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All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Recycling of Pretreated Polyolefin-Based Ocean-Bound Plastic Waste by Incorporating Clay and Rubber

Plastic waste found in oceans has become a major concern because of its impact on marine organisms and human health. There is significant global interest in recycling these materials, but their reclamation, sorting, cleaning, and reprocessing, along with the degradation that occurs in the natural environment, all make it difficult to achieve high quality recycled resins from ocean plastic waste. To mitigate these limitations, various additives including clay and rubber were explored. In this study, we compounded different types of ocean-bound (o-HDPE and o-PP) and virgin polymers (v-LDPE and v-PS) with various additives including a functionalized clay, styrene-multi-block-copolymer (SMB), and ethylene-propylene-based rubber (EPR). Physical observation showed that all blends containing PS were brittle due to the weak interfaces between the polyolefin regions and the PS domains within the polymer blend matrix. Blends containing clay showed rough surfaces and brittleness because of the non-uniform distribution of clay particles in the polymer matrix. To evaluate the properties and compatibility of the blends, characterizations using differential scanning calorimetry (DSC), scanning electron microscopy (SEM), and small-amplitude oscillatory shear (SAOS) rheology were carried out. The polymer blend (v-LDPE, o-HDPE, o-PP) containing EPR showed improved elasticity. Incorporating additives such as rubber could improve the mechanical properties of polymer blends for recycling purposes.

42 ENGINEERING↗
NASA NTRS1974

Grain orientation in lunar soil

Orientation of lunar soil particles in a vertical plane, as seen in the radiographs of core tubes was characterized by preparing orientation diagrams for the different stratigraphic units. Radiographs of double-core drive tubes 64001/64002, 60009/60010, and 60013/60014 were used. The orientation results reinforced the stratigraphic differences. Another source of fabric data was the laboratory-deposited sample 14163,148. The artificial deposition results showed that the grain arrangements were dependent upon the method of deposition. These results from lunar soil and other data from a crushed basalt simulant can be a basis for the inference that lunar soil grain orientation and properties are useful in interpreting lunar surface history.

Mahmood, A.↗
NASA NTRS1978

Ion tracking in an electrostatic potential distribution

An ion tracking system utilizing a single detector was designed to resolve two dimensional potential distributions in a vacuum. The ion detector consisted of a continuous dynode electron multiplier tube mounted behind a series of aperture plates. The detector was located on a track below a wedge shaped structure used to produce the desired potential distribution. A 150 volt electron beam aimed at selected regions, ionized the residual gas in the chamber. The ions were ejected from their source points by electrostatic forces causing them to drift downward toward the detector. Measurements of particle energy, detector position, and entry angle of the incoming particle flux were used to initialize a computer trajectory-tracing program. The program assumes a known theoretically calculated potential distribution near the wedge for computation of particle trajectories, providing a basis for evaluating the data. Special attention was given to characterization of the ion detector.

Ross, D. P.↗
NASA NTRS1988

Comparative study of cross-field and field-aligned electron beams in active experiments

Beam-plasma interactions associated with the cross-field and field-aligned injection of electron beams from spacecraft were investigated using a two-dimensional (three velocity component) electrostatic particle simulations. It is shown that the beam properties and plasma response can be characterized well by the ratio between the stagnation time and the plasma response time, which depends on the ratio of the ambient plasma density to the beam density, the beam width, the beam energy, and the spacecraft length. It was found that the beams injected across the field lines tend to lose their coherence after about one or two gyrations due to space-charge oscillations induced by the beam, irrespective of the spacecraft charging. These oscillations scatter the beam electrons into a hollow cylinder of a radius equal to a beam electron gyroradius and thickness of the order of two beam Debye lengths. Parallel injected beams are subjected to similar oscillations, which cause the beam to expand to fill a solid cylinder of a comparable thickness.

