understanding the kinetics of grain boundary motion and of pore coarsening and new materials for fuel cells and batteries; are developed. New experimental techniques using lasers for forming fine, monosized powders and for forming stable and metastable structures from liquids, and solar materials research are also developed. Colloidal science and ceramics processing are explored; and research programs on the presintering science necessary for controlled green microstructures are outlined.
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Correlation between ultrasonic velocity and density of ceramic turbine blades
A computer-aided ultrasonic velocity measurement system to detect small density variations in structural ceramic materials has been developed. Longitudinal wave ultrasonic velocity and density of ceramic turbine blades and bars were measured and statistically correlated. Density variations of 1 to 2 percent were reliably detected. Burst speed of ceramic blades was inversely proportional to the grain size of the material.
Khandelwal, P. K.↗
Morphologies, Processing and Properties of Ceramic Foams from Pre-Ceramic Foams from Pre-Ceramic Polymer Routes
The current research is focused on processing ceramic foams that have potential as a thermal protection material. Ceramic foams with different architectures were formed from the pyrolysis of pre-ceramic polymers at 1200 C in different atmospheres. In some systems a sacrificial polyurethane was used as the blowing agent. We have also processed foams using sacrificial fillers to introduce controlled cell sizes. Each sacrificial filler or blowing agent leads to a unique morphology. The effect of different fillers on foam morphologies will be presented. The presentation will also focus on characterization of these foams in terms of mechanical and thermal properties. Foams processed using these approaches having bulk densities ranging from 0.15 to 0.9 g per cubic centimeter and a cell sizes from 5 to 500 micrometers. Compression strengths ranged from 2 to 7 MPa for these materials.
Stackpoole, Mairead↗
Considerations in Friction and Wear
The abrasion of ceramic materials is discussed. The friction and wear properties of ceramics which arise primarily from adhesion between sliding surfaces in contact was examined. The role of chemical bonding in adhesion and friction and the influence of surface films, temperature, and crystallographic orientation effects on tribological response with respect to adhesion, friction, and wear are discussed. The complex interaction of various deformation and fracture mechanisms in ceramics, the effect of crystallographic orientation on abrasion, friction, and fracture behavior is addressed.
Miyoshi, K.↗
NASA/CARES dual-use ceramic technology spinoff applications
NASA has developed software that enables American industry to establish the reliability and life of ceramic structures in a wide variety of 21st Century applications. Designing ceramic components to survive at higher temperatures than the capability of most metals and in severe loading environments involves the disciplines of statistics and fracture mechanics. Successful application of advanced ceramics material properties and the use of a probabilistic brittle material design methodology. The NASA program, known as CARES (Ceramics Analysis and Reliability Evaluation of Structures), is a comprehensive general purpose design tool that predicts the probability of failure of a ceramic component as a function of its time in service. The latest version of this software, CARESALIFE, is coupled to several commercially available finite element analysis programs (ANSYS, MSC/NASTRAN, ABAQUS, COSMOS/N4, MARC), resulting in an advanced integrated design tool which is adapted to the computing environment of the user. The NASA-developed CARES software has been successfully used by industrial, government, and academic organizations to design and optimize ceramic components for many demanding applications. Industrial sectors impacted by this program include aerospace, automotive, electronic, medical, and energy applications. Dual-use applications include engine components, graphite and ceramic high temperature valves, TV picture tubes, ceramic bearings, electronic chips, glass building panels, infrared windows, radiant heater tubes, heat exchangers, and artificial hips, knee caps, and teeth.
Powers, Lynn M.↗
Methods for providing ceramic matrix composite components with increased thermal capacity
A method for enhancing the cooling capability of a turbine component made from a ceramic matrix composite. The method improves the thermal performance of the component by producing a surface having increased cooling capacity, thereby allowing the component to operate at a higher temperature. The method tailors the available surface area on the cooling surface of the composite component by depositing a particulate layer of coarse grained ceramic powders of preselected size onto the surface of the ceramic matrix composite component. The size of the particulate is selectively tailored to match the desired surface finish or surface roughness of the article. The article may be designed to have different surface finishes for different locations, so that the application of different sized powders can provide different cooling capabilities at different locations, if desired. The compositions of the particulates are chemically compatible with the ceramic material comprising the outer surface or portion of the ceramic matrix composite. The particulates are applied using a slurry and incorporated into the article by heating to an elevated temperature without melting the matrix, the particulates or the fiber reinforcement.
