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At least 1,801 records · Page 100
All sourcesNASA NTRSDOE OSTI
DOE OSTI2020

Pressurization Analysis for Heating of a Screw Top Utility Can Loaded With Plutonium Oxide Powder by a 1273 K Fire

The documented safety analysis for the Savannah River National Laboratory (SRNL) evaluates the consequences of a postulated 1273 K fire in a glovebox. The radiological dose consequences for a pressurized release of plutonium oxide powder during such a fire depend on the maximum pressure that is attained inside the oxide storage containers. The oxide storage configuration selected for analysis is can/bag/can, comprised of oxide powder inside an 8.38 × 10 -6 m 3 stainless steel B vial inside 0.006 kg of polyethylene bagging inside a one-quart screw top utility can of the type commonly used to package solvents or rubber cements. To enable evaluation of the dose consequences, temperature and pressure transients have been calculated for exposure of a typical set of storage containers to the fire. The pressurization analysis credits venting to and from the B vial but does not credit venting or leakage from the can. Due to the low rate of venting from the B vial into the can gas space, the can pressure is nearly independent of the B vial pressure. Calculated maximum pressures are compared to the utility can burst pressure. In lieu of a structural analysis of the utility cans, burst pressures and leakage rates were measured using compressed nitrogen gas. The measured gauge burst pressure was 0.250 ± 0.043 MPa. The measured burst pressures are lower than the calculated maximum pressure due to fire exposure, indicating that the utility cans could burst during exposure to a 1273 K fire.

98 NUCLEAR DISARMAMENT, SAFEGUARDS, AND PHYSICAL P↗
DOE OSTI2013

Influence of Cracks in Cementitious Engineered Barriers in a Near-Surface Disposal System: Assessment Analysis of the Belgian Case

In large cement-based structures such as a near surface disposal facility for radioactive waste voids and cracks are inevitable. However, the pattern and nature of cracks are very difficult to predict reliably. Cracks facilitate preferential water flow through the facility because their saturated hydraulic conductivity is generally higher than the conductivity of the cementitious matrix. Moreover, sorption within the crack is expected to be lower than in the matrix and hence cracks in engineered barriers can act as a bypass for radionuclides. Consequently, understanding the effects of crack characteristics on contaminant fluxes from the facility is of utmost importance in a safety assessment. In this paper we numerically studied radionuclide leaching from a crack-containing cementitious containment system. First, the effect of cracks on radionuclide fluxes is assessed for a single repository component which contains a radionuclide source (i.e. conditioned radwaste). These analyses reveal the influence of cracks on radionuclide release from the source. The second set of calculations deals with the safety assessment results for the planned near-surface disposal facility for low-level radioactive waste in Dessel (Belgium); our focus is on the analysis of total system behaviour in regards to release of radionuclide fluxes from the facility. Simulation results are interpreted through a complementary safety indicator (radiotoxicity flux). We discuss the possible consequences from different scenarios of cracks and voids. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2013

Destructive testings: dry drilling operations with TruPro system to collect samples in a powder form, from two hulls containing immobilized wastes in a hydraulic binder

The TruPro{sup R} process enables to collect a significant number of samples to characterize radiological materials. This innovative and alternative technique is experimented for the ANDRA quality-control inspection of cemented packages. It proves to be quicker and more prolific than the current methodology. Using classical statistics and geo-statistics approaches, the physical and radiological characteristics of two hulls containing immobilized wastes (sludges or concentrates) in a hydraulic binder are assessed in this paper. The waste homogeneity is also evaluated in comparison to ANDRA criterion. Sensibility to sample size (support effect), presence of extreme values, acceptable deviation rate and minimum number of data are discussed. The final objectives are to check the homogeneity of the two characterized radwaste packages and also to validate and reinforce this alternative characterization methodology. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2013