Winglee, R. M.↗
NASA NTRS1989

Physical characterization of asteroid surfaces from photometric analysis

The feasibility of using photometric models like Hapke's (1981, 1984, 1986) equation for deriving physical properties of asteroids from photometric observations is discussed. Using data for Ceres and Vesta, it is shown that the incomplete phase-angle coverage limits the reliable determination of Hapke's photometric parameters from asteroid disk-integrated phase curves (the second limitation is the nonsphericity of many asteroids). However, within this limitations, certain trends among asteroids can be compared. It is shown that there is a general similarity among the Hapke's parameters other than the h parameter, which characterizes the width of the opposition surge in terms of soil structure (porosity, particle-size distribution, and the rate of compaction with depth), derived for similar objects, e.g., average C asteroids and Ceres, and average S asteroids, 1982 Apollo, and Vesta.

Helfenstein, P.↗
NASA NTRS1998

Optical Instrumentation for Temperature and Velocity Measurements in Rig Turbines

Non-intrusive optical measurement techniques have been examined in the context of developing robust instruments which can routinely yield data of engineering utility in high speed turbomachinery test rigs. The engineering requirements of such a measurement are presented. Of particular interest were approaches that provide both velocity and state-variable information in order to be able to completely characterize transonic flowfields. Consideration of all of the requirements lead to the selection of particle image velocimetry (PIV) for the approach to velocity measurement while laser induced fluorescence of oxygen (O2 LIF) appeared to offer the most promise for gas temperature measurement. A PIV system was developed and demonstrated on a transonic turbine stage in the MIT blowdown turbine facility. A comprehensive data set has been taken at one flow condition. Extensive calibration established the absolute accuracy of the velocity measurements to be 3-5 %. The O2 LIF proved less successful. Although accurate for low speed flows, vibrational freezing of O2 prevented useful measurements in the transonic, 300-600 K operating range of interest here.

Ceyhan, I.↗
NASA NTRS1998

Research on Orbital Plasma Electrodynamics (ROPE)

This final report summarizes some of the important scientific contributions to the Research on Orbital Plasma Electrodynamics (ROPE) investigation, to the Tethered Satellite System (TSS) mission, and to NASA that resulted from the work carried out under this contract at Carmel Research Center. These include Dr. Intriligator's participation in the PIT for the TSS-1R simulations and flight, her participation in ROPE team meetings and IWG meetings, her scientific analyses, and her writing and submitting technical papers to scientific journals. The scientific analyses concentrated on the characterization of energetic ions and their possible relation to pickup ion effects, correlation of particle and other effects (e.g., magnetic field, satellite surface), and collaboration with theorists including with ROPE co-investigators. In addition, scientific analyses were carried out of the effects due to satellite gas releases.

Intriligator, Devrie S.↗
NASA NTRS2002

Combustion Synthesis of Fullerenes and Fullerenic Nanostructures In Microgravity

The objectives of the proposed research were to determine the effects of gravity on fullerenes formation in flames and, based on the observed effects, to develop fundamental understanding of fullerenes formation and to identify engineering principles for fullerenes production. The research method consisted of the operation of laminar diffusion flames under normal- and reduced-gravity conditions, and the collection from the flames and subsequent analysis of condensables including any fullerenes present, using coupled high performance liquid chromatography/mass spectrometry and high resolution transmission electron microscopy. The focus included fullerene molecules C60 and C70 and fullerenic nanostructures including tubes, spherules and other shapes. The normal-gravity experiments were performed at MIT and complementary reduced-gravity experiments were to have been contributed by NASA. The independent variables of interest are gravity, fuel type, fuel/oxygen ratio, pressure, gas velocity at burner, diluent type and concentration. Given the large number of variables and the absence of data on either fullerene formation in diffusion flames or gravitational effects on fullerene formation in diffusion or premixed flames, the first part of the work was exploratory while the later part involved detailed study of the most interesting mechanisms. Samples of condensable material from laminar low pressure benzene/argon/oxygen diffusion flames were collected and analyzed by high-performance liquid chromatography to determine the yields of fullerenes, and by high-resolution transmission electron microscopy (HRTEM) to characterize the fullerenic material, i.e., curved-layer nanostructures, on and within the soot particles. The highest concentration of fullerenes was always detected just above the visible stoichiometric surface of a flame. The percentage of fullerenes in the condensable material increases with decreasing pressure. The overall highest amount of fullerenes was found for a surprisingly high dilution fuel with argon. The maximum flame temperature seems to be of minor importance in fullerene formation. The HRTEM analysis of the soot showed an increase of the curvature of the carbon layers, and hence increased fullerenic character. After this maximum, the curvature decreases. In addition to the soot, the samples included fullerenic nanostructures, such as tubes and spheroids including highly-ordered multilayered or onion-like structures. The soot itself shows highly ordered regions that appear to have been cells of ongoing fullerenic nanostructure formation.

