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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 199 records · Page 11
All sourcesNASA NTRSDOE OSTI
DOE OSTI2020

Experimental Investigation of Inhibitive Drilling Fluids Performance: Case Studies from United States Shale Basins

Shale formations are attractive prospects due to their potential in oil and gas production. Some of the largest shale formations in the mainland US, such as the Tuscaloosa Marine Shale (TMS), have reserves estimated to be around 7 billion barrels. Despite their huge potential, shale formations present major concerns for drilling operators. These prospects have unique challenges because of all their alteration and incompatibility issues with drilling and completion fluids. Most shale formations undergo numerous chemical and physical alterations, making their interaction with the drilling and completion fluid systems very complex to understand. In this study, a high-pressure, high-temperature (HPHT) drilling simulator was used to mimic real time drilling operations to investigate the performance of inhibitive drilling fluid systems in two major shale formations (Eagle Ford Shale and Tuscaloosa Marine Shale). A series of drilling experiments using the drilling simulator and clay swelling tests were conducted to evaluate the drilling performance of the KCl drilling fluid and cesium formate brine systems and their effectiveness in minimizing drilling concerns. Cylindrical cores were used to mimic vertical wellbores. It was found that the inhibitive muds systems (KCl and cesium formate) provided improved drilling performance compared to conventional fluid systems. Among the inhibitive systems, the cesium formate brine showed the best drilling performances due to its low swelling rate and improved drilling performance.

04 OIL SHALES AND TAR SANDS↗
DOE OSTI2023

Direct imaging of shock wave splitting in diamond at Mbar pressure

Understanding the behavior of matter at extreme pressures of the order of a megabar (Mbar) is essential to gain insight into various physical phenomena at macroscales—the formation of planets, young stars, and the cores of super-Earths, and at microscales—damage to ceramic materials and high-pressure plastic transformation and phase transitions in solids. Under dynamic compression of solids up to Mbar pressures, even a solid with high strength exhibits plastic properties, causing the induced shock wave to split in two: an elastic precursor and a plastic shock wave. This phenomenon is described by theoretical models based on indirect measurements of material response. The advent of x-ray free-electron lasers (XFELs) has made it possible to use their ultrashort pulses for direct observations of the propagation of shock waves in solid materials by the method of phase-contrast radiography. However, there is still a lack of comprehensive data for verification of theoretical models of different solids. Here, we present the results of an experiment in which the evolution of the coupled elastic–plastic wave structure in diamond was directly observed and studied with submicrometer spatial resolution, using the unique capabilities of the x-ray free-electron laser (XFEL). The direct measurements allowed, for the first time, the fitting and validation of the 2D failure model for diamond in the range of several Mbar. Our experimental approach opens new possibilities for the direct verification and construction of equations of state of matter in the ultra-high-stress range, which are relevant to solving a variety of problems in high-energy-density physics.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Morphological and nanomechanical changes in tungsten in high heat flux conditions

Abstract Morphological and nanomechanical alteration of tungsten in extreme environments, like those in edge localized modes in nuclear fusion environments, up to 46.3 GWm −2 heat fluxes were experimentally simulated using electrothermal plasma. Surface and subsurface damage to the tungsten is seen mainly in the form of pore formation, cracks, and resolidified melt instabilities. Mirco voids, rosette-type microfeatures, core-shell structure, particle enrichment, and submicron channels all manifest in the damaged subsurface. The formation of voids in the subsurface was determined to originate from the ductile fracture of hot tungsten by plastic flow but not developed to cracking. The voids were preferentially settled in grain boundaries, interfaces. The directionality of elongated voids and grains is biased to the heat flow vector or plasma pathway, which is the likely consequence of the thermally driven grain growth and sliding in the high-temperature conditions. The presence of a border between the transient layer and heat-affected zone is observed and attributed to plasma shock and thermal spallation of fractural tungsten at high temperature. Plasma peening-like hardening effects in tungsten were observed in the range of 22.7–46.3 GWm −2 but least in the case of the lowest heat flux, 12.5 GWm −2 .

