Results for “surface characterization” — Page 10

NASA NTRS2001

Carbon Nanotube Tip Probes: Stability and Lateral Resolution in Scanning Probe Microscopy and Application to Surface Science to Semiconductors

In this paper we present results on the stability and lateral resolution capability of carbon nanotube (CNT) scanning probes as applied to atomic force microscopy (AFM). Surface topography images of ultra-thin films (2-5 nm thickness) obtained with AFM are used to illustrate the lateral resolution capability of single-walled carbon nanotube probes. Images of metal films prepared by ion beam sputtering exhibit grain sizes ranging from greater than 10 nm to as small as approximately 2 nm for gold and iridium respectively. In addition, imaging stability and lifetime of multi-walled carbon nanotube scanning probes are studied on a relatively hard surface of silicon nitride (Si3N4). AFM images Of Si3N4 surface collected after more than 15 hrs of continuous scanning show no detectable degradation in lateral resolution. These results indicate the general feasibility of CNT tips and scanning probe microscopy for examining nanometer-scale surface features of deposited metals as well as non-conductive thin films. AFM coupled with CNT tips offers a simple and nondestructive technique for probing a variety of surfaces, and has immense potential as a surface characterization tool in integrated circuit manufacturing.

Nguyen, Cattien V.↗

NASA NTRS2005

RIO Tinto Faulted Volcanosedimentary Deposits as Analog Habitats for Extant Subsurface Biospheres on Mars: A Synthesis of the MARTE Drilling Project Geobiology Results

Geochemistry and mineralogy on Mars surface characterized by the MER Opportunity Rover suggest that early Mars hosted acidic environments in the Meridiani Planum region [1, 2]. Such extreme paleoenvironments have been suggested to be a regional expression of the global Mars geological cycle that induced acidic conditions by sulfur complexation and iron buffering of aqueous solutions [3]. Under these assumptions, underground reservoirs of acidic brines and, thereby, putative acidic cryptobiospheres, may be expected. The MARTE project [4, 5] has performed a drilling campaign to search for acidic and anaerobic biospheres in R o Tinto basement [6] that may be analogs of these hypothetical communities occurring in cryptic habitats of Mars. This Rio Tinto geological region is characterized by the occurrence of huge metallic deposits of iron sulfides [7]. Late intensive diagenesis of rocks driven by a compressive regimen [8] largely reduced the porosity of rocks and induced a cortical thickening through thrusting and inverse faulting and folding. Such structures play an essential role in transporting and storing water underground as any other aquifers do in the Earth. Once the underground water reservoirs of the Ro Tinto basement contact the hydrothermal pyrite deposits, acidic brines are produced by the release of sulfates and iron through the oxidation of sulfides [9].

Fernandez-Remolar, D. C.↗

NASA NTRS2005

Oxide Ceramic Films Grown on 60 Nitinol for NASA and Department of Defense Applications

Both the NASA Glenn Research Center and the U.S. Army Research Laboratory, Development and Engineering Center (ARDEC) have worked to develop oxide ceramic films grown on 60 nitinol (60-wt% nickel and 40-wt% titanium) to decrease friction and increase wear resistance under unlubricated conditions. In general, oxide and nonoxide ceramic films have unique capabilities as mechanical-, chemical-, and thermal-barrier materials in diverse applications, including high-temperature bearings and gas bearings requiring low friction, wear resistance, and chemical stability. All oxide ceramic films grown on 60 nitinol were furnished by ARDEC, and materials and surface characterization and tribological experiments were conducted at Glenn.

Miyoshi, Kazuhisa↗

NASA NTRS2006

Reliability of Radioisotope Stirling Convertor Linear Alternator

Onboard radioisotope power systems being developed and planned for NASA s deep-space missions would require reliable design lifetimes of up to 14 years. Critical components and materials of Stirling convertors have been undergoing extensive testing and evaluation in support of a reliable performance for the specified life span. Of significant importance to the successful development of the Stirling convertor is the design of a lightweight and highly efficient linear alternator. Alternator performance could vary due to small deviations in the permanent magnet properties, operating temperature, and component geometries. Durability prediction and reliability of the alternator may be affected by these deviations from nominal design conditions. Therefore, it is important to evaluate the effect of these uncertainties in predicting the reliability of the linear alternator performance. This paper presents a study in which a reliability-based methodology is used to assess alternator performance. The response surface characterizing the induced open-circuit voltage performance is constructed using 3-D finite element magnetic analysis. Fast probability integration method is used to determine the probability of the desired performance and its sensitivity to the alternator design parameters.