Howard, Jack B.↗
NASA NTRS1994

(abstract) Sciencecraft

The technological capabilities are now at hand to design an integrated system that combines science instruments, spacecraft, and propulsion elements into a single system. The authors have called this a sciencecraft since it is intended to provide automatic scientific observations of planetary and astrophysical objects. Integration of function allows lower mass and cost and supports a short development cycle. A specific science mission is described in this paper, a flyby of Neptune, Triton, and an object in the Kuiper belt. The SCIENCECRAFT system is described. It has electric propulsion and is capable of measuring the surface constituents and morphology of objects visited and characterizing their atmospheres both in emission and adsorption (against the Sun). Miniature fields and particles experiments are incorporated that will provide interplanetary information together with details of the magnetic and electric attributes of each object. The Sciencecraft is Delta launched and has a flight time to the Kuiper belt of 7 years. The design is such that the craft functions in a largely autonomous mode to provide low cost mission operations.

planetary astrophysics science instruments spacecr↗
NASA NTRS2008

Solar Probe Plus: Report of the Science and Technology Definition Team

Solar Probe+ will be an extraordinary and historic mission, exploring what is arguably the last region of the solar system to be visited by a spacecraft, the Sun s outer atmosphere or corona as it extends out into space. Approaching as close as 9.5 RS* (8.5 RS above the Sun s surface), Solar Probe+ will repeatedly sample the near-Sun environment, revolutionizing our knowledge and understanding of coronal heating and of the origin and evolution of the solar wind and answering critical questions in heliophysics that have been ranked as top priorities for decades. Moreover, by making direct, in-situ measurements of the region where some of the most hazardous solar energetic particles are energized, Solar Probe+ will make a fundamental contribution to our ability to characterize and forecast the radiation environment in which future space explorers will work and live.

Source record↗
NASA NTRS2013

Alabama Ground Operations during the Deep Convective Clouds and Chemistry Experiment

The Deep Convective Clouds and Chemistry (DC3) field campaign investigates the impact of deep, midlatitude convective clouds, including their dynamical, physical and lighting processes, on upper tropospheric composition and chemistry. DC3 science operations took place from 14 May to 30 June 2012. The DC3 field campaign utilized instrumented aircraft and ground ]based observations. The NCAR Gulfstream ]V (GV) observed a variety of gas ]phase species, radiation and cloud particle characteristics in the high ]altitude outflow of storms while the NASA DC ]8 characterized the convective inflow. Groundbased radar networks were used to document the kinematic and microphysical characteristics of storms. In order to study the impact of lightning on convective outflow composition, VHF ]based lightning mapping arrays (LMAs) provided detailed three ]dimensional measurements of flashes. Mobile soundings were utilized to characterize the meteorological environment of the convection. Radar, sounding and lightning observations were also used in real ]time to provide forecasting and mission guidance to the aircraft operations. Combined aircraft and ground ]based observations were conducted at three locations, 1) northeastern Colorado, 2) Oklahoma/Texas and 3) northern Alabama, to study different modes of deep convection in a variety of meteorological and chemical environments. The objective of this paper is to summarize the Alabama ground operations and provide a preliminary assessment of the ground ]based observations collected over northern Alabama during DC3. The multi ] Doppler, dual ]polarization radar network consisted of the UAHuntsville Advanced Radar for Meteorological and Operational Research (ARMOR), the UAHuntsville Mobile Alabama X ]band (MAX) radar and the Hytop (KHTX) Weather Surveillance Radar 88 Doppler (WSR ]88D). Lightning frequency and structure were observed in near real ]time by the NASA MSFC Northern Alabama LMA (NALMA). Pre ]storm and inflow proximity soundings were obtained with the UAHuntsville mobile sounding unit and the Redstone Arsenal (QAG) morning sounding.