Steibel, James Dale↗
Testing Ceramics for Diesel Engines
Adaptation of diesel engine allows prestressed ceramic materials evaluated under realistic pressure, temperature, and stress without introducing extraneous stress. Ceramic specimen part of prechamber of research engine. Specimen held in place by clamp, introduces required axial compressive stress. Specimen -- cylindrical shell -- surrounded by chamber vented or pressurized to introduce requisite radial stress in ceramic. Pressure chamber also serves as safety shield in case speimen disintegrates. Materials under consideration as cylinder liners for diesel engines.
Schneider, H. W.↗
A mechanical tension testing facility for brittle materials
Mechanical test facility for measuring deformation and fracture stresses in tension of brittle ceramic material
DEFORMATION↗
High-temperature ceramics for automobile gas turbines
The employment of the high operational temperatures makes it necessary to use, for the construction of the turbines, ceramic materials such as silicon nitride or silicon carbide. Investigations concerning the development of turbine components made of such materials are conducted by a German automobile manufacturer and the ceramics industry. The current status of these investigations is reviewed. Flame tubes and guide-vane rings have successfully passed tests lasting 20 hours. Prototype turbine wheels have withstood the effects of peripheral speeds of 450 m/s. They also showed resistance to thermal shocks which were as high as 6-0 K/s.
Walzer, P.↗
A study of strength evaluations of EDNi/EDCu/NARloy-Z bonded joints
Dissimilar material interfaces can be found in many materials and structural bonds such as composite materials, welded parts, inclusion in matrix, bond between metallic and ceramic materials, and so forth. One of such structural bonds can be seen in the main combustion chamber (MCC) of the Space Shuttle Main Engine (SSME). In this study, from a practical sense, the primary concern is to understand the systems response of EDNi/EDCu/NARloy-Z bonded joints using stress values approximated by the finite element method to determine an influence of the variation of structural bond parameters on the bonded joints, and consequently main combustion chamber of the Space Shuttle Main Engine. The results presented in this study could be an appropriate indicator for a good bond of EDNi/DECu/NARloy-Z layers with the desired thickness of copper deposition in the SSME MCC manufacturing process. Furthermore, the results from this study appear to be applicable to any bonded joints that can be characterized by the parameters and assumptions used in this analysis.
Min, J. B.↗
Foamed in place ceramic refractory insulating material Patent
Characteristics of foamed-in-place ceramic refractory insulating material and method of fabrication
Eubanks, A. G.↗
Thallous halide materials for use in cryogenic applications
Thallous halides, either alone or in combination with other ceramic materials, are used in cryogenic applications such as heat exchange material for the regenerator section of a closed-cycle cryogenic refrigeration section, as stabilizing coatings for superconducting wires, and as dielectric insulating materials. The thallous halides possess unusually large specific heats at low temperatures, have large thermal conductivities, are nonmagnetic, and are nonconductors of electricity. They can be formed into a variety of shapes such as spheres, bars, rods, or the like and can be coated onto substrates.
Lawless, William N.↗
Paper-Thin Coating Offers Maximum Protection
Wessex Incorporated has recently taken a technology that was originally developed for NASA as a protective coating for ceramic materials used in heatshields for space vehicles, and modified it for use in applications such as building materials, machinery, and transportation. The technology, developed at NASA Ames Research Center as a protective coating for flexible ceramic composites (PCC), is environmentally safe, water-based, and contains no solvents. Many other flame-retardant materials contain petroleum-based components, which can produce toxic smoke under flame. Wessex versions of PCC can be used to shield ceramics, wood, plasterboard, steel, plastics, fiberglass, and other materials from catastrophic fires. They are extraordinarily tough and exhibit excellent resistance to thermal shock, vibration, abrasion, and mechanical damage. One thin layer of coating provides necessary protection and allows for flexibility while avoiding excessive weight disadvantages. The coating essentially reduces the likelihood of the underlying material becoming so hot that it combusts and thus inhibits the "flashover" phenomenon from occurring.
