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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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DOE OSTI2019

Fortifying Environmental Compliance Strategies at Hanford - 19541

At the Hanford Site, located near Richland, Washington, the Department of Energy is cleaning up legacy radioactive and mixed-waste generated from the Manhattan Project in the 1940's. A major component of cleaning up the waste is maintaining compliance with federal and state environmental regulations. Environmental compliance is also determined through permits, agreements, and consent orders issued by regulating agencies such as the Washington State Department of Health: Office of Radiation Protection, Washington State Department of Ecology Nuclear Waste Program, and the Environmental Protection Agency. Maintaining compliance at Hanford reduces environmental impacts and addresses violations, or non-compliances. The following strategies improve compliance and support the avoidance of enforcement actions. At Hanford, regulatory agency environmental enforcement actions, and their corrective actions, are tracked to completion using databases maintained by inspection subject matter experts. The databases are used to provide the Department of Energy and contractor management with up-to-date status of regulatory agency activity and the required corrective actions. Trending enforcement actions helps target compliance vulnerabilities. Findings and corrective actions that are entered into the databases are then trended by date, location, responsible contractor, agency, and type of compliance issue. The ability to review previous non-compliances in certain locations of the Site, or by general alleged violation, provides the project's environmental contacts with information on what types of issues to look for on pre-inspection walk downs. Finding non-compliances during pre-inspection walk downs allows the contractor to correct the issue and avoid potential fines from regulating agencies. The walk downs are conducted by environmental specialists and project personnel looking for issues that may be viewed as a compliance problem. Using agency checklists and previous inspection correspondence can help to provide valuable information during pre-inspection activities. Training regulatory agency inspectors on Site security requirements, cultural and ecological standards, and inspection protocols allows for increased efficiency and reduces potential miscommunication between regulatory agencies and the regulated contractors. The training also allows the contractors to give the regulating agencies the up-to-date policies and procedures that will be addressed during the inspection. Hanford has pre-identified inspection coordinators within each contractor to assist in coordinating with Department of Energy personnel, projects, and management prior to the inspections. These inspection coordinators notify affected management, accommodate and escort the regulators to locations they ask to inspect, set up requested interviews, and gather requested information that will need to be cleared for public release. These practices make for positive experiences and interactions with the regulating agency personnel and help reduce and eliminate environmental non-compliances, findings, violations, and fines. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

NASA NTRS2012

Environmentally Friendly Corrosion Preventative Compounds

The objective of the Ground Systems Development and Operations Program Environmentally Friendly Corrosion Protective Coatings and Corrosion Preventive Compounds (CPCs) project is to identify, test, and develop qualification criteria for the use of environmentally friendly corrosion protective coatings and CPCs for flight hardware and ground support equipment. This document is the Final Report for Phase I evaluations, which included physical property, corrosion resistance, and NASA spaceport environment compatibility testing and analysis of fifteen CPC types. The CPCs consisted of ten different oily film CPCs and five different wax or grease CPC types. Physical property testing encompassed measuring various properties of the bulk CPCs, while corrosion resistance testing directly measured the ability of each CPC material to protect various metals against corrosion. The NASA spaceport environment compatibility testing included common tests required by NASA-STD-6001, "Flammability, Odor, Offgassing, and Compatibility Requirements and Test Procedures for Materials in Environments that Support Combustion". At the end of Phase I, CPC materials were down-selected for inclusion in the next test phases. This final report includes all data and analysis of results obtained by following the experimental test plan that was developed as part of the project. Highlights of the results are summarized by test criteria type.