36 MATERIALS SCIENCE↗
DOE OSTI2021

MHD simulations of cold bubble formation from 2/1 tearing mode during massive gas injection in a tokamak

Massive gas injection (MGI) experiments have been carried out in many tokamaks to study disruption dynamics and mitigation schemes. Two events often observed in those experiments are the excitation of the m = 2, n = 1 magnetohydrodynamic mode, and the formation of cold bubble structure in the temperature distribution before the thermal quench (TQ). Here m is the poloidal mode number, n the toroidal mode number. The physics mechanisms underlying those phenomena, however, have not been entirely clear. In this work, our recent NIMROD simulations of the MGI process in a tokamak have reproduced the main features of both events, which has allowed us to examine and establish the causal relation between them. In these simulations, the 3/1 and 2/1 islands are found to form successively after the arrival of impurity ion cold front at the corresponding q = 3 and q = 2 rational surfaces. At the interface between impurity and plasma, a local thin current sheet forms due to an enhanced local pressure gradient and moves inward following the gas cold front, this may contribute to the formation of a dominant 2/1 mode. Following the growth of the 2/1 tearing mode, the impurity penetration into the core region inside the q = 2 surface gives rise to the formation of the cold bubble temperature structure and initiates the final TQ. Here, a subdominant 1/1 mode developed earlier near the q = 1 surface alone does not cause such a cold bubble formation, however, the exact manner of the preceding impurity penetration depends on the nature of the 1/1 mode: kink-tearing or quasi-interchange.

2/1 tearing mode↗
DOE OSTI2021

Utah FORGE Well 16A(78)-32 Core Photos

Images of core samples collected from Utah FORGE well 16A(78)-32. These images were created by stitching together multiple photographs resulting in a circumferential view of the cores exterior in two dimensions. Core footages (measured depths) are indicated in the file names, and are annotated on each image. The images, of which there are 30 in the .zip file, are in a .jpg format.

15 GEOTHERMAL ENERGY↗
DOE OSTI2022

Search for Supernova Neutrinos and Constraint on the Galactic Star Formation Rate with the KamLAND Data

We present the results of a search for core-collapse supernova neutrinos, using long-term KamLAND data from 2002 March 9 to 2020 April 25. We focus on the electron antineutrinos emitted from supernovae in the energy range of 1.8–111 MeV. Supernovae will make a neutrino event cluster with the duration of ~10 s in the KamLAND data. We find no neutrino clusters and give the upper limit on the supernova rate to be 0.15 yr –1 with a 90% confidence level. The detectable range, which corresponds to a >95% detection probability, is 40–59 kpc and 65–81 kpc for core-collapse supernovae and failed core-collapse supernovae, respectively. This paper proposes to convert the supernova rate obtained by the neutrino observation to the Galactic star formation rate. Assuming a modified Salpeter-type initial mass function, the upper limit on the Galactic star formation rate is <(17.5–22.7) M ⊙ yr –1 with a 90% confidence level.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2022

Mudstone Baffles and Barriers in Lower Cretaceous Strata at a Proposed CO 2 Storage Hub in Kemper County, Mississippi, United States

