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All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Unraveling H2 chemisorption and physisorption on metal decorated graphene using quantum Monte Carlo

Molecular hydrogen has the potential to significantly reduce the use of carbon dioxide emitting energy processes. However, hydrogen gas storage is a major bottleneck for its large-scale use as current storage methods are energy intensive. Among different storage methods, physisorbing molecular hydrogen at ambient pressure and temperatures is a promising alternative—particularly in light of the advancements in tunable lightweight nanomaterials and high throughput screening methods. Nonetheless, understanding hydrogen adsorption in well-defined nanomaterials remains experimentally challenging and reference information is scarce despite the proliferation of works predicting hydrogen adsorption. We focus on Li, Na, Ca, and K, decorated graphene sheets as substrates for molecular hydrogen adsorption, and compute the most accurate adsorption energies available to date using quantum diffusion Monte Carlo (DMC). Building on our previous insights at the density functional theory (DFT) level, we find that a weak covalent chemisorption of molecular hydrogen, known as Kubas interaction, is feasible on Ca decorated graphene according to DMC, in agreement with DFT. This finding is in contrast to previous DMC predictions of the 4H2/Ca+ gas cluster (without graphene) where chemisorption is not favored. However, we find that the adsorption energy of hydrogen on metal decorated graphene according to a widely used DFT method is not fully consistent with DMC. The reference adsorption energies reported herein can be used to find better work-horse methods for application in large-scale modeling of hydrogen adsorption. Furthermore, the implications of this work affect strategies for finding suitable hydrogen storage materials and high-throughput methods.

Chemistry↗
NASA NTRS1989

Three-dimensional spherical models of convection in the earth's mantle

Three-dimensional spherical models of mantle convection in the earth reveal that upwelling cylindrical plumes and downwelling planar sheets are the primary features of mantle circulation. Thus subduction zones and descending sheetlike slabs in the mantle are fundamental characteristics of thermal convection in a spherical shell and are not merely the consequences of the rigidity of the slabs, which are cooler than the surrounding mantle. Cylindrical mantle plumes that cause hot spots such as Hawaii are probably the only form of active upwelling and are therefore not just secondary convective currents separate from the large-scale mantle circulation.

Bercovici, Dave↗
NASA NTRS1994

Formation and vesiculation of biomembranes during spaceflight

Shuttle flight, sounding rocket flight, and parabolic flight experiments demonstrate the formation of bilayer membrane vesicles (liposomes) in reduced gravity, following the dilution of detergent from detergent-phospholipid mixed micelles. The reduction in detergent concentration initiates assembly of bilayer membrane sheets, which are sensitive to solution disturbances. An increase in disturbances by forced dilution results in small diameter liposomes (less than 150 nm), in both ground and flight samples. In the absence of forced dilution, liposomes remain small at 1-g, but exhibit much larger diameters at 0-g (1000-2000 nm). Our spaceflight data reveal that membrane assembly and vesiculation are strongly influenced by gravity-induced solution disturbances (e.g., convection currents), which limit vesicle diameter.

Claassen, Dale E.↗
NASA NTRS1999

Mixing Characteristics of Coaxial Injectors at High Gas to Liquid Momentum Ratios

A study of the spray of a swirl coaxial gas-liquid injector operating at high gas to liquid momentum ratios is reported. Mixing and droplet size characteristics of the swirl injector are also compared to a shear coaxial injector, currently being used in the Space Shuttle Main Engine fuel preburner. The injectors were tested at elevated chamber pressures using water as a LOX simulant and nitrogen and helium as gaseous hydrogen simulants. The elevated chamber pressure allowed for matching of several of the preburner injector conditions including; gas to liquid momentum ratio, density ratio and Mach number. Diagnostic techniques used to characterize the spray included; strobe back-light imaging, laser sheet spray imaging, mechanical patternation, and a phase Doppler interferometry. Results thus far indicate that the radial spreading of the swirl coaxial spray is much less than was reported in previous studies of swirl injectors operating at atmospheric back-pressure. The swirl coaxial spray does, however, exhibit a smaller overall droplet size which may be interpreted as an increase in local mixing.

