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At least 199 records · Page 11

Ultra-fast and sensitive magneto-optical hydrogen sensors using a magnetic nano-cap array

Magnetism in curved nano-geometries has opened a new path to design novel characteristics and phenomena that could greatly impact the future fundamental and applied studies of materials. Here, in this report, a hexagonally-packed array of magnetic nano-caps (or nano-patches, NP) exhibiting unique magnetic anisotropy and optimal nanostructure for fast hydrogen kinetics is explored as a sensing element for the spark-free magnetic-circular-dichroism (MCD) H 2 sensor. The MCD H 2 sensor outperforms the state-of-the-art optical sensors reported to date and satisfies the most challenging performance targets imposed by US Department of Energy. In particular, a Pd 67 Co 33 NP sensor exhibits response time of t 90 < 0.9 s, recovery time of t 10 < 9.0 s over the 1-100 mbar H 2 partial pressure range, and limit of detection (LOD) of ~1 ppm. The LOD improves to <700 ppb, when the signal-to-noise ratio is enhanced by stacking three NP arrays. Using a 30-nm TAF (Teflon AF 2400) polymer coating, the sorption kinetics of the Pd 67 Co 33 /TAF sensor are significantly accelerated, with t 90 < 0.4 s and t 10 < 2.8 s over the same pressure range. When the Pd 67 Co 33 /TAF sensor is further coated with a 100-nm poly(methyl methacrylate) (PMMA) layer, a rapid sorption time of t 90 < 0.5 s, LOD < 1 ppm and excellent sensor accuracy (<2.5% full scale) are maintained, while the sensor obtains strong selectivity against interference gases and moisture and a negligible aging effect. The MCD nano-cap sensor platform may have a great impact on the future deployment of H 2 fuel, H 2 environmental monitoring sensors, and fast proton-based magneto-ionic devices.

Fast and sensitive hydrogen sensors↗

Ground calibration plan for the Athena/X-IFU microcalorimeter spectrometer

The X-ray Integral Field Unit is the X-ray imaging spectrometer on board one of ESA’s next large missions, Athena. Athena is set to investigate the theme of the Hot and Energetic Universe, with a launch planned in the late-2030s. Based on a high-sensitivity transition edge sensor (TES) detector array operated at very low temperature (50 mK), X-IFU will provide spatially resolved high-resolution spectroscopy of the X-ray sky in the 0.2 to 12 keV energy band, with an energy resolution goal of 4 eV up to 7 keV [3 eV design goal]. This work presents the current calibration plan of the X-IFU. It provides the requirements applicable to the X-IFU calibration, describes the overall calibration strategy, and details the procedure and sources needed for the ground calibration of each parameter or characteristics of the X-IFU.

47 OTHER INSTRUMENTATION↗

“Mirror” magnet experiment for quench studies, quench analysis techniques development and in support of superconducting magnet modeling

In order to progress on various research points related to superconducting magnets, we suggest performing series of tests with induced and natural quenches on a mirror magnet, probably using a “11 T” coil. The “mirror” is to have voltage taps instrumented on half the strands, on both coil ends. It is to be instrumented with multiple spot-heaters, of the order of ten, in designated pole-turn areas. Instrumentation is to include quench antenna array facing the inner coil surface, as well as acoustic sensors on the inner layer pole. Further, acoustic sensors at the magnet ends and an acoustic calibration transducer are to be installed. Thus, we are to test sensitivity and precision of acoustic and quench antenna (QA) array sensors, both at close proximity to the coil, and we are to test and commission acoustic on-magnet real-time “calibration”. New or extended DAQ will be tested as well. In addition to diagnostic development, the purpose of the magnet experiment is to investigate current redistribution in the coil, both during quenching and in operating conditions; to assess voltage build up across strands and in the coil segments during quenching, to explore voltage signature differentiation between different type of quenches; to improve modeling of processes during quenching and for magnet design purposes. In this experiment, we expect to be able to characterize the processes during a quench in unprecedented details.

