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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 199 records · Page 11
All sourcesNASA NTRSDOE OSTI
NASA NTRS1998

Investigation of Thermal High Cycle and Low Cycle Fatigue Mechanisms of Thick Thermal Barrier Coatings

Thick thermal barrier coating systems in a diesel engine experience severe thermal low cycle fatigue (LCF) and high cycle fatigue (HCF) during engine operation. In this paper, the mechanisms of fatigue crack initiation and propagation in a ZrO2-8wt.% Y2O3 thermal barrier coating, under simulated engine thermal LCF and HCF conditions, are investigated using a high power CO2 laser. Experiments showed that the combined LCF/HCF tests induced more severe coating surface cracking, microspallation and accelerated crack growth, as compared to the pure LCF test. Lateral crack branching and the ceramic/bond coat interface delaminations were also facilitated by HCF thermal loads, even in the absence of severe interfacial oxidation. Fatigue damages at crack wake surfaces, due to such phenomena as asperity/debris contact induced cracking and splat pull-out bending during cycling, were observed especially for the combined LCF/HCF tests. It is found that the failure associated with LCF is closely related to coating sintering and creep at high temperatures, which induce tensile stresses in the coating after cooling. The failure associated with HCF process, however, is mainly associated with a surface wedging mechanism. The interaction between the LCF, HCF and ceramic coating creep, and the relative importance of LCF and HCF in crack propagation are also discussed based on the experimental evidence.

Zhu, Dongming↗
NASA NTRS1998

Investigation of Thermal High Cycle and Low Cycle Fatigue Mechanisms of Thick Thermal Barrier Coatings

Thick thermal barrier coating systems in a diesel engine experience severe thermal low cycle fatigue (LCF) and high cycle fatigue (HCF) during engine operation. In this paper, the mechanisms of fatigue crack initiation and propagation in a ZrO2-8wt% Y2O3 thermal barrier coating, under simulated engine thermal LCF and HCF conditions, are investigated using a high power CO2 laser. Experiments showed that the combined LCF-HCF tests induced more severe coating surface cracking, microspallation and accelerated crack growth, as compared to the pure LCF test. Lateral crack branching and the ceramic/bond coat interface delaminations were also facilitated by HCF thermal loads, even in the absence of severe interfacial oxidation. Fatigue damage at crack wake surfaces, due to such phenomena as asperity/debris contact induced cracking and splat pull-out bending during cycling, was observed especially for the combined LCF-HCF tests. It is found that the failure associated with LCF is closely related to coating sintering and creep at high temperatures, which induce tensile stresses in the coating after cooling. The failure associated with HCF process, however, is mainly associated with a surface wedging mechanism. The interaction between the LCF, HCF and ceramic coating creep, and the relative importance of LCF and HCF in crack propagation are also discussed based on the experimental evidence.

Zhu, Dongming↗
DOE OSTI2021

Essential effect of the electrolyte on the mechanical and chemical degradation of LiNi 0.8 Co 0.15 Al 0.05 O 2 cathodes upon long-term cycling

Capacity fading during long-term cycling (>1500×) is still a critical challenge for Li-ion batteries that use Ni-rich layered oxides, e.g. LiNi 0.8 Co 0.15 Al 0.05 O 2 (NCA), as the cathode. Microcracks have been previously recognized as one of the primary reasons for the observed capacity fade. Although there exists a generally developed mechanical understanding of microcracks, the role of the electrolyte has not been clearly understood, especially after extended cycling and at the atomic scale. Here, we unveil the microstructural evolution of spherical NCA secondary particles after long-term cycling using scanning transmission electron microscopy accompanied with electron energy loss spectroscopy. In this work, we found that the microcracks initiated and grew through grain boundaries, which then serve as the pathway for electrolyte penetration into secondary NCA particles. Additionally, the rock-salt phase reconstruction is prone to occur at the (003) surfaces of the primary particles or the crack surfaces, largely due to electrolyte (LiPF 6 EC/EMC) corrosion. Crack propagation within the NCA grains is primarily a joint consequence from electrolyte corrosion and mechanical strain during lithiation/delithiation. During extended cycling, due to the distinctive surface facets, the primary grains located in the center of the secondary particles experience more intensive electrolyte corrosion, leading to a reduced contact with nearby particles, impairing the overall capacity. These results establish the initiation and growth mechanism of microcracks and voids in NCA-based cathodes during cycling and point out the role of the electrolyte in affecting the degradation of NCA-based cathodes.