Strakey, P. A.↗
NASA NTRS2013

Mass Properties for Space Systems Standards Development

Current Verbiage in S-120 Applies to Dry Mass. Mass Margin is difference between Required Mass and Predicted Mass. Performance Margin is difference between Predicted Performance and Required Performance. Performance estimates and corresponding margin should be based on Predicted Mass (and other inputs). Contractor Mass Margin reserved from Performance Margin. Remaining performance margin allocated according to mass partials. Compliance can be evaluated effectively by comparison of three areas (preferably on a single sheet). Basic and Predicted Mass (including historical trend). Aggregate potential changes (threats and opportunities) which gives Mass Forecast. Mass Maturity by category (Estimated/Calculated/Actual).

Beech, Geoffrey↗
DOE OSTI2025

Development of Hydrogen Burner for FT4000® Aeroderivative Engine - Final Report

This report details an effort to develop a retrofittable fuel/air injector for the FT4000® aeroderivative gas turbine that enables use of hydrogen as a carbon-free fuel for efficient power generation. The FT4000 engine’s low-NOx combustor was developed by Pratt & Whitney and RTX Technology Research Center with core technology from the Pratt & Whitney PW4000 turbofan aircraft engine. The current FT4000 production engine operates on either natural gas or No. 2 fuel oil with water injection to achieve high thermal efficiency and low emissions. This engine is fielded by Mitsubishi Power Aero and delivers 70 MW of power with a simple-cycle efficiency of over 41% when operating with wet compression. The work reported here advances the technology readiness level of the FT4000 combustor for operation with hydrogen, starting with an experimental assessment of the current production hardware with increasing hydrogen content mixed with natural gas and ending with improved nozzle concepts for fully robust operation with 100% hydrogen. High-pressure single-sector combustor rig tests have been completed, demonstrating the ability for the dual fuel nozzle to operate an FT4000 combustor on 100% hydrogen with low nitrogen oxide (NOx) emissions. Metal temperature measurements and video images of the flame structure from zero to 100% hydrogen highlight opportunities to improve the fuel nozzle robustness for high hydrogen conditions. The design of new fuel/air mixer concepts to improve durability and operability with high hydrogen levels was also completed. A total of eleven new concepts were developed and analyzed, ranging from modifications to the bill-of-materials nozzle to fully clean sheet designs. The concepts were evaluated with non-reacting and reacting flow evaluations to assess the performance of the new hardware designs. Non-reacting tests included Phase Doppler Particle Analysis (PDPA) for droplet size and velocity, mechanical patternation for liquid water flux, and planar laser induced fluorescence (PLIF) with acetone-seeding for gaseous fuel/air mixing characterization. Five scaled candidate fuel nozzle designs, in addition to a scaled bill-of-materials nozzle, were then successfully evaluated in an atmospheric pressure burner rig. The nozzles were evaluated for performance with natural gas, hydrogen/natural gas blends, and pure hydrogen. For 100% hydrogen, the nozzles were evaluated with and without water injection. Optical and infrared imaging of the flame and fuel nozzle was captured. NOx emissions were sampled from fixed emissions probes. The results show measurable differences between the various designs, and the data was used to down-select the two most promising designs to advance to future full pressure rig testing. Results from this study have cleared the current production FT4000 engines with dual fuel nozzles to operate at baseload power on blends of hydrogen mixed with natural gas and water. Two promising nozzle designs have been developed to enable fully robust operation with up to 100% hydrogen. These nozzles require validation at full baseload operating conditions before they can be introduced to the field.

03 NATURAL GAS↗
NASA NTRS1982

The vertical filamentary structures of quiescent prominences

The thin vertical filaments making up the quiescent prominence plasma, as revealed by fine spatial resolution H-alpha photographs, are characterized by a magnetostatic theory in which a horizontal row of long vertical filaments whose weights are supported by bowed magnetic field lines is described by a class of exact equilibrium solutions. The Kippenhahn-Schlueter (1957) solution for a long sheet without filamentary structures is a member of this class of solutions. In illustrating the role of the magnetic field in supporting and thermally shielding the filament plasma, it is found that the filament can have a sharp transition perpendicular to the local field, while the transition in the direction of the local field is diffuse. A consequence of the filamentary structure is that its support by the Lorentz force requires the electric current to have a component along the magnetic field.

