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Definition of Mutually Optimum NDI and Proof Test Criteria for 2219 Aluminum Pressure Vessels. Volume 2: Optimization and Fracture Studies

Certain behavioral aspects associated with fracture and crack extension that cannot be studied using other techniques were evaluated with the ultrasonic method. Characterization of collimated beam techniques showed that significant beam width reduction could be accomplished. Techniques for collimation are given. The crack-opening displacement-gage correction-factor study showed that displacement resulting from crack opening and that from plasticity could be readily differentiated. Crack closure studies using both ultrasonic and crack-opening displacement measurements showed an opening and closing behavior associated with load-unload curves. The results of this work were in general agreement with the closure concepts of Elber. Ultrasonic measurements used to study the nature of flaw extension characteristics associated with failure of the ligament between the flaw front and back surface showed that penetration could occur by an abrupt fracturing after subcritical growth or by continuous growth.

Schwartzberg, F. R.↗

A new basis for the determination of fracture toughness

A study is presented which shows that the growth of the plastic zone and the constraint in a compact tension specimen depends significantly on specimen width. The analysis permits the estimation of the contribution of the growth of plastic zone to the deviation from linearity. The contribution of the crack growth to the deviation from linearity is evaluated from the analysis of a typical R-curve data. A combination of these two analyses enables one to define a very simple procedure for the determination of fracture toughness. The fracture toughness is defined as the stress intensity value at which the crack extension starts. The good agreement between analytical results and experimental KQ and KIC values determined over a wide range of thicknesses, widths, and materials justifies the proposed procedures. The KIC determined according to this procedure is independent of specimen width and such a procedure enhances the range of applicability of the K concept to a wider combination of configurations and materials.

Banerjee, S.↗

The fracture behavior of graphite/epoxy laminates

The results of uniaxial tensile tests conducted on a variety of graphite/epoxy laminates containing narrow rectangular slits and square or circular holes with various aspect ratios are discussed. The techniques used to study stable-crack or damage-zone growth - namely, birefringence coatings, COD gages, and microscopic observations are discussed. Initial and final-fracture modes are discussed as well as the effect of notch size and shape and laminate type on the fracture process. Characteristic lengths are calculated using the point, average and inherent flaw theories and comparisons with observations are discussed. Further, the effect of flaw geometry on stress states and deformations is assessed.

Yeow, Y. T.↗

A fracture specimen for high-temperature testing

A wedge-loaded tapered DCB specimen is proposed for fracture toughness and stable crack growth measurements of ceramic materials at elevated temperatures. The specimen is wedge-loaded by a compression pin seated in the starter notch. By appropriate selection of the specimen's taper and starter notch angle, the stress intensity factor is maintained relatively constant through 50 percent of the test section. Room temperature fracture toughness testings of commercial grade polycrystalline alumina specimens indicate that the crack will run straight for approximately 50 percent of the length of the test section without side grooving. A moderate 10 percent side grooving was sufficient to maintain straight crack extension throughout the entire specimen length.

Kobayashi, A. S.↗

Friction and fracture of single-crystal silicon carbide in contact with itself and titanium

An investigation was conducted to examine the friction properties and mechanical behavior of single-crystal silicon carbide (0001) surface sliding against itself and against polycrystalline titanium. The results indicate hexagon-shaped pits of silicon carbide and the formation of platelet hexagon-shaped wear debris of silicon carbide due to cleavages of both prismatic and basal planes as a result of silicon carbide sliding against itself. The fracturing of silicon carbide also occurs near the adhesive bond to titanium. The wear debris produced by brittle fracture plows the titanium and transfers to it. Further, the silicon carbide wear debris, which adhered and transferred to titanium, plows the silicon carbide surface and transfers back to it

Miyoshi, K.↗

Reusable solid rocket motor case - Optimum probabilistic fracture control

A methodology for the reliability analysis of a reusable solid rocket motor case is discussed in this paper. The analysis is based on probabilistic fracture mechanics and probability distribution for initial flaw sizes. The developed reliability analysis can be used to select the structural design variables of the solid rocket motor case on the basis of minimum expected cost and specified reliability bounds during the projected design life of the case. Effects on failure prevention plans such as nondestructive inspection and the material erosion between missions can also be considered in the developed procedure for selection of design variables. The reliability-based procedure that has been discussed in this paper can easily be modified to consider other similar structures of reusable space vehicle systems with different fracture control plans.