25 ENERGY STORAGE↗
DOE OSTI2023

Minor Elements and Solidification Cracking During Laser Powder-Bed Fusion of a High $\gamma ^{\prime }$ CoNi-Base Superalloy

Here, the cracking behavior of a high γ' volume fraction CoNi-base superalloy fabricated via laser powder bed fusion (LPBF) is studied in relation to the content of carbon and boron. Severe cracking occurred with the increase in boron content from 0.08 to 0.16 at. pct (0.015 to 0.029 wt pct), while compositions with 0.1 to 0.36 at. pct C (0.02 to 0.076 wt pct) and 0.08 at. pct B exhibited minimal cracking. Assessment of cracks in the high-boron composition shows a variation in crack density with printing parameters, and alignment of the cracks with the build direction. Scanning electron microscopy (SEM) of the crack surfaces shows evidence of a solidification cracking mode. Differential thermal analysis (DTA) reveals a decreased incipient melting temperature for the high-boron composition, and atom probe tomography (APT) is used to measure the enrichment at grain boundaries, revealing distinct boron segregation. Scheil-Gulliver solidification simulations for the different C and B levels are consistent with the incipient melting behavior observed with DTA. Evaluation of the solidification cracking susceptibility from the simulations allow for comparison of the CoNi alloy behavior to Ni-base superalloys studied for LPBF fabrication and displays how such metrics may aid in the design of new precipitation-strengthened superalloys for additive manufacturing (AM).

36 MATERIALS SCIENCE↗
NASA NTRS1987

Energy dissipation associated with crack extension in an elastic-plastic material

Crack extension in elastic-plastic material involves energy dissipation through the creation of new crack surfaces and additional yielding around the crack front. An analytical procedure, using a two-dimensional elastic-plastic finite element method, was developed to calculate the energy dissipation components during a quasi-static crack extension. The fracture of an isotropic compact specimen was numerically simulated using the critical crack-tip-opening-displacement (CTOD) growth criterion. Two specimen sizes were analyzed for three values of critical CTOD. Results from the analyses showed that the total energy dissipation rate consisted of three components: the crack separation energy rate, the plastic energy dissipation rate, and the residual strain energy rate. All three energy dissipation components and the total energy dissipation rate initially increased with crack extension and finally reached constant values.

Shivakumar, K. N.↗
NASA NTRS1986

Short fatigue cracks in notched aluminum specimens

The short-crack fatigue behavior in notched specimens of Al 2024-T3 was studied at values of the stress ratio, R, equal to 0.5, 0.0, -1.0, and -2.0. Crack growth was monitored using a replica technique for cracks ranging in length from a few tens of a micron to the specimen's thickness (2.3 mm). Crack opening displacement was measured for surface cracks as short as 0.035 mm using the interferometric strain/displacement gage, a laser-based optical technique described by Sharpe (1982). It was found that the growth rates of short cracks were faster than the rates of long cracks for R values of -1.0 and -2.0. No significant difference was observed for R = 0.0, and at R = 0.5, the short cracks actually grew more slowly that the long ones. At all R values, the closure stresses measured for short cracks were smaller than those predicted for large cracks.

Lee, J. J.↗
NASA NTRS1987

Energy dissipation associated with crack extension in an elastic-plastic material

Crack extension in elastic-plastic material involves energy dissipation through the creation of new crack surfaces and additional yielding around the crack front. An analytical procedure, using a two-dimensional elastic-plastic finite element method, was developed to calculate the energy dissipation components during a quasi-static crack extension. The fracture of an isotropic compact specimen was numerically simulated using the critical crack-tip-opening-displacement (CTOD) growth criterion. Two specimen sizes were analyzed for three values of critical CTOD. Results from the analysis showed that the total energy dissipation rate consisted of three components: the crack separation energy rate, the plastic energy dissipation rate, and the residual strain energy rate. All three energy dissipation components and the total energy dissipation rate initially increased with crack extension and finally reached constant values.

Shivakumar, K. N.↗
NASA NTRS1972

Stresses in bonded materials with a crack perpendicular to the interface.

The problem of two elastic bonded half planes containing a crack perpendicular to the interface is considered. First the solution for the semi-infinite crack under concentrated wedge loading is given. Then the problem of a finite crack fully imbedded in one of the half planes of terminating at the interface is considered. The Mellin transform in conjunction with the dislocations is used to formulate the problem and to derive the integral equation. The integral equation is solved; the stress intensity factors, the crack surface displacement, and the stresses around the crack tip terminating at the interface are obtained. Noting that the power of the singularity for the interface tip of the crack is not -1/2, a tentative fracture criterion dealing with the initiation of fracture propagation is proposed.