43 PARTICLE ACCELERATORS↗

Integrated Harsh Environment Gas / Temperature Wireless Microwave Acoustic Sensor System for Fossil Energy Applications

There is a significant need for sensors capable of detecting gases, such as H 2 , O 2 , NO x , SO x within harsh environments encountered in power plants, industrial manufacturing, oil and gas exploration, and aerospace applications. This project successfully demonstrated the use of wireless microwave acoustic sensor technology for the detection of gases (H 2 or O 2 ) from ambient temperatures up to 650°C. The work focused on langasite (LGS) based surface acoustic wave resonator (SAWR) sensors as the harsh-environment sensor platform and explored multiple combinations of high-temperature thin films and device structures which were used to increase the sensor platform stability and detection capability at temperatures in the operational range of 150°C to 700°C. Specific material configurations that were investigated include: yttria-stabilized-zirconia (YSZ) decorated with Pt nanoparticles, atomic layer deposited (ALD) Al 2 O 3 , palladium, and Pt/Al 2 O 3 co-deposited electrode alloys. Through the deposition of YSZ at temperatures as high as 850°C and the use of graded alloy concentrations of Pt in the fabrication of the Pt/Al 2 O 3 electrode structures, film stress problems were mitigated, and sensor operation and stability achieved. To test and evaluate SAWR sensor performance for the detection of H 2 and O 2 under the influence of temperature variations, a comprehensive gas sensor control system and test apparatus was created to operate within a laboratory box furnace-controlled environment. In addition to the advancement in thin film materials through the deposition and fabrication techniques mentioned above, the work characterized the performance of sensors containing these films in the presence of oxidizing and reducing gases between 25°C and 700°C. In particular, the work revealed that the exposure of the SAWR sensor surfaces to oxidizing environments significantly improve the sensor response to H 2 , whereas the exposure of the sensor to reducing environments at high temperatures (≈ 500°C) renders the sensor irresponsive to H 2 , requiring sensor surface treatment at high temperatures (above 500°C) to recover the responsiveness to H 2 . The SAWR sensors have been also tested for wireless operation and array operation using multiple orientations to resolve the detection of gases under temperature variations. The work developed at the University of Maine was aided by a collaboration with the NETL Research and Innovation Center, Pittsburgh, PA, where thin film materials and device structures fabricated at UMaine were tested and characterized using NETL gas reactors and surface analysis techniques. SAWR sensors fabricated at UMaine were exposed multiple times to temperatures up to 700°C and H 2 concentrations up to 100% in the NETL facilities to measure the sensor performance. Environetix Technologies Corporation, a UMaine harsh-environment sensor spin-off company, also provided support and assistance in sensor system testing and implementation. The sensor small size and configuration allows flexible sensor placement and embedding of multiple sensor arrays into a variety of components within power systems and other aerospace or industrial settings that need to be interrogated wirelessly. The SAW platform is an attractive option for high-temperature harsh-environment gas sensing applications due to its inherent features, namely small size, capability of battery-free and wireless operation, and cost effective scale production using well-established production techniques from the semiconductor industry. The research findings achieved in this work, particularly advances regarding the fabrication and performance of the SAWR gas sensor platform, can be adapted and transferred to industrial power plants and other harsh environments.

01 COAL, LIGNITE, AND PEAT↗

Multichannel angular spectrometer

A multichannel angular spectrometer includes an array of fiber pickups having an arcuate arrangement and focused about a sample volume. A broadband light source is configured to illuminate a sample within the sample volume. At least one dispersion element is in optical communication with the array of fiber pickups. An imaging sensor is in optical communication with the array of fiber pickups. The imaging sensor is configured to image the broadband light received by the array of fiber pickups and dispersed by the at least one dispersion element. A processor is in electrical communication with the imaging sensor. The processor has a power supply and computer-readable memory.

47 OTHER INSTRUMENTATION↗

Monitoring changes in human activity during the COVID-19 shutdown in Las Vegas using infrasound microbarometers

While studies of urban acoustics are typically restricted to the audio range, anthropogenic activity also generates infrasound (<20 Hz, roughly at the lower end of the range of human hearing). Shutdowns related to the COVID-19 pandemic unintentionally created ideal conditions for the study of urban infrasound and low frequency audio (20–500 Hz), as closures reduced human-generated ambient noise, while natural signals remained relatively unaffected. An array of infrasound sensors deployed in Las Vegas, NV, provides data for a case study in monitoring human activity during the pandemic through urban acoustics. The array records a sharp decline in acoustic power following the temporary shutdown of businesses deemed nonessential by the state of Nevada. This decline varies spatially across the array, with stations close to McCarran International Airport generally recording the greatest declines in acoustic power. Further, declines in acoustic power fluctuate with the time of day. As only signals associated with anthropogenic activity are expected to decline, this gives a rough indication of periodicities in urban acoustics throughout Las Vegas. This study's results reflect the city's response to the pandemic and suggest spatiotemporal trends in acoustics outside of shutdowns.