Preventative Compounds↗

DOE OSTI2017

2016 Results for Avian Monitoring at the TA-36 Minie Site, TA-39 Point 6, and TA-16 Burn Ground at Los Alamos National Laboratory

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2018

2017 Results for Avian Monitoring at the TA-36 Minie Site, TA-39 Point 6, and TA-16 Burn Ground at Los Alamos National Laboratory

Los Alamos National Security, LLC (LANS) biologists in the Environmental Compliance and Protection Division at Los Alamos National Laboratory (LANL) initiated a multi-year program in 2013 to monitor avifauna (birds) at two open detonation sites and one open burn site on LANL property. Monitoring results from these efforts were compared among years to monitor trends. The objectives of this study were to determine whether LANL operations impact bird species richness, diversity, abundance, or composition. Additionally, nesting success of secondary-cavity nesting birds was examined using nestboxes. LANS biologists completed the fifth year of this effort in 2017. The overall results from 2017 continue to indicate that operations are not negatively affecting bird populations; however, we are seeing some species turnover through time and that will continue to be monitored. Three bird point count surveys were completed at each of the treatment sites at the Technical Area (TA) 36 Minie site, the TA-39 point 6, and the TA-16 burn ground between May and July 2017. A total of 785 birds representing 59 species were recorded at the treatment sites. Three bird point count surveys were also completed at each of the control sites between May and July 2017. Occupancy and nest success data from nestboxes at treatment sites were compared with the overall avian nestbox monitoring network. Species richness and diversity at the treatment sites were not statistically different than their associated controls. Avian abundance showed more variability but treatment and controls were trending together year to year. Species composition seems to indicate some species turnover in the habitat types but very little difference between treatment and control sites.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2015

Nanopillar-based enhanced-fluorescence detection of sur-face-immobilized beryllium.

The unique properties associated with beryllium metal ensures the continued use in many industries despite the documented health and environmental risks. While engineered safeguards and personal protective equipment can reduce risks associated with working with the metal, it has been mandated by the Environmental Protection Agency (EPA) and Occupational Safety and Health Administration (OSHA) that the workplace air and surfaces must be monitored for toxic levels. While many methods have been developed to monitor levels down to the low μg/m 3 , the complexity and expense of these methods have driven the investigation into alternate methodologies. Herein, we use a combination of the previously developed fluorescence Be(II) ion detection reagent, 10-hydroxybenzo[h]quinoline (HBQ), with an optical field enhanced silicon nanopillar array, creating a new surface immobilized (si-HBQ) platform. The si-HBQ platform allows the positive control of the reagent for demonstrated reusability and a pillar diameter based tunable enhancement. Furthermore, native silicon nanopillars are overcoated with thin layers of porous silicon oxide to develop an analytical platform capable of a 0.0006 μg/L limit of detection (LOD) using sub-μL sample volumes. Additionally, we demonstrate a method to multiplex the introduction of the sample to the platform, with minimal 5.2% relative standard deviation (RSD) at 0.1 μg/L, to accommodate the potentially large number of samples needed to maintain industrial compliance. The minimal sample and reagent volumes and lack of complex and highly specific instrumentation, as well as positive control and reusability of traditionally consumable reagents, create a platform that is both accessible and economically advantageous.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1972

Evaluation of coated columbian alloy heat shields for space shuttle thermal protection system application. Volume 1: Phase 1 - Environmental criteria and material characterization, October 1970 - March 1972

The studies presented are directed toward establishing criteria for a niobium alloy thermal protection system for the space shuttle. Evaluation of three niobium alloys and two silicon coatings for heat shield configurations culminated in the selection of two coating/substrate combinations for environmental criteria and material characterization tests. Specimens were exposed to boost and reentry temperatures, pressure, and loads simulating a space shuttle orbiter flight profile.

Black, W. E.↗

NASA NTRS2002

Thermal Cyclic Behavior of Thermal and Environmental Barrier Coatings Investigated Under High-Heat-Flux Conditions