The Cretaceous and Tertiary deposits in Mississippi, Alabama, and the adjacent continental shelf constitute a widespread succession of sandstone, mudstone, and carbonate that has proven to be an important target for geologic CO 2 storage in the onshore Gulf of Mexico basin. Integrated analysis of stratigraphy, sedimentology, and reservoir properties based on cores and geophysical well logs indicates that the Paluxy Formation and Washita- Fredericksburg interval present gigatonne-class storage opportunities. The distribution, geometry, and composition of the area is a direct reflection of the original depositional environments, and understanding these factors is essential for understanding the geologic storage potential of the Paluxy Formation and Washita-Fredericksburg interval at the Kemper County energy facility in Mississippi. Geologic characterization of the Mississippi Embayment at the energy facility focused primarily on characterizing the confinement potential of the storage complex. Integration of core analyses and geophysical well logs has yielded a high-resolution stratigraphic analysis of storage reservoirs, baffles, barriers, and seals. Scanning electron microscopy (SEM) coupled with energy dispersive X-ray spectroscopy (EDS), and quantitative X-ray diffraction (XRD) was used to characterize microfabric, pore types, and mineralogy within mudstone of the east-central Mississippi Embayment at the Kemper County energy facility. Mudstone beds in the Paluxy Formation and Washita-Fredericksburg interval have variable thickness and continuity. High water saturation in the Cretaceous mudstone units influences swelling smectite clay and mudrock permeability based on pulse decay analysis is 1–96 nD. These low permeability values indicate that the mudstone units are effective baffles, barriers, and confining intervals that make significant migration of injected CO 2 out of the storage complex unlikely. The numerous baffles and barriers within the target reservoir intervals, moreover, favor the retention of multiple CO 2 in plumes within the abundant stacked sandstone bodies.

03 NATURAL GAS↗
DOE OSTI2023

The role of the metal core in the performance of WO x inverse catalysts

In this study, metal-metal oxide inverse catalysts are valuable in diverse applications but selecting pairs is challenging. Here we investigate the role of metal cores (Pt, Ru, Rh, Pd, Ni) in the formation and dynamics of Brønsted acid sites on WO x overlayer on carbon. By in situ/ex situ characterizations, probe chemistry kinetics, and DFT calculations, we demonstrate that metals with varying work functions promote the WO x dispersion, enhancing the Brønsted acidity than the 3D crystallites on carbon at submonolayer coverages by tuning the oxidation state of WO x . The metal core impacts the water splitting and hydroxylation of WO x . Water splitting on Ru-WO x is thermodynamically favorable compared to Ni-WO x and increases the dehydration rate on the former, leading to an activity enhancement by increasing the H 2 pulsing frequency. This study provides insights into optimizing inverse catalysts.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Cluster environment quenches the star formation of low-mass satellite galaxies from the inside-out

ABSTRACT Environment plays a critical role in the star formation history of galaxies. Tidal and hydrodynamical stripping, prominent in cluster environment, can remove the peripheral gas of galaxies and star formation may thus be environmentally suppressed from the outside-in. We revisit the environmental dependence of the radial gradient of specific star formation rate (sSFR) profile. We probe the radial gradient by using the archival spectral indices D4000n and HδA measured from SDSS fibre spectra, to indicate central sSFR and the total sSFR from fitting the spectral energy distribution. Despite the low spatial resolution, the wealth of SDSS data allows to disentangle the dependences on stellar mass, sSFR, and environment. We find that low-mass satellite galaxies in the mass range $9\lt \mathrm{log}\, \mathcal {M}_{\star }/\mathcal {M}_{\odot }\lt 9.8$ on average quench in more inside-out pattern compared to isolated galaxies matched in mass, sSFR, and fibre coverage. This environmental effect is particularly strong for galaxies below the star formation main sequence, and peaks for those in the core of massive clusters where the phase-space diagram reveals clear links between the inside-out quenching and orbital properties. Our results suggest that both tidal and hydrodynamical interactions in cluster environment suppress the star formation of satellites mainly from the inside-out. As accreted gas of low angular momentum from hot gas haloes is an important source for replenishing central gas reservoir, we discuss how gas stripping in clusters may lead to starvation and cause inside-out quenching when the outer star-forming discs are not significantly affected.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2024

Prospects for direct detection of black hole formation in neutron star mergers with next-generation gravitational-wave detectors