Low, B. C.↗
NASA NTRS1976

Heavy ions from the Galilean satellites and the centrifugal distortion of the Jovian magnetosphere

The Galilean satellites constitute a potentially significant source of plasma to the Jovian atmosphere. The paper examines the distortion of the Jovian magnetosphere that would result from injection of ions at the Galilean satellites. The magnetic distortion produced is a localized perturbation near the equatorial plane, in contrast to the large-scale distortion produced by Jovian atmospheric ions. The study estimates the relative perturbation currents resulting from the two sources in terms of the unknown ion production rate at the satellites. It is found that the two perturbations would be of comparable magnitudes if the ion source flux at all of the Galilean satellites were comparable to the photo-ion escape flux from Jupiter's atmosphere. More specifically, ions produced by the Galilean satellites should be confined near the equatorial plane of Jupiter's magnetosphere in a sheet whose thickness is determined by a centrifugal scale height given essentially by the ion thermal speed divided by the corotation frequency.

Hill, T. W.↗
NASA NTRS1991

Evaluation of Surlyn 8920 as PHE Visor Material and Evaluations of New Adhesives for Improving Bonding Between Teflon and Stainless Steel at Cryogenic Temperature

Two studies are presented, and in the first study, Surlyn 8920 (an ionic and amorphous low density polyethylene made by Dupont) was evaluated as a possible replacement of Plexyglass G as PHE visor material. Four formulations of the polymer were made by adding different amounts of UV stabilizer, energy quencher, and antioxident in a Brabender Plasticorder. The formulated polymers were molded in the form of sheets in a compression molder. Cut samples from the molded sheets were exposed in a weatherometer and tested on Instron Tensile Tester for strength and elongation. Specially molded samples of the formulated polymers were subjected to Charpy Impact Tests. In the second study, preliminary evaluations of adhesives for improvement of bonding between Teflon and stainless steel (SS) were performed. Kapton, a high temperature polyimide made by Dupont, and a rubber based adhesive made by Potter Paint Co., were evaluated against industrial quality epoxy, the current material used to bond Teflon and SS. The degreased surfaces of the SS discs were etched mechanically, with a few of these etched chemically. The surfaces of the SS discs were etched mechanically, with a few of these etched chemically. Bonding strengths were evaluated using lap shear tests on the Instron Tensile Tester for the samples bonded by Kapton and industrial quality epoxy. Bond strengths were also evaluated using a pull test on the Instron for the samples bonded by Potter adhesive (CWL-152) and industrial quality epoxy. Based on limited lap shear data, Kapton gave bond strength favorable compared to that of industrial epoxy. Based on limited pull test data, Kapton bonded and CWL-152 bonded samples showed poor strength compared to epoxy bonded sample.

Ray, Asit K.↗
NASA NTRS1979

Slicing of Silicon into Sheet Material. Silicon Sheet Growth Development for the Large Area Silicon Sheet Task of the Low Cost Solar Array Project

The use of multiblade slurry sawing to produce silicon wafers from ingots was investigated. The commercially available state of the art process was improved by 20% in terms of area of silicon wafers produced from an ingot. The process was improved 34% on an experimental basis. Economic analyses presented show that further improvements are necessary to approach the desired wafer costs, mostly reduction in expendable materials costs. Tests which indicate that such reduction is possible are included, although demonstration of such reduction was not completed. A new, large capacity saw was designed and tested. Performance comparable with current equipment (in terms of number of wafers/cm) was demonstrated.