Environmental barrier coatings (EBC's) have been developed to protect silicon-carbide- (SiC) based ceramic components in gas turbine engines from high-temperature environmental attack. With continuously increasing demands for significantly higher engine operating temperature, future EBC systems must be designed for both thermal and environmental protection of the engine components in combustion gases. In particular, the thermal barrier functions of EBC's become a necessity for reducing the engine-component thermal loads and chemical reaction rates, thus maintaining the required mechanical properties and durability of these components. Advances in the development of thermal and environmental barrier coatings (TBC's and EBC's, respectively) will directly impact the successful use of ceramic components in advanced engines. To develop high-performance coating systems, researchers must establish advanced test approaches. In this study, a laser high-heat-flux technique was employed to investigate the thermal cyclic behavior of TBC's and EBC's on SiC-reinforced SiC ceramic matrix composite substrates (SiC/SiC) under high thermal gradient and thermal cycling conditions. Because the laser heat flux test approach can monitor the coating's real-time thermal conductivity variations at high temperature, the coating thermal insulation performance, sintering, and delamination can all be obtained during thermal cycling tests. Plasma-sprayed yttria-stabilized zirconia (ZrO2-8 wt% Y2O3) thermal barrier and barium strontium aluminosilicate-based environmental barrier coatings (BSAS/BSAS+mullite/Si) on SiC/SiC ceramic matrix composites were investigated in this study. These coatings were laser tested in air under thermal gradients (the surface and interface temperatures were approximately 1482 and 1300 C, respectively). Some coating specimens were also subject to alternating furnace cycling (in a 90-percent water vapor environment at 1300 C) and laser thermal gradient cycling tests (in air), to investigate the water vapor effect. All cyclic tests were conducted using a 60-min hot-time temperature.

Zhu, Dongming↗

DOE OSTI2015

Hanford site asbestos management lessons learned - 15183

The U.S. Department of Energy (DOE) is responsible for the environmental cleanup of the Hanford Site central plateau. As part of this responsibility, DOE contractors conduct deactivation, decommissioning, decontamination, and demolition (D4) of retired/inactive facilities, including very large chemical processing facilities. To date, DOE contractors have demolished hundreds of facilities, reducing baseline site maintenance costs and reducing the environmental threats and hazards that the degrading buildings present. Many of these Hanford facilities include asbestos-containing materials (as well as other hazardous components), which must be managed in compliance with applicable regulations and standards. In most cases, the facilities are demolished as Comprehensive Environmental Response, Compensation and Liability Act (CERCLA) removal or remedial actions. In an effort to streamline cleanup operations and to utilize site cleanup funding more efficiently, while still being protective of personnel and the environment, agreements were reached between the US Environmental Protection Agency (EPA) Hanford Project Office, the Washington Department of Ecology (Ecology), the Benton Clean Air Agency (BCAA) and the US Department of Energy Richland Operations Office (DOE-RL) on approaches to be utilized for demolition. One of these approaches would involve leaving cement asbestos board siding (e.g. transite), an EPA National Emissions Standards for Hazardous Air Pollutants (NESHAP) Category II non-friable asbestos-containing material, in place during demolition using heavy equipment, employing a set of controls that would maintain protection of personnel and the environment. This agreement was documented in a number of formal communications, including Notices of Intent issued as required by the asbestos NESHAP regulation, letters between the various agencies, CERCLA work plans, and the approved contractor baselines. A large number of buildings were demolished with transite siding in place, using the agreed upon controls and approaches. Personnel breathing zone and work area perimeter monitoring verified that the controls employed were protective in that there were no exceedances of permissible exposure limits during or after the demolition operations. EPA later reconsidered their previous concurrence with demolishing transite materials in place and issued a joint letter with Ecology revoking concurrence on any of the aforementioned CERCLA decision documents and associated work plans. DOE and their contractors took action to comply with the approach to demolition preferred by EPA for future demolitions, and initiated a series of actions to modify asbestos management practices in their operations accordingly. This paper will discuss both the actions taken to address EPA concerns with sites where transite materials were left in place for demolition and actions taken to ensure that the central plateau D4 program complies with the 40 CFR 61 Subpart M, National Emission Standard for Asbestos, (Asbestos NESHAP) methods for asbestos management. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2016

Environmental levels of Zn do not protect embryos from Cu toxicity in three species of amphibians

Not Available

Weir, Scott M.↗

DOE OSTI2016

Dose Assessment of LANL-Derived Residual Radionuclides in Soils within C Tracts (C-2, C-3, and C-4) for Land Transfer Decisions

In 2015, soil sampling for radiological materials was conducted within Tract A-16-b specifically for land conveyance decisions. Measurements of radionuclides in soil samples were evaluated against a recreational use scenario, and all measurements were below screening action levels for each radionuclide. The total estimated dose was less than 1 mrem/y (< 10 μSv/y) for a hypothetical recreational user (compared to an action level of 15 mrem/y (150 μSv/y). Dose estimates were based on the 95% upper confidence limits for radionuclide concentrations within the tracts. Additionally, dose estimates less than 3 mrem/y are considered to be As Low As Reasonably Achievable, so no follow-up analysis was conducted. Release of this property is consistent with the requirements of DOE Order 458.1 and Los Alamos National Laboratory Policy 412.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2015