Management of the decommissioning of the Thetis reactor

The Thetis research reactor on the site of the Nuclear Sciences Institute of the Ghent University has been in operation from 1967 until December 2003. This light-water moderated graphite-reflected low-enriched uranium pool-type reactor has been used for various purposes e.g. the production of radioisotopes and activation analyses. During the first years its core power was 15 kW. In the early '70, a core enlargement allowed for operation at typically 150 kW, while the maximum was allowed to be 250 kW In September 2007, Ghent University entrusted to SCK-CEN the management of the back-end of the spent fuel and the decommissioning of the reactor. In 2010, the spent fuel was removed from the reactor and transported to Belgoprocess for cementation in 400 l drums and interim storage awaiting final disposal. This activity allows tackling the decommissioning of the reactor. The objective is to complete its decommissioning by the end of 2014. In the framework of the decommissioning of the Thetis reactor, SCK-CEN set-up the final decommissioning plan and the decommissioning licensing file. These documents include among others a radiological inventory of the reactor. The graphite moderator blocks, the control and the safety pates, the liner of the pool were modeled to assess the activation products (isotopic vector and intensity). At the end of the unloading of the reactor in 2010 a brief mapping of the equipment's and internals of the reactor pool was performed. In 2012, we realized a more detailed mapping. These results confirmed those performed earlier and allowed to confirm the assumptions made in the final decommissioning plan. We set-up the terms of reference for the first decommissioning phase of the reactor namely the dismantling of the reactor i.e. reactor pool, circuits and rabbit system, equipment's and ventilation ducts. The removal of asbestos is also included into this phase. We conducted the selection process and the awarding of this decommissioning job. We gained the decommissioning license in May 2012. We also prepared the software tool allowing managing the decommissioning project by updating the inventory and recording the progress, the characterization measurements and the material and waste production. This software allows also to trace all the material streams and to report to the Authorities. This software is a simplified release of the ones developed by SCK-CEN in the framework of other decommissioning projects like BR3 and Belgonucleaire. The dismantling of the reactor i.e. reactor pool, circuits and rabbit system, will be performed in 2013. In 2014, it is planned to map all the surfaces of the infrastructure to highlight residual contamination of floor, walls and ceiling. The contaminated surfaces will be decontaminated and controlled. The objective is to reach the free release of the reactor building and laboratories by the end of 2014. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2013

Key differentiators influencing the choice of robust shielded containers

The NDA's Upstream Optioneering project has examined the potential implications of using an alternative type of waste package and its influence on the waste management lifecycle across the NDA estate. Robust Shielded Containers (RSCs) are radioactive waste packages that provide integral radiological shielding, reducing the need for remote handling. The robustness of the container could remove the need to immobilise waste by cement encapsulation. RSCs are routinely used to package ILW for interim storage in Germany and have fairly recently been considered for use in the UK because RSCs have the potential to simplify the waste management lifecycle and enable risk and hazard reduction. In particular, the current baseline (included in Magnox Limited lifetime plans) follows the strategy set out in the Magnox Operating Decommissioning Programme (MODP), in which Type II MOSAIK and Type VI Ductile Cast Iron Containers (DCICs) are used to package (in non-encapsulated form) most Magnox ILW arising prior to 2050. By considering representative types of Intermediate Level Waste (ILW) and exploring potential packaging options for these wastes, this paper identifies the factors that could differentiate between cases in which RSCs would, or would not, be an appropriate option. The potential role of RSCs across the waste management lifecycle is examined, from retrieval of waste through to emplacement at a Geological Disposal Facility (GDF), including consideration of other potential uses of RSCs, such as temporary storage of raw wastes for which appropriate treatment and conditioning measures have yet to be developed. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2013