Shah, Ashwin↗

NASA NTRS2010

Land Surface Emission Modeling to Support Physical Precipitation Retrievals

Land surface modeling and data assimilation can provide dynamic land surface state variables necessary to support physical precipitation retrieval algorithms over land. It is well-known that surface emission, particularly over the range of frequencies to be included in the Global Precipitation Measurement Mission (GPM), is sensitive to land surface states, including soil properties, vegetation type and greenness, soil moisture, surface temperature, and snow cover, density, and grain size. In order to investigate the robustness of both the land surface model states and the microwave emissivity and forward radiative transfer models, we have undertaken a multi-site investigation as part of the NASA Precipitation Measurement Missions (PMM) Land Surface Characterization. Working Group.

Peters-Lidard, Christina D.↗

NASA NTRS2011

NASA Tech Briefs, December 2011

Topics covered include: 1) SNE Industrial Fieldbus Interface; 2) Composite Thermal Switch; 3) XMOS XC-2 Development Board for Mechanical Control and Data Collection; 4) Receiver Gain Modulation Circuit; 5) NEXUS Scalable and Distributed Next-Generation Avionics Bus for Space Missions; 6) Digital Interface Board to Control Phase and Amplitude of Four Channels; 7) CoNNeCT Baseband Processor Module; 8) Cryogenic 160-GHz MMIC Heterodyne Receiver Module; 9) Ka-Band, Multi-Gigabit-Per-Second Transceiver; 10) All-Solid-State 2.45-to-2.78-THz Source; 11) Onboard Interferometric SAR Processor for the Ka-Band Radar Interferometer (KaRIn); 12) Space Environments Testbed; 13) High-Performance 3D Articulated Robot Display; 14) Athena; 15) In Situ Surface Characterization; 16) Ndarts; 17) Cryo-Etched Black Silicon for Use as Optical Black; 18) Advanced CO2 Removal and Reduction System; 19) Correcting Thermal Deformations in an Active Composite Reflector; 20) Umbilical Deployment Device; 21) Space Mirror Alignment System; 22) Thermionic Power Cell To Harness Heat Energies for Geothermal Applications; 23) Graph Theory Roots of Spatial Operators for Kinematics and Dynamics; 24) Spacesuit Soft Upper Torso Sizing Systems; 25) Radiation Protection Using Single-Wall Carbon Nanotube Derivatives; 26) PMA-PhyloChip DNA Microarray to Elucidate Viable Microbial Community Structure; 27) Lidar Luminance Quantizer; 28) Distributed Capacitive Sensor for Sample Mass Measurement; 29) Base Flow Model Validation; 30) Minimum Landing Error Powered-Descent Guidance for Planetary Missions; 31) Framework for Integrating Science Data Processing Algorithms Into Process Control Systems; 32) Time Synchronization and Distribution Mechanisms for Space Networks; 33) Local Estimators for Spacecraft Formation Flying; 34) Software-Defined Radio for Space-to-Space Communications; 35) Reflective Occultation Mask for Evaluation of Occulter Designs for Planet Finding; and 36) Molecular Adsorber Coating

Source record↗

NASA NTRS2011

Geo-Statistical Approach to Estimating Asteroid Exploration Parameters

NASA's vision for space exploration calls for a human visit to a near earth asteroid (NEA). Potential human operations at an asteroid include exploring a number of sites and analyzing and collecting multiple surface samples at each site. In this paper two approaches to formulation and scheduling of human exploration activities are compared given uncertain information regarding the asteroid prior to visit. In the first approach a probability model was applied to determine best estimates of mission duration and exploration activities consistent with exploration goals and existing prior data about the expected aggregate terrain information. These estimates were compared to a second approach or baseline plan where activities were constrained to fit within an assumed mission duration. The results compare the number of sites visited, number of samples analyzed per site, and the probability of achieving mission goals related to surface characterization for both cases.