Cook, T. S.↗
NASA NTRS1982

Transient thermal stress problem for a circumferentially cracked hollow cylinder

The transient thermal stress problem for a hollow elasticity cylinder containing an internal circumferential edge crack is considered. It is assumed that the problem is axisymmetric with regard to the crack geometry and the loading, and that the inertia effects are negligible. The problem is solved for a cylinder which is suddenly cooled from inside. First the transient temperature and stress distributions in an uncracked cylinder are calculated. By using the equal and opposite of this thermal stress as the crack surface traction in the isothermal cylinder the crack problem is then solved and the stress intensity factor is calculated. The numerical results are obtained as a function of the Fourier number tD/b(2) representing the time for various inner-to-outer radius ratios and relative crack depths, where D and b are respectively the coefficient of diffusivity and the outer radius of the cylinder.

Nied, H. F.↗
NASA NTRS1988

COD measurements at various positions along a crack

Load versus crack-opening-displacement (COD) was measured at various positions along the border of a fatigue crack as it grew from a small surface crack on the edge of an aluminum specimen into a through-the-thickness crack. Displacements were measured with a laser-based interferometric system with a gage length of 70 microns and a resolution of 0.01 micron. These load-COD curves can be used to determine opening loads and thereby investigate the effect of closure on the growth of small cracks. In general, the opening loads decrease as the crack grows.

Sharpe, W. N., Jr.↗
NASA NTRS1990

A study of hydrogen environment effects on microstructure property behavior of NASA-23 alloy and related alloy systems

This work is part of the overall advanced main combustion chamber (AMCC) casting characterization program of the Materials and Processes Laboratory of the Marshall Space Flight Center. The influence of hydrogen on the tensile properties and ductility behavior of NASA-23 alloy were analyzed. NASA-23 and other referenced alloys in cast and hipped conditions were solution treated and aged under selected conditions and characterized using optical metallography, scanning electron microscopy, and electron microprobe analysis techniques. The yield strength of NASA-23 is not affected much by hydrogen under tensile tests carried at 5000 psig conditions; however, the ultimate strength and ductility properties are degraded. This implies that the physical mechanisms operating would be related to the plastic deformation process. The fracture surfaces characteristics of NASA-23 specimens tensile tested in hydrogen, helium, and air were also analyzed. These revealed surface cracks around specimen periphery with the fracture surface showing a combination of intergranular and transgranular modes of fracture. It is seen that the specimens charged in hydrogen seem to favor a more brittle fracture mode in comparison to air and helium charged specimens. The AMCC casting characterization program is to be analyzed for their hydrogen behavior. As a result of this program, the basic microstructural factors and fracture characteristics in some cases were analyzed.

Diwan, Ravinder M.↗
NASA NTRS1976

Fracture analysis of surface and through cracks in cylindrical pressure vessels

A previously developed fracture criterion was applied to fracture data for surface- and through-cracked cylindrical pressure vessels to see how well the criterion can correlate fracture data. Fracture data from the literature on surface cracks in aluminum alloy, steel, and epoxy vessels, and on through cracks in aluminum alloy, titanium alloy steel, and brass vessels were analyzed by using the fracture criterion. The criterion correlated the failure stresses to within + or - 10 percent for either surface or through cracks over a wide range of crack size and vessel diameter. The fracture criterion was also found to correlate failure stresses to within + or - 10 percent for flat plates (center-crack or double-edge-crack tension specimens) and cylindrical pressure vessels containing through cracks.

Newman, J. C., Jr.↗
DOE OSTI2020

Multi-physics modeling of injected nanoparticles effect on remediation of CO 2 leakage through cracks