Management of historical waste from research reactors: the Dutch experience

Most radioactive waste emerges as well-defined waste streams from operating power reactors. The management of this is an on-going practice, based on comprehensive (IAEA) guidelines. A special waste category however consists of the historical waste from research reactors, mostly originating from various experiments in the early years of the nuclear era. Removal of the waste from the research site, often required by law, raises challenges: the waste packages must fulfill the acceptance criteria from the receiving storage site as well as the criteria for nuclear transports. Often the aged waste containers do not fulfill today's requirements anymore, and their contents are not well documented. Therefore removal of historical waste requires advanced characterization, sorting, sustainable repackaging and sometimes conditioning of the waste. This paper describes the Dutch experience of a historical waste removal campaign from the Petten High Flux research reactor. The reactor is still in operation, but Dutch legislation asks for central storage of all radioactive waste at the COVRA site in Vlissingen since the availability of the high- and intermediate-level waste storage facility HABOG in 2004. In order to comply with COVRA's acceptance criteria, the complex and mixed inventory of intermediate and low level waste must be characterized and conditioned, identifying the relevant nuclides and their activities. Sorting and segregation of the waste in a Hot Cell offers the possibility to reduce the environmental footprint of the historical waste, by repackaging it into different classes of intermediate and low level waste. In this way, most of the waste volume can be separated into lower level categories not needing to be stored in the HABOG, but in the less demanding LOG facility for low-level waste instead. The characterization and sorting is done on the basis of a combination of gamma scanning with high energy resolution of the closed waste canister and low-resolution localized gamma scanning inside a hot cell. A complicating factor is that the conditioning of the waste, consisting of compacting and cementing, would require such an extensive infrastructure at the Petten site, that it appeared to be more practical to have it executed by a foreign service provider. Therefore the waste packages have to comply with cross-border transport and waste acceptance criteria, and the national legislation of this service provider too. This paper describes this historical waste project, focusing on the fast and precise characterization approach, the expert system behind it, and the sorting and repackaging effort at the Petten site. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2017

An optically passive method that rate doubles 2-GHz timing fiducials

Solid-state optical comb-pulse generators provide a convenient and accurate method to include timing fiducials in a streak camera image for time base correction. Commercially available vertical-cavity surface-emitting lasers (VCSEL’s) emitting in the visible currently in use can be modulated up to 2 GHz. An optically passive method is presented to interleave a time-delayed path of the 2-GHz comb with itself, producing a 4-GHz comb. This technique can be applied to VCSEL’s with higher modulation rates. A fiber-delivered, randomly polarized 2 GHz VCSEL comb is polarization split into s polarization and p polarization paths. One path is time delayed relative to the other by twice the 2-GHz rate with 1-ps accuracy; the two paths then recombine at the fiber-coupled output. High throughput (≥90%) is achieved by carefully using polarization beam-splitting cubes, a total internal reflection beam-path–steering prism, and antireflection coatings. The glass path-length delay block and turning prism are optically contacted together. The beam polarizer cubes that split and recombine the paths are precision aligned and permanently cemented into place. We expect the palm-sized, inline fiber-coupled, comb-rate–doubling device to maintain its internal alignment indefinitely.

optical comb-pulse generators, timing fiducials, s↗
DOE OSTI2022

Understanding the Elastic, Plastic, and Damage Features in Fracturing of Self-reinforced Thermoplastic Composites via Non-destructive Digital Imaging Correlation

This work demonstrated the utilization of non-destructive Digital Imaging Correlation (DIC) method to characterize the elastic, plastic, and damage features during the Mode I intra-laminar fracturing process of self-reinforced thermoplastic composites by using a self-reinforced polypropylene (PP) composite as an example. The DIC results clearly showed the development of huge plastic zone (PZ) and non-negligible Fracture Process Zone (FPZ) in front of the notch tip during the fracturing process, and the geometries and sizes of the foregoing zones at the peak load were further quantified. Such an interesting fracturing behavior of self-reinforced thermoplastic composites is way different from brittle materials (e.g., glass, acrylic, etc.), ductile materials (e.g., aluminum, steel, etc.), and even quasi-brittle materials (e.g., concrete, nanoparticle-reinforced composites, tough ceramics, wood, cement, carbon/glass fiber-reinforced polymers, etc.). Thus, understanding the elastic, plastic, and damage features is the first step before better characterizing the material fracture properties of self-reinforced thermoplastic composites through new analytical methods and computational modeling. These efforts are of utmost importance for wide applications of self-reinforced thermoplastic composites in various engineering fields in the future.