probability↗

NASA NTRS2014

Landsat-8: Science and Product Vision for Terrestrial Global Change Research

Landsat 8, a NASA and USGS collaboration, acquires global moderate-resolution measurements of the Earth's terrestrial and polar regions in the visible, near-infrared, short wave, and thermal infrared. Landsat 8 extends the remarkable 40 year Landsat record and has enhanced capabilities including new spectral bands in the blue and cirrus cloud-detection portion of the spectrum, two thermal bands, improved sensor signal-to-noise performance and associated improvements in radiometric resolution, and an improved duty cycle that allows collection of a significantly greater number of images per day. This paper introduces the current (2012-2017) Landsat Science Team's efforts to establish an initial understanding of Landsat 8 capabilities and the steps ahead in support of priorities identified by the team. Preliminary evaluation of Landsat 8 capabilities and identification of new science and applications opportunities are described with respect to calibration and radiometric characterization; surface reflectance; surface albedo; surface temperature, evapotranspiration and drought; agriculture; land cover, condition, disturbance and change; fresh and coastal water; and snow and ice. Insights into the development of derived 'higher-level' Landsat products are provided in recognition of the growing need for consistently processed, moderate spatial resolution, large area, long-term terrestrial data records for resource management and for climate and global change studies. The paper concludes with future prospects, emphasizing the opportunities for land imaging constellations by combining Landsat data with data collected from other international sensing systems, and consideration of successor Landsat mission requirements.

Landsat↗

NASA NTRS2019

Climates of Warm Earth-Like Planets III: Fractional Habitability from a Water Cycle Perspective

The habitable fraction of a planet's surface is important for the detectability of surface biosignatures. The extent and distribution of habitable areas are influenced by external parameters that control the planet's climate, atmospheric circulation, and hydrological cycle. We explore these issues using the ROCKE-3D general circulation model, focusing on terrestrial water fluxes and thus the potential for the existence of complex life on land. Habitability is examined as a function of insolation and planet rotation for an Earth-like world with zero obliquity and eccentricity orbiting the Sun. We assess fractional habitability using an aridity index that measures the net supply of water to the land. Earth-like planets become "superhabitable" (a larger habitable surface area than Earth) as insolation and day-length increase because their climates become more equable, reminiscent of past warm periods on Earth when complex life was abundant and widespread. The most slowly rotating, most highly irradiated planets, though, occupy a hydrological regime unlike any on Earth, with extremely warm, humid conditions at high latitudes but little rain and subsurface water storage. Clouds increasingly obscure the surface as insolation increases, but visibility improves for modest increases in rotation period. Thus, moderately slowly rotating rocky planets with insolation near or somewhat greater than modern Earth's appear to be promising targets for surface characterization by a future direct imaging mission.

Del Genio, Anthony D.↗

NASA NTRS2019

Climates of Warm Earth-like Planets. III. Fractional Habitability from a Water Cycle Perspective

The habitable fraction of a planet's surface is important for the detectability of surface biosignatures. The extent and distribution of habitable areas are influenced by external parameters that control the planet's climate, atmospheric circulation, and hydrological cycle. We explore these issues using the ROCKE-3D general circulation model, focusing on terrestrial water fluxes and thus the potential for the existence of complex life on land. Habitability is examined as a function of insolation and planet rotation for an Earth-like world with zero obliquity and eccentricity orbiting the Sun. We assess fractional habitability using an aridity index that measures the net supply of water to the land. Earth-like planets become "superhabitable" (a larger habitable surface area than Earth) as insolation and day-length increase because their climates become more equable, reminiscent of past warm periods on Earth when complex life was abundant and widespread. The most slowly rotating, most highly irradiated planets, though, occupy a hydrological regime unlike any on Earth, with extremely warm, humid conditions at high latitudes but little rain and subsurface water storage. Clouds increasingly obscure the surface as insolation increases, but visibility improves for modest increases in rotation period. Thus, moderately slowly rotating rocky planets with insolation near or somewhat greater than modern Earth's appear to be promising targets for surface characterization by a future direct imaging mission.