LANL Environmental ALARA Program Status Report for CY 2014

Los Alamos National Laboratory is committed to ensuring that radiation exposures of members of the public and the environment from LANL operations, past and present, are as low as reasonably achievable (ALARA). A Finding (RL.2-F-1) and Observation (RL.2-0-1) in the NNSA/ LASO report, September 2007, Release of Property (Land) Containing Residual Radioactive Material Self-Assessment Report, indicated that LANL had no policy or documented process in place for the release of property containing residual radioactive material. In response, LANL developed PD410, Los Alamos National Laboratory Environmental ALARA Program. This document was officially published as a Laboratory-wide policy and became effective on August 8, 2008 and was updated in 2011. The document provides program authorities, responsibilities, descriptions, processes, and thresholds for conducting qualitative and quantitative ALARA analyses for prospective and actual radiation exposures to the public and the environment from DOE activities conducted on site.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2016

Sampling and Analysis Plan (SAP) for Assessment of LANL-Derived Residual Radionuclides in Soils within Tract A-16-d for Land Conveyance and Transfer

The A-16-D tract consists of the easternmost portion of DP mesa and is bounded on the North by the canyon bottom of DP canyon and on the South by the edge of the initial slope into Los Alamos Canyon (see Figure 1).

54 ENVIRONMENTAL SCIENCES↗

NASA NTRS2007

Crew Exploration Vehicle Environmental Control and Life Support Fire Protection Approach

As part of preparing for the Crew Exploration Vehicle (CEV), the National Aeronautics and Space Administration (NASA) worked on developing the requirements to manage the fire risk. The new CEV poses unique challenges to current fire protection systems. The size and configuration of the vehicle resembles the Apollo capsule instead of the current Space Shuttle or the International Space Station. The smaller free air volume and fully cold plated avionic bays of the CEV requires a different approach in fire protection than the ones currently utilized. The fire protection approach discussed in this paper incorporates historical lessons learned and fire detection and suppression system design philosophy spanning from Apollo to the International Space Station. Working with NASA fire and materials experts, this approach outlines the best requirements for both the closed out area of the vehicle, such as the avionics bay, and the crew cabin area to address the unique challenges due to the size and configuration of the CEV.

Lewis, John F.↗

NASA NTRS2014

Characterization of Encapsulated Corrosion Inhibitors for Environmentally Friendly Smart Coatings

Research efforts are under way to replace current corrosion inhibitors with more environmentally friendly alternatives. However, problems with corrosion inhibition efficiency, coating compatibility and solubility have hindered the use of many of these materials as simple pigment additives.This paper will present technical details on how the Corrosion Technology Lab at NASAs Kennedy Space Center (KSC) has addressed these issues by encapsulating environmentally friendly inhibitors into organic and inorganic microparticles and microcapsules. The synthetic process for polymer particles was characterized and post-synthesis analysis was performed to determine the interactions between the inhibitors and the encapsulation material. The pH-controlled release of inhibitors from various particle formulations in aqueous base was monitored and compared to both electrochemical and salt immersion accelerated corrosion experiment. Furthermore, synergistic corrosion inhibition effects observed during the corrosion testing of several inhibitor combinations will be presented.

Environmentally Friendly↗

NASA NTRS2016

Weathering the Storm: Unmanned Aircraft Systems in the Maritime, Atmospheric and Polar Environments

Unmanned systems have the potential to efficiently, effectively, economically, and safely bridge critical observation requirements in an environmentally friendly manner. As the United States Atmospheric, Marine and Arctic areas of interest expand and include hard-to-reach regions of the Earth (such as the Arctic and remote oceanic areas) optimizing unmanned capabilities will be needed to advance the United States science, technology and security efforts. Through increased multi-mission and multi-agency operations using improved inter-operable and autonomous unmanned systems, the research and operations communities will better collect environmental intelligence and better protect our country against hazardous weather, environmental, marine and polar hazards. This presentation will examine UAS (Unmanned Aircraft Systems) operations which includes developing a coordinated effort to maximize the efficiency and capabilities of unmanned systems across the federal government and research partners. Numerous intra- and inter-agency operational demonstrations and assessments have been made to verify and validated these UAS observations. The NASA-specific elements will consist of an overview of NASA UAVs (Unmanned Aerial Vehicles) available to science and recent missions.