One potential risk in CO 2 sequestration is the leakage of carbon dioxide, which can result in contamination of underground water, creating potential threats to existing ecosystems. The common leakage pathway is through the pre-existing fractures or discontinuities within cement in the wellbore, incurred by the environmental conditions imposed on the cement. Injecting nanoparticles into pre-existing cracks is one of the most recently proposed ideas for mitigating fracture propagation in cement CO 2 sequestration. To demonstrate the feasibility of this new technology, a numerical approach was taken in this work, as it is challenging to investigate it in a laboratory setting. We proposed a coupled ALE (Arbitrary Lagrangian–Eulerian)–DEM (Discrete Element Method)–peridynamic modeling strategy within the LS-Dyna package to investigate the intertwined interaction among the CO 2 fluid flow, native fluid (e.g., brine), particle clusters, and cracks within the cement. The numerical results demonstrate that injected nanoparticles can effectively reduce the pressure exerted on the crack surface. Accordingly, the potential fracture propagation at the crack tip would be reduced compared to corresponding cases without nanoparticels as pressurized by fluid flow. This result verifies the effectiveness of proposed nanoparticle injection technology. Finally, using this established modeling strategy, the effect of filling particles on the fracture mitigation for different crack geometries (e.g. particle cluster patterns, aspect ratio of crack aperture and length) and CO 2 reservoir pressure are examined. The result shows that injected particles successfully reduce the fracture propagation in these scenarios.

42 ENGINEERING↗
NASA NTRS1974

Study of a flight monitor for jet engine disk cracks using the critical length criterion of fracture mechanics

A disk crack detector is discussed which is intended to operate while in flight. The crack detector monitors the disk rim for radial surface cracks emanating from the blade root interface. An eddy current type sensor with a remotely located capacitance-resistance bridge and signal analyzer is able to detect reliably a simulated crack 1/8 in. long. The sensor was tested at rim velocities of 600 fps and at 1000 F. Fracture mechanics is used to calculate the critical crack length. Knowledge of the crack growth rate permits the calculation of the number of stress cycles remaining for the detected crack to grow to critical size. A plot is presented of the remaining life as a function of the critical crack length and the operating stress. It is shown that for a disk of Inconel 718 a through-the-thickness crack operating under a rim stress of 50 kpsi has a critical length of 0.7-in. and a remaining life of 130 flights.

Barranger, J. P.↗
NASA NTRS1991

Environment enhanced fatigue of advanced aluminum alloys and metal matrix composites

The environmental fatigue crack propagation behavior of advanced Al-Li-Cu based alloys and metal matrix composites is being characterized. Aqueous NaCl and water vapor, which produce atomic hydrogen by reactions on clean crack surfaces, are emphasized. The effects of environment sensitive crack closure, stress ratio, and precipitate microstructure are assessed. Mechanistic models are sought for intrinsic crack tip damage processes to enable predictions of cracking behavior outside of the data, metallurgical improvements in material cracking resistance, and insight on hydrogen compatibility.

Slavik, Donald C.↗
NASA NTRS1994

Small crack test program for helicopter materials

Crack propagation tests were conducted to determine crack growth behavior in five helicopter materials for surface cracks between 0.005 to 0.020 inches in depth. Constant amplitude tests were conducted at stress ratios R equals 0.1 and 0.5, and emphasis was placed on near threshold data (i.e., 10-8 to 10-6 inches/cycle). Spectrum tests were conducted using a helicopter spectrum. The test specimen was an unnotched tension specimen, and cracks were initiated from a small EDM notch. An optical/video system was used to monitor crack growth. The material for the test specimens was obtained from helicopter part forgings. Testing was conducted at stresses below yield to reflect actual stresses in helicopter parts.

Annigeri, Bal↗
NASA NTRS2003

Fracture Evaluation of In-Situ Sensors for High Temperature Applications

The feasibility of fabricating an in-situ crack sensor for real-time detection of surface cracks propagating in engine components was evaluated using a computational fracture mechanics model. The in-situ sensor system would be required to: (1) Be capable of sustaining normal function in a severe environment; (2) Transmit a signal if a detected crack in the component was above a predetermined length, but below a critical length that would lead to failure; (3) Act neutrally upon the overall performance of the engine system and not interfere with the engine maintenance operations. In this work, fracture mechanics methodologies are used to identify the requirements for an in-situ sensor system that could withstand the engine operating environment, foreign object damage, and minimally degrade engine performance. A computational fracture mechanics model was developed to evaluate the feasibility of fabricating an in-situ crack sensor for real-time damage propagation detection in engine components.

Forth, Scott C.↗
NASA NTRS2010

Evaluation of a Small-Crack Monitoring System

A new system has been developed to obtain fatigue crack growth rate data from a series of images acquired during fatigue testing of specimens containing small surface cracks that initiate at highly-polished notches. The primary benefit associated with replica-based crack growth rate data methods is preserving a record of the crack configuration during the life of the specimen. Additionally, this system has the benefits of both reducing time and labor, and not requiring introduction of surface replica media into the crack. Fatigue crack growth rate data obtained using this new system are found to be in good agreement with similar results obtained from surface replicas.

Newman, John A.↗