Exoplanet atmospheric variability↗

NASA NTRSDate not supplied

Examination of Lunar Regolith Simulants By SEM-EDS and Imaging Raman Spectroscopy

The Artemis series lunar missions will include sample returns from the lunar south pole. Lunar regolith simulants (RS) generated in the lab provide opportunities to compare two surface science techniques: scanning electron microscopy (SEM-EDS) and Raman induced surface spectroscopy. The results will also be applicable for supporting future commercial lunar payload services (CLPS) and Artemis surface. Surface characterization contributes to continued development of lunar regolith studies and adds to various regolith databases. In characterizing various lunar regolith simulants, part of the aim should be to standardize techniques and utilize anticipated methods available for astromaterials studied during, or returned from, upcoming missions, particularly samples collected from the Moon’s south pole and permanently shadowed regions (PSRs).. An initial survey of available simulants has been started with Raman scanning process for particle counting the results of which will enrich the NASA-JSC Simulant Development Lab (SDL) simulant properties database and the Colorado School of Mines Planetary Simulant Data Base. An SEM-EDS dataset of raw regolith simulant materials are collected.

Raman Microscopy↗

NASA NTRSDate not supplied

The Material Response of PICA-NuSil to a Hypersonic Flow Environment

Phenolic Impregnated Carbon Ablator (PICA) is NASA’s baseline thermal protection system for missions to Mars. PICA is friable; therefore, NuSil ® CV-1144-0 is applied to the surface of flight hardware to mitigate the contamination of spacecraft sensors. NuSil is composed of a polysiloxane resin system that can transform into an oxidation-resistant coating upon heating. Therefore, a pathfinder campaign was conducted at the Hypersonic Materials Environmental Test System (HyMETS) at the NASA Langley Research Center to investigate the material response of instrumented sphere-cone models made from PICA coated with NuSil ® . Analysis of the post-test data is presented and suggests that NuSil ® impacts the material response of test articles subjected to oxidizing atmospheres, as evidenced by a reduction of the measured surface temperature and in-depth temperature response. Finally, a four-step ablation mechanism is proposed based on observations from high-speed video, optical emission spectroscopy, thermal analysis, and post-test surface characterization.

PICA PICA-NuSil Siloxane Silicone↗

NASA NTRS2002

Properties of M40J Carbon/PMR-II-50 Composites Fabricated with Desized and Surface Treated Fibers. Characterization of M40J Desized and Finished Fibers

To increase performance and durability of high temperature composites for potential rocket engine components, it is necessary to optimize wetting and interfacial bonding between high modulus carbon fibers and high temperature polyimide resins. It has been previously demonstrated that the electro-oxidative shear treatments used by fiber manufacturers are not effective on higher modulus fibers that have fewer edge and defect sites in the surface crystallites. In addition, sizings commercially supplied on most carbon fibers are not compatible with polyimides. This study was an extension of prior work characterizing the surface chemistry and energy of high modulus carbon fibers (M40J and M60J, Torray) with typical fluorinated polyimide resins, such as PMR-II-50. A continuous desizing system which utilizes environmentally friendly chemical- mechanical processes was developed for tow level fiber and the processes were optimized based on weight loss behavior, surface elemental composition (XPS) and morphology (FE-SEM) analyses, and residual tow strength of the fiber, and the similar approaches have been applied on carbon fabrics. Both desized and further treated with a reactive finish were investigated for the composite reinforcement. The effects of desizing and/or subsequent surface retreatment on carbon fiber on composite properties and performance including fiber-matrix interfacial mechanical properties, thermal properties and blistering onset behavior will be discussed in this presentation.

Allred, Ronald E.↗

NASA NTRS1978

Asteroid surface materials - Mineralogical characterizations from reflectance spectra

The use of general and specific diagnostic spectral features and parameters to interpret most of the published high-quality reflectance spectra of asteroids is discussed. Such diagnostics are shown to provide the most complete and sophisticated mineralogically and petrologically based interpretation of the asteroid surface materials. Previous investigations of asteroid surface materials are exhaustively reviewed, emphasizing the general approaches employed, sources of information, previous characterizations of asteroid surface materials, and asteroid spectral groups. The interpretive methodology is then applied to spectral reflectance data for many individual members of the various spectral groups. A range of mineral assemblages similar to certain meteorite classes is identified, and evidence is presented for a selective high-temperature event that melted certain asteroid parent bodies and permitted their differentiation as some function of distance from the sun or the protosun and of the size of the protoasteroid. Possible candidates are proposed for the source bodies of different meteorite groups.