Fleming, J. R.↗
NASA NTRS1978

Interplanetary magnetic holes: Theory

Magnetic holes in the interplanetary medium are explained as stationary, non-propagating, equilibrium structures in which there are field-aligned enhancements of the plasma density and/or temperature. Magnetic anti-holes are considered to be associated with depressions in the plasma pressure. In this model, the observed changes in the magnetic field intensity and direction are due to diamagnetic currents that are carried by ions which drift in a sheath as the result of gradients in the magnetic field and in the plasma pressure within the sheath. The thickness of the sheaths considered is approximately a few ion Larmor radii. An electric field is normal to the magnetic field in the sheath. Solutions of Vlasov's equation and Maxwell's equations are presented which account for several types of magnetic holes, including null-sheets, that were observed.

Burlaga, L. F.↗
NASA NTRS1995

Universities Earth System Scientists Program

This document constitutes the final technical report for the National Aeronautics and Space Administration (NASA) Grant NAGW-3172. This grant was instituted to provide for the conduct of research under the Universities Space Research Association's (USRA's) Universities Earth System Scientist Program (UESSP) for the Office of Mission to Planet Earth (OMTPE) at NASA Headquarters. USRA was tasked with the following requirements in support of the Universities Earth System Scientists Programs: (1) Bring to OMTPE fundamental scientific and technical expertise not currently resident at NASA Headquarters covering the broad spectrum of Earth science disciplines; (2) Conduct basic research in order to help establish the state of the science and technological readiness, related to NASA issues and requirements, for the following, near-term, scientific uncertainties, and data/information needs in the areas of global climate change, clouds and radiative balance, sources and sinks of greenhouse gases and the processes that control them, solid earth, oceans, polar ice sheets, land-surface hydrology, ecological dynamics, biological diversity, and sustainable development; (3) Evaluate the scientific state-of-the-field in key selected areas and to assist in the definition of new research thrusts for missions, including those that would incorporate the long-term strategy of the U.S. Global Change Research Program (USGCRP). This will, in part, be accomplished by study and evaluation of the basic science needs of the community as they are used to drive the development and maintenance of a global-scale observing system, the focused research studies, and the implementation of an integrated program of modeling, prediction, and assessment; and (4) Produce specific recommendations and alternative strategies for OMTPE that can serve as a basis for interagency and national and international policy on issues related to Earth sciences.

Estes, John E.↗
NASA NTRS2000

Al-Li Alloy 1441 for Fuselage Applications

A cooperative investigation was conducted to evaluate Al-Cu-Mg-Li alloy 1441 for long service life fuselage applications. Alloy 1441 is currently being used for fuselage applications on the Russian Be-103 amphibious aircraft, and is expected to be used for fuselage skin on a new Tupolev business class aircraft. Alloy 1441 is cold-rollable and has several attributes that make it attractive for fuselage skin applications. These attributes include lower density and higher specific modulus with similar strength as compared to conventional Al-Cu-Mg alloys. Cold-rolled 1441 Al-Li sheet specimens were tested at NASA Langley Research Center (LaRC) and at the All-Russia Institute of Aviation Materials (VIAM) in Russia to evaluate tensile properties, fracture toughness, impact resistance, fatigue life and fatigue crack growth rate. In addition, fuselage panels were fabricated by Tupolev Design Bureau (TDB) using 1441 skins and Al-Zn-Mg-Cu alloy stiffeners. The panels were subjected to cyclic pressurization fatigue tests at TDB and at LaRC to simulate fuselage pressurization/depressurization during aircraft service. This paper discusses the results from this investigation.

Bird, R. K.↗
DOE OSTI2020

Synthesis of nickel selenide thin films for high performance all-solid-state asymmetric supercapacitors

As a significant semiconductor, nickel selenide shows enormous potential and extensive application prospects in the field of sensor, photocatalysis and supercapacitor. In this paper, nickel selenide (Ni 3 Se 2 , NiSe) thin films were successfully fabricated on stainless-steel sheet using a facile, effective electrodeposition technique. The morphologies, microstructures and chemical compositions of the thin films are characterized systematically. Electrochemical tests exhibit that the Ni3Se2 and NiSe possess high specific capacitance of 581.1 F/g and 1644.7 F/g, respectively. A flexible, all-solid-state asymmetric supercapacitor is assembled by utilizing NiSe film as positive electrode and activated carbon as negative electrode. The solid device delivers a high areal capacitance of 27.0 mF/cm 2 at the current density of 0.7 mA/cm 2 . Furthermore, the maximum volumetric energy density and power density of the NiSe//AC asymmetric SCs can achieve 0.26 mWh/cm 3 and 33.35 mW/cm 3 , respectively. The device shows robust cycling stability with 84.6% capacitance retention after 10000 cycles, outstanding flexibility and satisfactory mechanical stability. Moreover, two devices in series can light up a red light-emitting diode, which displayed great potential applications for energy storage.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS1978