Carey, Lawrence↗
NASA NTRS2013

Advanced Colloids Experiment (ACE) Science Overview

The Advanced Colloids Experiment is being conducted on the International Space Station (ISS) using the Light Microscopy Module (LMM) in the Fluids Integrated Rack (FIR). Work to date will be discussed and future plans and opportunities will be highlighted. The LMM is a microscope facility designed to allow scientists to process, manipulate, and characterize colloidal samples in micro-gravity where the absence of gravitational settling and particle jamming enables scientists to study such things as:a.The role that disordered and ordered-packing of spheres play in the phase diagram and equation of state of hard sphere systems,b.crystal nucleation and growth, growth instabilities, and the glass transition, c.gelation and phase separation of colloid polymer mixtures,d.crystallization of colloidal binary alloys,e.competition between crystallization and phase separation,f.effects of anisotropy and specific interactions on packing, aggregation, frustration and crystallization,g.effects of specific reversible and irreversible interactions mediated in the first case by hybridization of complementary DNA strands attached to separate colloidal particles,h.Lock and key interactions between colloids with dimples and spheres which match the size and shape of the dimples,i.finding the phase diagrams of isotropic and interacting particles,j.new techniques for complex self-assembly including scenarios for self-replication, k.critical Casimir forces,l.biology (real and model systems) in microgravity,m.etc. By adding additional microscopy capabilities to the existing LMM, NASA will increase the tools available for scientists that fly experiments on the ISS enabling scientists to observe directly what is happening at the particle level. Presently, theories are needed to bridge the gap between what is being observed (at a macroscopic level when photographing samples) with what is happening at a particle (or microscopic) level. What is happening at a microscopic level will be directly accessible with the availability of the Light Microscopy Module (LMM) on ISS. To meet these goals, the ACE experiment is being built-up in stages, with the availability of confocal microscopy being the ultimate objective. Supported by NASAs Physical Sciences Research Program, ESAESTEC, and the authors respective governments.

Microgravity Biology Research↗
NASA NTRS2017

Synthesis of Ti Oxides at Reducing Conditions: Implications for Beamline Standards and Cosmochemistry

These initial experiments demonstrate the great potential for synthesizing customized compounds for use as standards, or in buffering experiments at reducing conditions. We are also investigating Cr and V oxides, as well as compounds containing these elements such as FeV2O4 and FeCr2O4. Oxygen fugacity exerts a major control on mineral major element chemistry and elemental valence of minerals in any plane-tary compositional system [1]. For Earth, Fe is multivalent ranging from nearly Fe0 at low fO2 in the deep mantle to Fe2+ to Fe3+ at high low fO2. For solar nebular and meteoritic materials fO2 ranges from near IW to ~10 log fO2 units below the IW buffer [1]. Phases in CAIs, for example, contain no Fe2+, but may contain Ti4+, Ti3+, or Ti2+, and Cr3+ or Cr2+, and V3+ or V2+ [1,2,3]. De-tailed study of inclusions may reveal important differences in fO2 thus reflecting different environments in the solar nebula [4]. XANES, FEG-SEM, and TEM can reveal such variations in micro and nano samples such as Stardust and cosmic dust particles [5], but successful application to reduced conditions depends upon the availability of well characterized standards. Acquiring appropriate standards for reduced phases that contain Ti3+ or Ti2+, Cr3+ or Cr2+, and V3+ or V2+ can be a challenge. Here we report our preliminary results at synthesizing reduced Ti bearing standards, and focus on the preliminary characterization.