Lightweight Composites, Self-reinforced Thermoplas↗
DOE OSTI2023

Towards a new generation long trace profiler LTP-2020: optical design of pencil beam interferometry sensor

Improvements in the quality of synchrotron beamline x-ray optics required for next-generation light sources (e.g. the ALS Upgrade project) drive the need to improve the performance of the metrology instrumentation used to measure these components. The Long Trace Profiler (LTP) that is in use at many synchrotron metrology laboratories around the world has some known issues that affect the accuracy of its measurements. The main error source is optical path difference (OPD) phase error introduced into the probe beam by inhomogeneities in the glass components used in the optical head. We have developed a new optical head design, LTP-2020, that replaces the cube polarizing beamsplitter (PBS) with a thin wedge plate polarizing beamsplitter (WPBS) and replaces the cemented doublet lens with an aspheric singlet. Both of these components significantly reduce the glass volume traversed by the laser probe beam. Careful attention to ghost ray interference produced by back reflection from optical surfaces is necessary to minimize distortion in the primary image that translates into systematic error in the slope angle measurement. We make extensive use of a commercial raytracing program to model the back reflections and adjust component parameters as necessary to minimize distortion. Deliberate misalignment of components is necessary to make the system perform correctly. Stringent requirements are placed on the 45◦ incidence coatings on the WPBS and on the normal incidence coatings on the lens and camera window elements. We encourage our colleagues who wish to upgrade their current LTP systems to join us in the procurement of these custom optical components.

Takacs, Peter Z.↗
DOE OSTI2014

SU-E-E-07: When the Old Ways Are the Best Ways: In Defense of Didactic Training

Purpose: Physics education for residents has taken on a more prominent role due to the new ABR examination format. We present a curriculum for a new radiology residency entering its second year. This curriculum favors an extensive traditional didactic teaching approach. The curriculum is designed to minimize the amount of independent learning that is necessary outside the classroom Methods and Materials: idactic training repeats yearly for all four years of residency and consists of two 1-hour lectures per week and several in-class tests. The impact of physics on clinical practice is introduced gradually throughout the residency using specific clinical cases. The extensive time spent with the residents allows lectures to be taught at a deep (almost physicist) level and reduces the necessity of learning base concepts outside of lecture. This frees the resident to use resources (e.g., AAPM/RSNA physics modules) to cement concepts through repetition or to learn a slightly confusing concept from a different teaching perspective. Consistent testing reduces the traditional resident studying technique of physics “cramming.” Results: On average, the first year residents scored in the 98th percentile on the American College of Radiology Diagnostic Radiology In-Service Training Exam (ACR DXIT). Feedback from the new first year residents was very positive and suggestions are constantly solicited and incorporated. For example, based on resident feedback, short-format quizzes each lecture were eliminated and replaced interactive questions during lecture. Residents felt they have advanced rapidly and have a better understanding of radiologic physics, though they have expressed concern that the 1-hour lecture block may not be optimal for learning physics. Conclusion: An extensive, physicist-led series of didactic lectures is effective in the teaching of physics to residents.

96 KNOWLEDGE MANAGEMENT AND PRESERVATION↗
DOE OSTI2016

TH-CD-206-08: An Anthropopathic Deformable Phantom for Geometric and Dose Accumulation Accuracy Validation of Deformable Image Registration

Purpose: To design and construct a three-dimensional (3D) anthropopathic abdominal phantom for evaluating deformable image registration (DIR) accuracy on images and dose deformation in adaptive radiation therapy (ART). Method: Organ moulds, including liver, kidney, spleen, stomach, vertebra and two metastasis tumors, are 3D printed using the contours from an ovarian cancer patient. The organ moulds are molded with deformable gels that made of different mixtures of polyvinyl chloride (PVC) and the softener dioctyl terephthalate. Gels with different densities are obtained by a polynomial fitting curve which describes the relation between the CT number and PVC-softener blending ratio. The rigid vertebras are constructed by moulding with white cement. The final abdominal phantom is assembled by arranging all the fabricated organs inside a hollow dummy according to their anatomies and sealed with deformable gel with averaged CT number of muscle and fat. Geometric and dosimetric landmarks are embedded inside the phantom for spatial accuracy and dose accumulation accuracy studies. Three DIR algorithms available in the open source DIR toolkit-DIRART, including the Demons, the Horn-Schunck and Lucas-Kanade method and the Level-Set Motion method, are tested using the constructed phantom. Results: Viscoelastic behavior is observed in the constructed deformable gel, which serves as an ideal material for the deformable phantom. The constructed abdominal phantom consists of highly realistic anatomy and the fabricated organs inside have close CT number to its reference patient. DIR accuracy studies conducted on the constructed phantom using three DIR approaches indicate that geometric accuracy of a DIR algorithm has achieved does not guarantee accuracy in dose accumulation. Conclusions: We have designed and constructed an anthropopathic abdominal deformable phantom with satisfactory elastic property, realistic organ density and anatomy. This physical phantom is recyclable and can be used for routine validations of DIR geometric accuracy and dose accumulation accuracy in ART. This work is supported in part by grant from VARIAN MEDICAL SYSTEMS INC, the National Natural Science Foundation of China (no 81428019 and no 81301940), the Guangdong Natural Science Foundation (2015A030313302) and the 2015 Pearl River S&T Nova Program of Guangzhou (201506010096).