A direct detection of black hole formation in neutron star mergers would provide invaluable information about matter in neutron star cores and finite temperature effects on the nuclear equation of state. We study black hole formation in neutron star mergers using a set of 190 numerical relativity simulations consisting of long-lived and black-hole-forming remnants. The postmerger gravitational-wave spectrum of a long-lived remnant has greatly reduced power at a frequency 𝑓 greater than 𝑓 peak , for 𝑓 ≳ 4 kHz, with 𝑓 peak ∈ [2.5,4] kHz. On the other hand, black-hole-forming remnants exhibit excess power in the same large 𝑓 region and manifest exponential damping in the time domain characteristic of a quasinormal mode. We demonstrate that the gravitational-wave signal from a collapsed remnant is indeed a quasinormal ringing. We report on the opportunity for direct detections of black hole formation with next-generation gravitational-wave detectors such as Cosmic Explorer and Einstein Telescope and set forth the tantalizing prospect of such observations up to a distance of 100 Mpc for an optimally oriented and located source with an SNR of 4.

Astronomy & Astrophysics↗
DOE OSTI2021

Core Mass Estimates in Strong Lensing Galaxy Clusters Using a Single-halo Lens Model

The core mass of galaxy clusters is an important probe of structure formation. Here we evaluate the use of a single-halo model (SHM) as an efficient method to estimate the strong lensing cluster core mass, testing it with ray-traced images from the Outer Rim simulation. Unlike detailed lens models, the SHM represents the cluster mass distribution with a single halo and can be automatically generated from the measured lensing constraints. In this work we find that the projected core mass estimated with this method, $M_{\text{SHM}}$, has a scatter of 8.52% and a bias of 0.90% compared to the "true" mass within the same aperture. Our analysis shows no systematic correlation between the scatter or bias and the lens-source system properties. The bias and scatter can be reduced to 3.26% and 0.34%, respectively, by excluding models that fail a visual inspection test. We find that the SHM success depends on the lensing geometry, with single giant arc configurations accounting for most of the failed cases due to their limiting constraining power. When excluding such cases, we measure a scatter and bias of 3.88% and 0.84%, respectively. Finally, we find that when the source redshift is unknown, the model-predicted redshifts are overestimated, and the $M_{\text{SHM}}$ is underestimated by a few percent, highlighting the importance of securing spectroscopic redshifts of background sources. Our analysis provides a quantitative characterization of $M_{\text{SHM}}$, enabling its efficient use as a tool to estimate the strong lensing cluster core masses in the large samples, expected from current and future surveys.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2023

Abbreviated Technical Report: Experimentally Interrogating Detonation Chemistry on Sub-Nanosecond to Nanosecond Timescales

Direct experimental measurement of chemical reactions during high explosive detonation remains challenging. Theory and modeling have long preceded experiment in the fundamental physical and chemical kinetic properties of detonation, and experimentation at the relevant timescales are needed to both validate models and provide fundamental understanding of detonation. In this LDRD-ER project, two approaches, x-ray diffraction and core-level x-ray Raman, were developed and used to further experimental capabilities to address this gap. We further developed dynamic x-ray diffraction to directly detect nanodiamond formation during detonation, providing experimental data towards resolving longstanding controversy in the scientific literature, and although the full kinetics have not yet been fully mapped, diamond diffraction appears on the same timescales as detonation soot formation. In the second research thrust, we have developed core-level x-ray Raman for use with high explosives. This technique provides information analogous to x-ray absorption spectroscopy and electron energy loss spectroscopy, but uses inelastic scattering of hard x-rays that can interrogate chemistry around light elements much deeper into the material. The low cross section and requisite high solid angle collection have hindered its use for ultra-fast spectroscopy. We developed and tested a high-q spectrometer which will substantially increase cross section and signal-to-noise, showing this method will also not dramatically alter, compared to x-ray absorption, the most discriminating spectral features of C, N, and O from various high explosives and expected detonation products. We have also used x-ray Raman combined with OCEAN electronic structure calculations to explore dynamic photodegradation mechanisms in PETN and CL-20 explosives. This provides a pathway towards implementing capability to dynamically explore chemistry at an x-ray free electron laser.