58 GEOSCIENCES↗

Low Noise Frequency-Domain Multiplexing of TES Bolometers Using SQUIDs at Sub-Kelvin Temperature

Digital Frequency-Domain Multiplexing (DfMux) is a technique that uses MHz superconducting resonators and Superconducting Quantum Interference Device (SQUID) arrays to read out sets of transition edge sensors. DfMux has been used by several Cosmic Microwave Background experiments, including most recently POLARBEAR-2 and SPT-3 G with multiplexing factors as high as 68, and is the baseline readout technology for the planned satellite mission LiteBIRD. Here, we present recent work focused on improving DfMux readout noise, reducing parasitic impedance, and improving sensor operation. We have achieved a substantial reduction in stray impedance by integrating the sensors, resonators, and SQUID array onto a single-carrier board operated at 250 mK. This also drastically simplifies the packaging of the cryogenic components and leads to better-controlled crosstalk. We demonstrate a low readout noise level of 8.6 pA/Hz1 1/2 , which was made possible by operating the SQUID array at a reduced temperature and with a low dynamic impedance. This is a factor of two improvement compared to the achieved readout noise level in currently operating Cosmic Microwave Background experiments using DfMux and represents a critical step toward maturation of the technology for the next generation of instruments.

47 OTHER INSTRUMENTATION↗

Operational Conditions of Silicon Pixel Arrays for X-Ray Spectroscopy

Arrays of silicon sensors can be utilized in those spectroscopic applications where a high event throughput is needed, for example in synchrotron-based experiments. Yet, in such arrays several noise contributions, beyond the well-known leakage, thermal and flicker noises, can be present which are absent in single channel detectors. Additional noise is generated ultimately by the condition at the silicon/silicon oxide interface, which in turn depends on the parameters of the silicon oxide over the not-implanted gaps. We discuss how to control this region to obtain the best spectroscopic performances.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Urban Seismic Site Characterization by Fiber-Optic Seismology

ccurate ground motion prediction requires detailed site effect assessment, but in urban areas where such assessments are most important, geotechnical surveys are difficult to perform, limiting their availability. Distributed acoustic sensing (DAS) offers an appealing alternative by repurposing existing fiber-optic cables, normally employed for telecommunication, as an array of seismic sensors. We present a proof-of-concept demonstration by using DAS to produce high-resolution maps of the shallow subsurface with the Stanford DAS array, California. We describe new methods and their assumptions to assess H/V spectral ratio—a technique widely used to estimate the natural frequency of the soil—and to extract Rayleigh wave dispersion curves from ambient seismic field. These measurements are jointly inverted to provide models of shallow seismic velocities and sediment thicknesses above bedrock in central campus. The good agreement with an independent survey validates the methodology and demonstrates the power of DAS for microzonation.

Geochemistry & Geophysics↗

Modular low cost trackerless spectral sensor

A photodiode sensor device and systems. The photodiode sensor device includes a housing portion. The housing portion includes a cylindrical enclosure. A window is disposed at a first end of the housing portion. A filter wheel is within the housing portion. A motor positioned within the housing is adjacent the filter wheel opposite the window. The motor is attached to the filter wheel. A photodiode sensor within the housing portion intermediate the first photodiode sensor and the window. The first photodiode sensor receives filtered light incident on the window and transmit a signal associated with sensed parameters of the filtered light. Also, a hemispherical dome for diffusing the light to a collimating lens has a grating, a focusing lens, and a linear detector array. An exit port transmits light to the collimating lens. The sensor array is opposite the grating for sensing the diffused light.

14 SOLAR ENERGY↗

The DataHawk2 uncrewed aircraft system for atmospheric research

Abstract. The DataHawk2 (DH2) is a small, fixed-wing, uncrewed aircraft system, or UAS, developed at the University of Colorado (CU) primarily for taking detailed thermodynamic measurements of the atmospheric boundary layer. The DH2 weighs 1.7 kg and has a wingspan of 1.3 m, with a flight endurance of approximately 60 min, depending on configuration. In the DH2's most modern form, the aircraft carries a Vaisala RSS-421 sensor for pressure, temperature, and relative humidity measurements, two CU-developed infrared temperature sensors, and a CU-developed fine-wire array, in addition to sensors required to support autopilot function (pitot tube with pressure sensor, GPS receiver, inertial measurement unit), from which wind speed and direction can also be estimated. This paper presents a description of the DH2, including information on its design and development work, and puts the DH2 into context with respect to other contemporary UASs. Data from recent field work (MOSAiC, the Multidisciplinary drifting Observatory for the Study of Arctic Climate) is presented and compared with radiosondes deployed during that campaign to provide an overview of sensor and system performance. These data show good agreement across pressure, temperature, and relative humidity as well as across wind speed and direction. Additional examples of measurements provided by the DH2 are given from a variety of previous campaigns in locations ranging from the continental United States to Japan and northern Alaska. Finally, a look toward future system improvements and upcoming research campaign participation is given.