Righter, K.↗
NASA NTRSDate not supplied

Impact of Air Traffic Reductions during the COVID-19 Pandemic on Aircraft-induced Clouds and their Radiative Effects

Air travel restrictions due to the novel coronavirus 2019 (COVID-19) pandemic drastically reduced air travel internationally during the spring of 2020. Such an extraordinary disruption of air traffic may have a profound effect on contrail formation that could allow for better quantification and scientific understanding of the radiative impacts of aviation-induced clouds on climate. This investigation synergizes MODIS, CrIS, and GOES-16 satellite analyses with weather analyses, including those from GEOS and MERRA, to compare contrail formation conditions and radiative forcings of linear contrails and thin cirrus detected over the contiguous United States (CONUS) and the North Atlantic for the 2020 air traffic slowdown period with parallel analyses conducted for a baseline period from a previous year with normal air traffic. A consistent analysis system for contrail detection and cloud property retrievals (e.g. optical depth, particle size, and altitude) from satellites, coupled with radiative transfer modeling are applied to characterize and contrast contrail cirrus properties and radiative effects estimated during the pandemic and baseline periods. Temperature and humidity profiles from numerical weather models and hyperspectral infrared measurements are used to estimate the contrail formation potential (CFP) over the study areas in order to help choose the most appropriate baseline period and to account for potential impacts of differences in meteorology on contrail formation and coverage. This study, using NASA satellite data and other assets, is expected to improve our understanding of the relationship between air traffic, contrail cirrus coverage and related impacts in order to better quantify the need for contrail formation mitigation strategies that could reduce aviation effects on climate.

William L Smith↗
NASA NTRS2019

Near-Sun Observations of an F-Corona Decrease and K-Corona Fine Structures

Remote observations of the solar photospheric light scattered by electrons (K-corona) and dust (F-corona/Zodiacal light) have been made from the ground during eclipses and from space at 1 AU and as close as 0.3 AU. Previous observations of dust scattering have not confirmed the existence of a theoretically-predicted dust free zone near the Sun. The transient nature of the corona has been well characterized for large events, but questions still remain (e.g. initiation, production of solar energetic particles) and for small events even the structure is uncertain. Here we report on imaging the solar corona, from the Parker Solar Probe spacecraft, during the first two perihelion passes (0.16-0.25 AU), each of ten days duration. The view from these distances is qualitatively similar to the historical view, but there are some significant differences in the details. We have uncovered at short elongations a decrease in the intensity of the F-coronal intensity, which is suggestive of the long-sought dust free zone. Also we have resolved the plasma structure of very small eruptions, which are being frequently ejected from the Sun. They take two forms - the commonly observed magnetic flux ropes or the predicted, but not yet observed, magnetic islands arising from the tearing mode instability in the current sheet. Our observations of the coronal streamer evolution confirm the large-scale topology of the solar corona, but they also reveal that, as recently predicted, streamers are composed of yet smaller sub-streamers channeling continual density fluctuations at all visible scales.

Astronomy and astrophysics↗
NASA NTRSDate not supplied

Low Energy Ionizing Radiation and Plasma Contributions to Radiation Dose in Materials at Sun-Earth Lagrange Points

- High energy radiation environments responsible for radiation damage to thick materials are well characterized and modeled: - Galactic cosmic rays — Badhwar-O’Neil 2020, CREME96, Nymmik - Solar particle events — Emission of Solar Protons, SAPPHIRE, JPL, King 1972 - Trapped radiation belts — AE8/AP8, AE9/AP9/IRENE - Low energy radiation environments responsible for radiation damage to thin materials relevant to Lagrange points and interplanetary missions have not been treated as comprehensively to date: - Solar wind - Magnetosheath - Magnetotail - Concern to spacecraft design and operations is radiation damage to surfaces and thin materials with mission critical applications on exterior of spacecraft - Applications: thermal control coatings, sunshields, multilayer insulation, optical thin film coatings, solar sails, thermo-optical properties of space exposed materials - Damage processes: radiation degradation (total dose), light ion sputtering, proton blistering of soft metals, modification of optical properties (α/ε), modification of charging properties (SEY, surface conductivity)