Atmospheric↗

NASA NTRS2015

Superhydrophobic Post Treatment and Coating Extenders for Improved Asset Sustainability

Launch structures, hardware, and ground support equipment, at NASA's John F. Kennedy Space Center in Florida, are exposed to a highly corrosive natural coastal marine environment. In addition, during launches, rocket exhaust deposition is also highly corrosive. Superhydrophobic coatings are being considered for additional corrosion protection on existing structures to enhance corrosion resistance and add an additional layer of protection against harsh environmental elements. These coatings have come into their own recently, and are now being investigated as corrosion protective coatings due to their water repelling capability. These coatings can be used on existing coatings, newly coated materials, or used on bare substrates. The coatings are not suitable for permanent corrosion protection, but can be used where additional corrosion control is desired or only when temporary corrosion control is needed, such as in hardware sitting on a launch pad for 30-45 days prior to a launch. In this study, superhydrophobic coatings were applied on various coated and uncoated substrates and exposed to the spaceport environment for various times up to 60 days. This paper highlights the current results of the superhydrophobic coatings performance evaluated by X-ray photoelectron spectroscopy, and contact angle measurements.

Coating↗

DOE OSTI2025

A mechanistic study on environment gas in laser powder bed fusion

A variety of protective or reactive environmental gases have recently gained growing attention in laser-based metal additive manufacturing (AM) technologies due to their unique thermophysical properties and the potential improvements they can bring to the build processes. However, much remains unclear regarding the effects of different gas environments on critical phenomena in laser AM, such as rapid cooling, energy coupling, and defect generation. Through simultaneous high-speed synchrotron x-ray imaging and thermal imaging, we identify distinct effects of two environmental gases in laser AM and gained a deeper understanding of the underlying mechanisms. Compared to the commonly used protective gas, argon, it is found that helium has a negligible effect on cooling the part. However, helium can suppress unstable keyholes by decreasing effective energy absorption, thus mitigating keyhole porosity generation and reducing pore size under certain processing conditions. In conclusion, these observations provide guidelines for the strategic use of environmental gases in laser AM to produce parts with improved quality.

36 MATERIALS SCIENCE↗

DOE OSTI2015

Betaine is a positive regulator of mitochondrial respiration

Highlights: • Betaine enhances cytochrome c oxidase activity and mitochondrial respiration. • Betaine increases mitochondrial membrane potential and cellular energy levels. • Betaine’s anti-tumorigenic effect might be due to a reversal of the Warburg effect. - Abstract: Betaine protects cells from environmental stress and serves as a methyl donor in several biochemical pathways. It reduces cardiovascular disease risk and protects liver cells from alcoholic liver damage and nonalcoholic steatohepatitis. Its pretreatment can rescue cells exposed to toxins such as rotenone, chloroform, and LiCl. Furthermore, it has been suggested that betaine can suppress cancer cell growth in vivo and in vitro. Mitochondrial electron transport chain (ETC) complexes generate the mitochondrial membrane potential, which is essential to produce cellular energy, ATP. Reduced mitochondrial respiration and energy status have been found in many human pathological conditions including aging, cancer, and neurodegenerative disease. In this study we investigated whether betaine directly targets mitochondria. We show that betaine treatment leads to an upregulation of mitochondrial respiration and cytochrome c oxidase activity in H2.35 cells, the proposed rate limiting enzyme of ETC in vivo. Following treatment, the mitochondrial membrane potential was increased and cellular energy levels were elevated. We propose that the anti-proliferative effects of betaine on cancer cells might be due to enhanced mitochondrial function contributing to a reversal of the Warburg effect.

60 APPLIED LIFE SCIENCES↗

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