54 ENVIRONMENTAL SCIENCES↗

Optimizing the differential connection schemes for detecting 3D magnetic perturbations in DIII-D

Optimizing the differential pair connection scheme (i.e. the set of pairs) of a toroidal array of magnetic sensors dedicated to measuring slowly rotating asymmetric fields can enhance the mode number detection capability and failure-resilience. In this work the condition number obtained from singular value decomposition (SVD) of the design matrix is used as a metric to evaluate the quality of a connection scheme. A large number of possible pair connections are usually available, so evaluating all of them may require extensive use of computational resources and can be very time consuming. Alternative methods to reduce the number of pairs evaluated without losing the capabilities of toroidal mode detection are presented in this paper. Here, three examples of the applications of such analysis for the 3D magnetic diagnostic system of DIII-D are also presented: the addition of two new toroidal arrays with n > 3 detection capabilities, the modification of an existing toroidal array in the low field side of the machine to accommodate the addition of a helicon antenna, and the design of changes in several toroidal arrays in the high field side to accommodate the addition of a lower hybrid current drive antenna on the center post.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Snapshot multispectral imaging using a diffractive optical network

Abstract Multispectral imaging has been used for numerous applications in e.g., environmental monitoring, aerospace, defense, and biomedicine. Here, we present a diffractive optical network-based multispectral imaging system trained using deep learning to create a virtual spectral filter array at the output image field-of-view. This diffractive multispectral imager performs spatially-coherent imaging over a large spectrum, and at the same time, routes a pre-determined set of spectral channels onto an array of pixels at the output plane, converting a monochrome focal-plane array or image sensor into a multispectral imaging device without any spectral filters or image recovery algorithms. Furthermore, the spectral responsivity of this diffractive multispectral imager is not sensitive to input polarization states. Through numerical simulations, we present different diffractive network designs that achieve snapshot multispectral imaging with 4, 9 and 16 unique spectral bands within the visible spectrum, based on passive spatially-structured diffractive surfaces, with a compact design that axially spans ~72 λ m , where λ m is the mean wavelength of the spectral band of interest. Moreover, we experimentally demonstrate a diffractive multispectral imager based on a 3D-printed diffractive network that creates at its output image plane a spatially repeating virtual spectral filter array with 2 × 2 = 4 unique bands at terahertz spectrum. Due to their compact form factor and computation-free, power-efficient and polarization-insensitive forward operation, diffractive multispectral imagers can be transformative for various imaging and sensing applications and be used at different parts of the electromagnetic spectrum where high-density and wide-area multispectral pixel arrays are not widely available.

36 MATERIALS SCIENCE↗

Resonator Stabilization Architecture to Suppress Switching Transient Crosstalk in I-CDM

The ever-increasing sizes of transition-edge sensor (TES) microcalorimeter arrays motivates improved multiplexed readout with large multiplexing factors, low power dissipation, and low levels of crosstalk. Current-summed code division multiplexing (I-CDM) has been proposed as an alternative to flux-summed code division multiplexing (Φ-CDM) because of its lower power dissipation and greater robustness against the failure of individual readout elements. Simulating I-CDM arrays, we find that unswitched circuit components provide a mechanism for crosstalk, the magnitude of which is determined by their inductance. To mitigate this source of crosstalk, we propose a technique called resonator-stabilized I-CDM (RI-CDM), which the simulations predict will reduce crosstalk by an order of magnitude. RI-CDM reads out dc-biased TESs on an amplitude-modulated carrier wave.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Commercially Fabricated Antenna-Coupled Transition Edge Sensor Bolometer Detectors for Next-Generation Cosmic Microwave Background Polarimetry Experiment