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Evaluation of ceramics for stator applications: Gas turbine engines interim report. Stator fabrication and evaluation
The objective was to assess current ceramic materials, fabrication processes, reliability prediction, and stator durability when subjected to simulated automotive gas turbine engine operating conditions. Ceramic one-piece stators were fabricated of two materials, silicon nitride and silicon carbide, using two near-net-shape processes, slip casting and injection molding. Non-destructive evaluation tests were conducted on all stators identifying irregularities which could contribute to failures under durability testing. Development of the test rig and automatic control system for repeatably controlling air flow rate and temperature over a highly transient durability duty cycle is discussed. Durability results are presented for repeated thermal cycle testing of the ceramic one-piece stators. Two duty cycles were used, encompassing the temperature ranges of 704 to 1204 C (1300 to 2200 F) and 871 to 1371 C (1600 to 2500 F). Tests were conducted on 28 stators, accumulating 135,551 cycles in 2441 hours of hot testing. Cyclic durability for the ceramic one-piece stator was demonstrated to be in excess of 500 hours, accumulating over 28,850 thermal cycles. Ceramic interface forces were found to be the significant factor in limiting stator life rather than the scatter in material strength properties or the variation in component defects encountered.
Arnon, N.↗
Ceramics for the advanced automotive gas turbine engine: A look at a single shaft design
The results of a preliminary analysis of a single shaft regenerative design with a single stage radial turbine are presented to show the fuel economy that can be achieved at high turbine inlet temperatures, with this particular advanced design, if the turbine tip speed and regenerator inlet temperature are not limited. The engine size was 100 hp for application to a 3500 lb auto. The fuel economy was analyzed by coupling the engine to the auto through a continuously variable speed-ratio transmission and operating the system at constant turbine inlet temperature over the Composite Driving Cycle. The fuel was gasoline and the analysis was for a 85 F day. With a turbine inlet temperature of 2500 F the fuel economy was 26.2 mpg, an improvement of 18 percent over that of 22.3 mpg with a turbine inlet temperature of 1900 F. The turbine tip speed needed for best economy with the 2500 F engine was 2530 ft/sec. The regenerator temperature was approximately 2200 F at idle. Disk stresses were estimated for one single stage radial turbine and two two-stage radial-axial turbines and compared with maximum allowable stress curves estimated for a current ceramic material. Results show a need for higher Weibull Modulus, higher strength ceramics.
Nosek, S. M.↗
The Role of Ceramics and Ceramic Matrix Composites in NASA's Advanced Space Propulsion Programs
In recent years, NASA has embarked on several new and exciting efforts in the exploration and use of space. The successful accomplishment of many planned missions and projects is dependent upon the development and deployment of previously unproven propulsion systems. Key to many of the propulsion systems is the use of structural ceramics and ceramic matrix composites. In spite of their promise, a number of programmatic and technical hurdles remain before the potential of ceramic materials can be realized. A programmatic environment which focuses on relatively short term hardware demonstration programs precludes traditional longer term material's development efforts. The challenge oftentimes becomes one of engineering ceramics into proposed missions. This is dependent upon a fundamental understanding of processing, degradation and design issues unique to space vehicle design and operations. A review of the general missions and benefits of utilizing ceramics and ceramic matrix composites will be presented. The design parameters and operating conditions will be presented for both specific missions/vehicles and classes of components. Key technical challenges and opportunities are identified along with suggested paths for addressing them.
Eckel, Andrew J.↗
The Role of Ceramics and Ceramic Matrix Composites in NASA's Advanced Space Propulsion Programs
In recent years, NASA has embarked on several new and exciting efforts in the exploration and use of space. The successful accomplishment of many planned missions and projects is dependent upon the development and deployment of previously unproven propulsion systems. Key to many of the propulsion systems is the use of structural ceramics and ceramic matrix composites. In spite of their promise, a number of programmatic and technical hurdles remain before the potential of ceramic materials can be realized. A programmatic environment which focuses on relatively short term hardware demonstration programs precludes traditional longer term material's development efforts. The challenge oftentimes becomes one of engineering ceramics into proposed missions. This is dependent upon a fundamental understanding of processing, degradation and design issues unique to space vehicle design and operations. A review of the general missions and benefits of utilizing ceramics and ceramic matrix composites will be presented. The design parameters and operating conditions will be presented for both specific missions/vehicles and classes of components. Key technical challenges and opportunities are identified along with suggested paths for addressing them.
Eckel, Andrew J.↗