Hanagud, S.↗

Comparison tests and experimental compliance calibration of the proposed standard round compact plane strain fracture toughness specimen

Standard round specimen fracture test results compared satisfactorily with results from standard rectangular compact specimens machined from the same material. The location of the loading pin holes was found to provide adequate strength in the load bearing region for plane strain fracture toughness testing. Excellent agreement was found between the stress intensity coefficient values obtained from compliance measurements and the analytic solution proposed for inclusion in the standard test method. Load displacement measurements were made using long armed displacement gages and hollow loading cylinders. Gage points registered on the loading hole surfaces through small holes in the walls of the loading cylinders.

Fisher, D. M.↗

A relation between semiempirical fracture analyses and R-curves

The relations between several semiempirical fracture analyses (SEFA) and the R-curve concept of fracture mechanics are examined and the conditions for equivalence between a SEFA and an R-curve are derived. A hypothetical material is employed to study the relation analytically. Equivalent R-curves are developed for several real materials using data from the literature. For each SEFA there is an equivalent R-curve whose magnitude and shape are determined by the SEFA formulation and its empirical parameters. If the R-curve is indeed unique, then the various empirical parameters cannot be constant, and vice versa. However, for one SEFA the differences are small enough that they may be within the range of normal data scatter for real materials.

Orange, T. W.↗

Increased fracture toughness of graphite-epoxy composites through intermittent interlaminar bonding

Intermittent interlaminar bonding, which can lead to a large increase in the fracture surface area, was achieved through the introduction of thin perforated Mylar between the layers of a multi-layer continuous-filament graphite-epoxy composite. For the best optimum condition included in this study, fracture toughness was increased from about 100 kJ/sq m for untreated specimens to an average of about 500 kJ/sq m, while tensile strength dropped from 500 MPa to 400 MPa, and elastic modulus remained the same at about 75 GPa. An approximate analysis is presented to explain the observed improvement in toughness.

Felbeck, D. K.↗

A single fracture toughness parameter for fibrous composite laminates

A general fracture toughness parameter Qc was previously derived and verified to be a material constant, independent of layup, for centrally cracked boron aluminum composite specimens. The specimens were made with various proportions of 0 and + or - 45 degree plies. A limited amount of data indicated that the ratio Qc/epsilon tuf' where epsilon tuf is the ultimate tensile strain of the fibers, might be a constant for all composite laminates, regardless of material and layup. In that case, a single value of Qc/epsilon tuf could be used to predict the fracture toughness of all fibrous composite laminates from only the elastic constants and epsilon tuf. Values of Qc/epsilon tuf were calculated for centrally cracked specimens made from graphite/polyimide, graphite/epoxy, E glass/epoxy, boron/epoxy, and S glass graphite/epoxy materials with numerous layups. Within ordinary scatter, the data indicate that Qc/epsilon tuf is a constant for all laminates that did not split extensively at the crack tips or have other deviate failure modes.

Poe, C. C., Jr.↗

Fundamental aspects in the quantitative ultrasonic determination of fracture toughness: General equations

The problem of establishing a theoretical groundwork for experimentally-found correlations between ultrasonic and fracture toughness factors in polycrystalline metals is discussed. It is noted that the link between these material properties and ultrasonic factors are the microstructural parameters that interact with stress wave propagation during deformation and fracture. The dynamic response of material inhomogeneities and the strains and displacements they undergo under incident stress waves are considered. Dynamic strains and displacements inside and outside scatterers are treated. The underlying approach, the formulation and governing equations for the eigenstrains, and the determination of the energy due to the presence of inhomogeneities are presented. The stress wave interaction problem is presented in terms of the dynamic eigenstrain concept.

Fu, L. S.↗

On the equivalence between semiempirical fracture analyses and R-curves

The relationship between the R-curves and semiempirical fracture analyses (SEFA) is investigated theoretically using a hypothetical material. Equivalent R-curves (ERC) are developed for real materials using data from the literature. It is shown that for each SEFA there is an ERC whose magnitude and shape are determined by the SEFA formulation and its empirical parameters. The ERC is equivalent in that it predicts exactly the same relationship between the fracture stress and the initial crack length (residual strength) as the SEFA. If the effective R-curve is unique, then the various empirical parameters cannot be constant, and vice versa. However, for one of the SEFA examined, Newman's SEFA, parameter variations are small enough to be within the range of normal data scatter for real materials.