36 MATERIALS SCIENCE↗
DOE OSTI2025

The formation and structure of iron-dominated planetesimals

Metal-rich asteroids and iron meteorites are considered core remnants of differentiated planetesimals and/or products of oxygen-depleted accretion. Investigating the origins of iron-rich planetesimals could provide key insights into planet formation mechanisms. Using differentiation models, we evaluate the interior structure and composition of representative-sized planetesimals (~200 km diameter), while varying oxygen fugacity and initial bulk meteoritic composition. Under the oxygen-poor conditions that likely existed early in the inner regions of the Solar System and other protoplanetary disks, core fractions remain relatively consistent across a range of bulk compositions (CI, H, EH, and CBa). Some of these cores could incorporate significant amounts of silicon (10–30 weight%) and explain the metal fractions of Fe-rich bodies in the absence of mantle stripping. Conversely, planetesimals forming under more oxidizing conditions, such as beyond snow lines, could exhibit smaller cores, enriched in carbon, sulfur (>1 wt%), and oxides. Sulfur-rich cores, like those formed from EH and H bulk compositions, could remain partly molten, sustain dynamos, and even drive sulfur-rich volcanism. Additionally, bodies with high carbon contents, such as CI compositions, can form graphitic outer layers. These variations highlight the importance of initial formation conditions in shaping planetesimal structures. Future missions, such as NASA’s Psyche mission, offer an opportunity to measure the relative abundances of key elements (Fe, Ni, Si, and S) necessary to distinguish among formation scenarios and structure models for Fe-rich and reduced planetesimals.

meteorites↗
DOE OSTI2024

Computed Tomography Scanning and Geophysical Measurements of UW Enterprises LP 1-250512-129 Well in Southwestern Indiana

The computed tomography (CT) facilities and the Multi-Sensor Core Logger (MSCL) at the National Energy Technology Laboratory (NETL) in Morgantown, West Virginia, were used to characterize Illinois Basin core of the Upper Devonian-Early Mississippian New Albany Shale Formation from Posey County, Indiana. The primary impetus of this work is a collaboration between Indiana Geological and Water Survey at Indiana University Bloomington, NETL, and Woolsey Operating Company LLC to characterize and make publicly available core information from the New Albany Shale of the Illinois Basin. Core characterization of this unconventional oil/gas well will aid in understanding the lithology changes and the fracture complexity of the New Albany Shale. There is a potential for this formation to be developed in the future for critical mineral and rare earth element (CM/REE) extraction. The resultant datasets are presented in this report and can be accessed from NETL's Energy Data eXchange (EDX) online system using the following link: https://edx.netl.doe.gov/dataset/uw-enterprises. All equipment and techniques used were non-destructive, enabling future examinations and analyses to be performed on this core. None of the equipment used was suitable for direct visualization of the pore space in the fine-grained structures studied; however, fractures, discontinuities, and millimeter-scale features were readily detectable with the methods tested. Imaging with the NETL medical CT scanner was performed on the entire core. Targeted higher resolution CT scanning of select sections was performed with NETL’s industrial and micro-CT scanner. Qualitative analysis of the medical CT images, coupled with X-ray fluorescence (XRF), P-wave, and magnetic susceptibility measurements from the MSCL were useful in identifying zones of interest for more detailed analysis. The ability to quickly identify key areas for more detailed study with higher resolution will save time and resources in future studies. The combination of methods used provides a multi-scale analysis of the core; the resulting macro and micro descriptions are relevant to many subsurface energy related examinations traditionally performed at NETL.