Joseph I. Minow↗
DOE OSTI2017

Vitrification of Sellafield Wastes with High Metallic Magnesium Alloy Content - 17495

The Sellafield nuclear complex, located in northwest England, is the largest such site in the United Kingdom. Sellafield Limited, which is the operating contractor for the Nuclear Decommissioning Authority, is evaluating thermal treatment technologies for a potential future facility to process a variety of Intermediate Level Waste sludges and slurries accumulated from historical site operations. In support of that effort, Atkins and the Vitreous State Laboratory (VSL) of The Catholic University of America conducted studies to evaluate the feasibility and implications of installing a joule-heated ceramic melter (JHCM) vitrification system to process a variety of sludge and slurry radioactive wastes at the Sellafield site. These sludges have the potential to contain a significant proportion of reactive metals in localized regions. The metallic fraction derives from unreacted Magnox spent fuel cladding. Thus, an important objective of this work was to investigate the performance of JHCM technology for the treatment of streams with localized regions of high reactive metal contents. The present work was focused on Site Ion Exchange Effluent Plant (SIXEP) Magnox sludges, investigated previously. Suitable waste simulants were developed for the SIXEP Magnox sludge waste stream, which included surrogates for all important radionuclides. High waste-loading, fully compliant glass formulations were designed using a combination of previous experience, extensive waste glass data bases, and small-scale crucible melts. Glasses from the test melts were characterized for properties that are important for processability and product quality. The most viable compositions were then selected for small-scale melter trials to collect information on processing rates and behavior, off-gas and secondary waste compositions, and overall system mass balance. These data were used to support the technology evaluation, which considered such factors as minimization of inactive additions, waste volume reduction, retention of radionuclides, minimization of secondary wastes, and overall process efficiency and effectiveness. The data were also used to develop sizing estimates for the full-scale facility and to estimate treatment durations under various treatment scenarios. A series of tests was then performed with partial replacement of the magnesium hydroxide with a metallic magnesium alloy that is close in composition to Magnox alloy. A commercially available magnesium alloy, Elecktron AZ31B, which has a nominal magnesium content of 95.7%, was used for this purpose. The testing was performed on a DuraMelter 10 (DM10) JHCM system to characterize the melter off-gas, glass product, and the effects of magnesium alloy particle size on feed processing. Data on processing rate and any processing issues, product glass composition, off-gas composition including hydrogen, and system operating parameters, including flows, temperatures, pressures, etc., were collected and analyzed to evaluate the effects of magnesium alloy on the vitrification process. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2016

Synthesis and characterization of Sn-doped hematite as visible light photocatalyst

Highlights: • Sn-doped hematite nanoparticles are prepared by SCS in one step. • The Sn doping have the ability to inhibit particle growth of hematite. • Sn can enhance visible light harvesting and e{sup −}/h{sup +} separation. • Sn-doped hematite degrades MB under visible light effectively. • The products with 5 mol% Sn have the highest photocatalytic activity. - Abstract: Sn-doped hematite nanoparticles are prepared by solution combustion synthesis. The products are characterized with various analytical and spectroscopic techniques to determine their structural, morphological, light absorption and photocatalytic properties. The results reveal that all the samples consist of nanocrystalline hematite with mesoporous structures, and Sn has the ability to inhibit the growth of hematite particle. Compared to pure hematite, the doped hematite samples with appropriate amount of Sn show better activities for degradation of methylene blue under visible light irradiation. The highest activity is observed for 5% Sn doped hematite and this product has long-term stability and no selectivity for dye degradation. The enhanced performance of 5% Sn doped hematite is ascribed to the smaller particle size, increased ability to absorb in visible light, efficient charge separation as well as improved e{sup −} transfer associated with the effects of appropriate amount of Sn doped sample.

36 MATERIALS SCIENCE↗

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