We report on the development of commercially fabricated multi-chronic antenna-coupled transition edge sensor (TES) bolometer arrays for cosmic microwave background (CMB) polarimetry experiments. The orders of magnitude increase in detector count for next-generation CMB experiments require a new approach in detector wafer production to increase fabrication throughput. Here, we describe collaborative efforts with a commercial superconductor electronics fabrication facility (SeeQC, Inc.) to fabricate antenna-coupled TES bolometer detectors. We have successfully fabricated an operational dual-polarization, dichroic sinuous antenna-coupled TES detector array on a 150-mm-diameter wafer. The fabricated detector arrays have average yield of 95% and excellent uniformity across the wafer. Both RF characteristics and TES bolometer properties are suitable for CMB observations. We successfully fabricated different types of TES bolometers optimized for frequency multiplexing readout, time-domain multiplexing readout, and microwave SQUID multiplexing readout. We also demonstrated high production throughput. We discuss the motivation, design considerations, fabrication processes, test results, and how industrial detector fabrication could be a path to fabricate hundreds of detector wafers for future CMB polarimetry experiments.

47 OTHER INSTRUMENTATION↗

Coherent Scattering of Low Mass Dark Matter from Optically Trapped Sensors

In this work, we propose a search for low mass dark matter particles through momentum recoils caused by their scattering from trapped, nanometer-scale objects. Our projections show that even with a modest array of femtogram-mass sensors, parameter space beyond the reach of existing experiments can be explored. The case of smaller, attogram-mass sensors is also analyzed-where dark matter can coherently scatter from the entire sensor-enabling a large enhancement in the scattering cross-section relative to interactions with single nuclei. Large arrays of such sensors have the potential to investigate new parameter space down to dark matter masses as low as 10 keV. If recoils from dark matter are detected by such sensors, their inherent directional sensitivity would allow an unambiguous identification of a dark matter signal.

79 ASTRONOMY AND ASTROPHYSICS↗

Characterization of Temperature Heterogeneity in Utility-Scale Power Plant Boilers by Spatially Distributed Ultrasonic Measurements

In extreme environments, even hardened insertion sensors fail quickly. For such environments, we have developed an ultrasonic (US) method for measuring the spatial distribution of temperatures in solid materials and, specifically, across containments of extreme processes. By deploying US sensors in multiple locations, spatial heterogeneity in temperatures inside harsh environments may be characterized. In this note, we update our progress on testing the developed approach in an industrial setting and its performance in describing the temperature distribution inside a 500 MW (electrical) coalfired utility boiler of an electrical power generation plant. We use waveguides (WG) structured to contain echogenic features that produce a train of echoes in response to an excitation pulse. The time of flight between echoes encodes the information on the temperature distribution in the corresponding segment of the WG, which we reconstruct using its parametrization. Five waveguides were welded to the boiler’s heat exchange surface (waterwall) and different locations at the same boiler elevation and produced reliable US waveforms 18 months after the installation. For several weeks during the latest trial, we performed US measurements in five locations spanning half of the boiler’s 14-meter width. The measurements were acquired during regular operation, including load cycling to adjust for demand and intermittent contributions of renewable power sources, and during boiler shutdown for emergency maintenance and the subsequent restart. The interpretation of US waveforms by signal processing resulted in an accurate estimation of temperature distribution along the waveguides. We captured daily cyclical variations in demand-following load. Measurements performed in multiple locations revealed unexpected temperature variations across the boiler. We conclude that an array of developed sensors can provide responsive and spatial temperature measurements while maintaining functionality despite prolonged exposure to an extreme environment.

Walton, Kenneth↗

Analysis of measurements from an array of radioxenon samplers near to Hartlepool Nuclear Power Station

As part of a scientific research and development project, the radionuclide fingerprint of an operating advanced gas-cooled reactor 25 (AGR) has been studied across several facets (Goodwin et al., 2024). One part of this project was to deploy an array of 26 radioxenon samplers to the region for a period of around 1 year, to measure any radioxenon emissions from the reactors of the 27 Hartlepool nuclear power station at a range of tens of kilometres away. The array of 3 sensors was operational for around 12 28 months from March 2022 and detected many occurrences of isotopes of radioxenon. Here we provide a detailed analysis and 29 interpretation of the data and where possible, attribution of detections to a source or region. Whilst a key part of this work is to 30 measure any emissions of radioxenon from Hartlepool, this work presents one of the most comprehensive efforts to determine the 31 source of a great number of (mostly) 133Xe detections. A combination of different types of atmospheric dispersion modelling 32 techniques, including the use of stack monitoring data from nearby civil radioxenon-emitting nuclear facilities has enabled the 33 majority of detections to be attributed to one or more possible sources. Whilst emissions from Hartlepool have been detected on 34 the systems, the majority of detections are associated with a medical isotope production facility in Fleurus, Belgium (IRE).

Advanced gas-cooled reactor↗