60 APPLIED LIFE SCIENCES↗
DOE OSTI2018

Net-zero emissions energy systems

Some energy services and industrial processes - such as long-distance freight transport, air travel, highly reliable electricity, and steel and cement manufacturing - are particularly difficult to provide without adding carbon dioxide (CO 2 ) to the atmosphere. Rapidly growing demand for these services, combined with long lead times for technology development and long lifetimes of energy infrastructure, make decarbonization of these services both essential and urgent. We examine barriers and opportunities associated with these difficult-to-decarbonize services and processes, including possible technological solutions and research and development priorities. A range of existing technologies could meet future demands for these services and processes without net addition of CO 2 to the atmosphere, but their use may depend on a combination of cost reductions via research and innovation, as well as coordinated deployment and integration of operations across currently discrete energy industries.

24 POWER TRANSMISSION AND DISTRIBUTION↗
DOE OSTI2019

A hydrated crystalline calcium carbonate phase: Calcium carbonate hemihydrate

As one of the most abundant materials in the world, calcium carbonate, CaCO 3 , is the main constituent of the skeletons and shells of various marine organisms. It is used in the cement industry and plays a crucial role in the global carbon cycle and formation of sedimentary rocks. For more than a century, only three polymorphs of pure CaCO 3 —calcite, aragonite, and vaterite—were known to exist at ambient conditions, as well as two hydrated crystal phases, monohydrocalcite (CaCO 3 ·1H 2 O) and ikaite (CaCO 3 ·6H 2 O). While investigating the role of magnesium ions in crystallization pathways of amorphous calcium carbonate, we unexpectedly discovered an unknown crystalline phase, hemihydrate CaCO 3 ·½H 2 O, with monoclinic structure. This discovery may have important implications in biomineralization, geology, and industrial processes based on hydration of CaCO 3 .

Science & Technology - Other Topics↗
DOE OSTI2016

Improved High-Quality Draft Genome Sequence of the Eurypsychrophile Rhodotorula sp. JG1b, Isolated from Permafrost in the Hyperarid Upper-Elevation McMurdo Dry Valleys, Antarctica

Here, we report the draft genome sequence of Rhodotorula sp. strain JG1b, a yeast that was isolated from ice-cemented permafrost in the upper-elevation McMurdo Dry Valleys, Antarctica. The sequenced genome size is 19.39 Mb, consisting of 156 scaffolds and containing a total of 5,625 predicted genes. This is the first known cold-adapted Rhodotorula sp. sequenced to date.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2025

The Thermococcales as a model system: historical perspectives and emerging tools

Thermococcales are among the most widely studied hyperthermophilic Archaea and have become key models for understanding life at extreme temperatures. Early work in the 1980s culminated in the isolation of novel Thermococcales species from hydrothermal vents that grew rapidly, tolerated extreme heat, and metabolized diverse substrates, making them uniquely amenable for laboratory studies. Their thermostable enzymes and emerging genetic tools facilitated detailed investigations of core processes such as DNA replication, repair, and transcription under conditions that challenge most life forms. These practical advantages, together with the accumulation of tools and protocols, cemented the role of Thermococcales as a model system. Here, we recount how chance discoveries, environmental adaptations, and experimental practicality intersected to establish Thermococcales as a central model for studying archaeal biology and extremophile physiology.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2025