Orange, T. W.↗

Fracture toughness of brittle materials determined with chevron notch specimens

Short bar, short rod, and four-point-bend chevron-notch specimens were used to determine the plane strain fracture toughness of hot-pressed silicon nitride and sintered aluminum oxide brittle ceramics. The unique advantages of this specimen type are: (1) the production of a sharp natural crack during the early stage of test loading, so that no precracking is required, and (2) the load passes through a maximum at a constant, material-independent crack length-to-width ratio for a specific geometry, so that no post-test crack measurement is required. The plane strain fracture toughness is proportional to the maximum test load and functions of the specimen geometry and elastic compliance. Although results obtained for silicon nitride are in good mutual agreement and relatively free of geometry and size effects, aluminum oxide results were affected in both these respects by the rising crack growth resistance curve of the material.

Shannon, J. L., Jr.↗

Thermal stress fracture in elastic-brittle materials

The reported investigation shows that the assessment of the possibility of the thermal fracture of brittle materials depends upon an accurate evaluation of the thermal stresses and the determination of the resulting stress intensity factors. The stress intensity factors can be calculated in a variety of ways ranging from the very precise to approximate, but only for a limited number of geometries. The main difficulty is related to the determination of the thermal stress field because of its unusual character and its dependence upon boundary conditions at points far from the region of thermal activity. Examination of a number of examples suggests that the best visualization of the thermal stresses and any associated fracture can be made by considering the problem to be the combination of thermal and isothermal problems or by considering that the prime effect of the temperature is in the generation of thermal strains and that the thermal stresses are simply the result of the region trying to accommodate these strains.

Emery, A. F.↗

Lunar floor-fractured craters - Evidence for viscous relaxation of crater topography

Viscous relaxation is evaluated quantitatively as a possible mechanism to account for the observed topographical modification of floor-fractured lunar craters. On the basis of a model of the moon as a viscous material of uniform Newtonian viscosity, the ultimate topographic profiles of fresh craters predicted taking into account viscous relaxation effects are compared with the observed profiles of floor-fractured craters of similar diameter. It is found that for a number of crater pairs, the agreement of the observations with the predictions of the simple viscous relaxation model is good, suggesting that isostatic adjustment of craters in areas of anomalously high temperatures at shallow depth may be a more important source of deformation than previously realized.

Hall, J. L.↗

Work of fracture in aluminum metal-matrix composites

Mechanical tests were conducted on B/Al composites and, for comparison, FP-Al2O3/Al composites in the as-fabricated condition and following high-temperature isothermal exposure or thermal cycling. In B/Al (1100), isothermal exposure at 773 K for 125 hr reduced toughness, measured by the work of fracture, from 76 to 10 kJ/sq m, and a similar reduction was observed after equivalent thermal cycling. In B/Al (6061), the same isothermal exposure reduced toughness from 44.5 to 8 kJ/sq m, but the effect of thermal cycling was less detrimental. In FP-Al2O3/Al, the work of fracture was insensitive to either type of treatment. Experimental results are interpreted in terms of matrix softening, interface properties, and fiber notch sensitivity.

Skinner, A.↗

Geoid height-age relation from Seasat altimeter profiles across the Mendocino Fracture Zone

Twenty-eight Seasat altimeter profiles crossing the Mendocino Fracture Zone are used together with seafloor ages determined from magnetic lineations to estimate the change in oceanic geoid height with age, between ages of 15 and 135 m.y. An unbiased estimate of the overall geoid offset along each profile is determined from a least-squares fit of the along-track derivative of the geoid to the geoid slope predicted from a simple two-layer gravitational edge effect model. Uncertainties based upon the statistical properties of each profile are also determined. A geoid slope-age relation is constructed by normalizing the geoid offsets and uncertainties by the age offsets. The results are in agreement with geoid slope-age relations determined from symmetrically spreading ridges (Sandwell and Schubert, 1980). However, the fracture zone estimates have smaller uncertainties and show less scatter. A comparison of these results with the geoid slope-age prediction of the boundary layer cooling model shows that the thermal structure begins to deviate from this model at an early age (20-40 m.y.). A plate cooling model with a thickness of 125 km is most compatible with the geoid slope-age estimates, although significant deviations occur; these may indicate that the lithospheric thermal structure is not entirely age dependent.

Sandwell, D. T.↗

Fracture of directionally solidified multicrystalline silicon

Fracture toughness data is given for multicrystalline silicon which has been prepared by directional solidification. Results indicated a plane-strain fracture toughness of 0.8 to 0.87 MN/m to the 3/2 power, which is consistent with data for single-crystal silicon.

Chen, C. P.↗

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