58 GEOSCIENCES↗
DOE OSTI2025

SPRUCE Measurements of Fine Root Production and Chemistry from Root Ingrowth Cores, Marcell Experimental Forest, Minnesota, 2022-2023

This dataset contains fine root production and tissue chemistry measurements from root ingrowth cores. Ingrowth cores were deployed in peat from June 28, 2022 to June 24, 2023 (2022-06-28 to 2023-06-24) inside SPRUCE Experiment plots at the Marcell Experimental Forest in northern Minnesota. The warming and elevated carbon dioxide (CO2) treatments in this dataset include +0 degrees Celsius (C) (+0 and +500 parts per million (ppm) elevated CO2), +4.5 degrees C (+0 and +500 ppm elevated CO2) and +9 degrees C (+0 and +500 ppm elevated CO2) for both hummocks and hollows, as well as +2.25 degrees C (+0 and +500 ppm) and +6.75 degrees C (+0 and +500 ppm) for hollows from minimum 10 cm depth from the peat surface. Measurements include root average diameter, root length, root biomass, and root tissue nitrogen (%N and δ15N) and carbon (%C and δ13C) concentration per plant functional type and microtopographical feature. Root length and biomass are standardized to 10 cm depth. These data were used to assess the warming and elevated CO2 response of fine roots across different peatland microtopographical features (hummocks and hollows) and plant functional types (shrub, spruce and larch). This dataset contains one data file in comma separate (.csv) format. Additional metadata are provided: one data dictionary and a file-level metadata file in comma separate (.csv) format and a user guide in PDF (*.pdf) format.

ESS-DIVE CSV File Formatting Guidelines Reporting ↗
DOE OSTI2024

Computed Tomography Scanning and Petrophysical Measurements of Eastern Williston Basin Twin Buttes and Hagel Formations

The computed tomography (CT) facilities and the Multi-Sensor Core Logger (MSCL) at the U.S. Department of Energy’s (DOE) National Energy Technology Laboratory (NETL) in Morgantown, West Virginia, were used to characterize core from two wells that represent coal resources across North Dakota. These include the MC23080C Well in Mercer County and the 23-B001 Well in Oliver County. The primary impetus of this work was to capture a detailed digital representation of the core from the MC23080C and 23-B001 Wells. The collaboration between the NETL and the Energy and Environment Research Center (EERC) enables other research entities to access information about this potential carbon ore, rare earth, and critical mineral resource plays in the Williston Basin. All equipment and techniques used were non-destructive, enabling future examinations and analyses to be performed on these cores. Fractures, discontinuities, and millimeter-scale features were readily detectable with the medical CT scanner acquired images. Imaging with the NETL medical CT scanner was performed on entire cores. Qualitative analysis of the medical CT images, coupled with X-ray fluorescence (XRF), gamma density, and magnetic susceptibility measurements from the MSCL were useful in identifying zones of interest for potential future analysis. Higher-resolution industrial and micro-CT images were acquired from selected zones along the depth of the core to visualize the structure in higher detail. The ability to quickly identify key areas for more detailed study with higher resolution will save time and resources in future studies. The combination of methods used provides a multi-scale analysis of the core, with the resulting macro- and micro-descriptions relevant to many subsurface energy-related examinations traditionally performed at NETL.

01 COAL, LIGNITE, AND PEAT↗
DOE OSTI2025

Facies Analysis and Depositional Environments of the Upper Cambrian Eau Claire Formation in Central and Northern Illinois

The Cambrian Eau Claire Formation is a confining unit for geologic carbon dioxide (CO2) storage, and potentially a confining unit for hydrogen storage, within the underlying Mount Simon Sandstone in the Central and Northern Illinois Basin. However, extensive regional studies on lateral continuity, environment of deposition, and depositional fabric of the Eau Claire Formation in the Illinois Basin are minimal compared to studies of the underlying Mount Simon Sandstone. This study presents an integrated facies analysis using sedimentological, stratigraphic, ichnological, and mineralogical data to interpret the depositional environments of the Eau Claire Formation, emphasizing the dynamic nature of sedimentary systems. By combining core analyses, thin-section analysis, facies interpretation from geophysical logs, and regional stratigraphic framework interpretation, this work provides insights into the integrated depositional framework across diverse depositional environments. These findings suggest that the Eau Claire Formation in the Central and Northern Illinois Basin was deposited in a shallow marine environment, ranging from tidal flats to offshore settings. Its mixed siliciclastic-carbonate succession was primarily controlled by relative sea-level change.

58 GEOSCIENCES↗