Ultrafast Spectroscopy and Dynamics of Photoredox Catalysis

Photoredox catalysis has emerged as a powerful platform for chemical synthesis, utilizing chromophore excited states as selective energy stores to surmount chemical activation barriers toward making desirable products. Developments in this field have pushed synthetic chemists to design and discover new photocatalysts with novel and impactful photoreactivity but also with uncharacterized excited states and only an approximate mechanistic understanding. This review highlights specific instances in which ultrafast spectroscopies dissected the photophysical and photochemical dynamics of new classes of photoredox catalysts and their photochemical reactions. After briefly introducing the photophysical processes and ultrafast spectroscopic methods central to this topic, the review describes selected recent examples that evoke distinct classes of photoredox catalysts with demonstrated synthetic utility and ultrafast spectroscopic characterization. Furthermore, this review cements the significant role of ultrafast spectroscopy in modern photocatalyzed organic transformations and institutionalizes the developing intersection of synthetic organic chemistry and physical chemistry.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2015

CaCl 2 ‐Accelerated Hydration of Tricalcium Silicate: A STXM Study Combined with 29 Si MAS NMR

The effect of calcium chloride (CaCl 2 ) on tricalcium silicate (C 3 S) hydration was investigated by scanning transmission X‐ray microscopy (STXM) with Near Edge X‐ray Absorption Fine Structure (NEXAFS) spectra and 29 Si MAS NMR. STXM is demonstrated to be a powerful tool for studying the chemical composition of a cement‐based hydration system. The Ca L 3,2 ‐edge NEXAFS spectra obtained by examining C 3 S hydration in the presence of CaCl 2 showed that this accelerator does not change the coordination of calcium in the calcium silicate hydrate (C‐S‐H), which is the primary hydration product. O K‐edge NEXAFS is also very useful in distinguishing the chemical components in hydrated C 3 S. Based on the Ca L 3,2 ‐edge spectra and chemical component mapping, we concluded that CaCl 2 prefers to coexist with unhydrated C 3 S instead of C‐S‐H. In Si K‐edge NEXAFS analysis, CaCl 2 increases the degree of silicate polymerization of C‐S‐H in agreement with the 29 Si CP/MAS NMR results, which show that the presence of CaCl 2 in hydrated C 3 S considerably accelerates the formation of middle groups ( Q 2 ) and branch sites ( Q 3 ) in the silicate chains of C‐S‐H gel at 1‐day hydration.

Li, Qinfei↗
DOE OSTI2017

Tropical Convective Transition Statistics and Causality in the Water Vapor–Precipitation Relation

Abstract Previous work by various authors has pointed to the role of lower-free-tropospheric humidity in affecting the onset of deep convection in the tropics. Empirical relationships between column water vapor (CWV) and precipitation have been inferred to result from these effects. Evidence from previous work has included deep convective conditional instability calculations for entraining plumes, in which the lower-free-tropospheric environment affects the onset of deep convection due to the differential impact on buoyancy of turbulent entrainment of dry versus moist air. The relationship between deep convection and water vapor is, however, a two-way interaction because convection also moistens the free troposphere. The present study adds an additional line of evidence toward fully establishing the causality of the precipitation–water vapor relationship. Parameter perturbation experiments using the coupled Community Earth System Model (CESM) with high-time-resolution output are analyzed for a set of statistics for the transition to deep convection, coordinated with observational diagnostics for the Green Ocean Amazon (GOAmazon) campaign and tropical western Pacific Atmospheric Radiation Measurement (ARM) sites. For low values of entrainment in the deep convective scheme, these statistics are radically altered and the observed pickup of precipitation with CWV is no longer seen. In addition to helping cement the dominant direction of causality in the fast-time-scale precipitation–CWV relationship, the results point to impacts of entrainment on the climatology. Because at low entrainment convection can fire before tropospheric moistening, the climatological values of relative humidity are lower than observed. These findings can be consequential to biases in simulated climate and to projections of climate change.

54 ENVIRONMENTAL SCIENCES↗

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