Interplanetary magnetic holes - Theory

Magnetic holes in the interplanetary medium are explained as stationary nonpropagating equilibrium structures in which there are field-aligned enhancements of the plasma density and/or temperature. Magnetic antiholes are considered to be associated with depressions in the plasma pressure. In this model the observed changes in the magnetic field intensity and direction are due to diamagnetic currents that are carried by ions which drift in a sheath as the result of gradients in the magnetic field and in the plasma pressure within the sheath. The thickness of the sheaths that we consider is approximately a few ion Larmor radii. An electric field is normal to the magnetic field in the sheath. Solutions of Vlasov's equation and Maxwell's equations are presented which account for several types of magnetic holes, including 'null sheets,' that have been observed.

Burlaga, L. F.↗
NASA NTRS1980

A mass reduction effort of the electric and hybrid vehicle

Weight reduction, cost competitiveness, and elimination of the intrusion beam resulted from the redesign and fabrication using composite materials of the door outer panel and intrusion beam from a Chevrolet Impala. The basis of the redesign involved replacing these two steel parts with a single compression molding using the unique approach of simultaneously curing a sheet molding compound outside panel with a continuous glass fiber intrusion strap. A weight reduction of nearly 11 pounds per door was achieved. Additional weight savings are possible by taking advantage of the elimination of the intrusion beam to design thinner door structures. The parts consolidation approach allows the composite structure to be cost competitive with the original steel design for both the lower production car models and for the near to midterm production vehicles using current state of the art composite production techniques. The design, prototype fabrication, costing, material, properties and compression molding production requirements are discussed.

Freeman, R. B.↗
NASA NTRS1990

Convection in Neptune's magnetosphere

It is assumed that nonthermal escape from Triton's atmosphere produces a co-orbiting torus of unionized gas (presumably nitrogen and hydrogen) that subsequently becomes ionized by electron impact to populate a partial Triton plasma torus analogous to the Io plasma torus in Jupiter's magnetosphere. Centrifugal and magnetic-mirror forces confine the ions to a plasma sheet located between the magnetic and centrifugal equators. The ionization rate, and hence the torus ion concentration, is strongly peaked at the two points (approximately 180 deg apart in longitude) at which Triton's orbit intersects the plasma equator. During the course of Neptune's rotation these intersection points trace out two arcs roughly 75 deg in longitudinal extent, which we take to be the configuration of the resulting (partial) plasma torus. The implied partial ring currents produce a quadrupolar (four-cell) convection system that provides rapid outward transport of plasma from the arcs. Ring-current shielding, however, prevents this convection system from penetrating very far inside the plasma-arc distance. It is suggested that this convection/shielding process accounts for the radial confinement of trapped particles (150 keV or greater) within L = 14.3 as observed by the Voyager LECP instrument.

Hill, T. W.↗
DOE OSTI2020

Electrochemical cells and methods of manufacturing the same

Electrochemical cells and methods of making electrochemical cells are described herein. In some embodiments, an apparatus includes a multi-layer sheet for encasing an electrode material for an electrochemical cell. The multi-layer sheet including an outer layer, an intermediate layer that includes a conductive substrate, and an inner layer disposed on a portion of the conductive substrate. The intermediate layer is disposed between the outer layer and the inner layer. The inner layer defines an opening through which a conductive region of the intermediate layer is exposed such that the electrode material can be electrically connected to the conductive region. Thus, the intermediate layer can serve as a current collector for the electrochemical cell.

25 ENERGY STORAGE↗

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