Gaffey, M. J.↗

NASA NTRS1997

Surface Catalysis and Characterization of Proposed Candidate TPS for Access-to-Space Vehicles

Surface properties have been obtained on several classes of thermal protection systems (TPS) using data from both side-arm-reactor and arc-jet facilities. Thermochemical stability, optical properties, and coefficients for atom recombination were determined for candidate TPS proposed for single-stage-to-orbit vehicles. The systems included rigid fibrous insulations, blankets, reinforced carbon carbon, and metals. Test techniques, theories used to define arc-jet and side-arm-reactor flow, and material surface properties are described. Total hemispherical emittance and atom recombination coefficients for each candidate TPS are summarized in the form of polynomial and Arrhenius expressions.

Stewart, David A.↗

NASA NTRS2023

SelenITA: A Dual Point Lunar Mission to Characterize the Near Surface Dust and Electromagnetic Plasma Environment

SelenITA is a dual CubeSat mission that will provide the first multi-point dust, plasma, and magnetic field measurements in lunar orbit. This mission will advance the understanding of the electromagnetic space environment at the Moon in support of the Artemis program, exploration, and the geosciences. Here we present the science rationale motivating the mission. The candidate mission science objectives include: (1) constrain the origins of crustal magnetic fields; (2) determine the nature of plasma interactions with crustal magnetic fields; (3) characterize plasma waves and turbulence at the Moon; (4) characterize the lunar surface electric potential in varying plasma environments; (5) constrain the composition, thermal state, and structure of the lunar upper mantle and crust; (6) characterize the ionizing radiation in lunar orbit; and lastly, (7) determine the density of the dust exosphere as a function of latitude, longitude, and altitude, including the lunar polar space environment. The measurement requirements include simultaneous two-point observations of the 3-component vector magnetic field, plasma distribution (flux, energy, density, temperature), and single-point observations of energetic particles (protons, electrons, gamma rays), and dust. These measurements are important because it helps us understand how future astronauts, robots, and space hardware will live and work on the lunar surface.

space weather↗

NASA NTRS2023

SelenITA: A Dual Point Lunar Mission to Characterize the Near Surface Dust and Electromagnetic Plasma Environment

SelenITA is a dual CubeSat mission that will provide the first multi-point dust, plasma, and magnetic field measurements in lunar orbit. This mission will advance the understanding of the electromagnetic space environment at the Moon in support of the Artemis program, exploration, and the geosciences. Here we present the science rationale motivating the mission. The candidate mission science objectives include: (1) constrain the origins of crustal magnetic fields; (2) determine the nature of plasma interactions with crustal magnetic fields; (3) characterize plasma waves and turbulence at the Moon; (4) characterize the lunar surface electric potential in varying plasma environments; (5) constrain the composition, thermal state, and structure of the lunar upper mantle and crust; (6) characterize the ionizing radiation in lunar orbit; and lastly, (7) determine the density of the dust exosphere as a function of latitude, longitude, and altitude, including the lunar polar space environment. The measurement requirements include simultaneous two-point observations of the 3-component vector magnetic field, plasma distribution (flux, energy, density, temperature), and single-point observations of energetic particles (protons, electrons, gamma rays), and dust. These measurements are important because it helps us understand how future astronauts, robots, and space hardware will live and work on the lunar surface.

space weather↗

NASA NTRS2016

Characterization of Low Pressure Cold Plasma in the Cleaning of Contaminated Surfaces

The characterization of low pressure cold plasma is a broad topic which would benefit many different applications involving such plasma. The characterization described in this paper focuses on cold plasma used as a medium in cleaning and disinfection applications. Optical Emission Spectroscopy (OES) and Mass Spectrometry (MS) are the two analytical methods used in this paper to characterize the plasma. OES analyzes molecules in the plasma phase by displaying the light emitted by the plasma molecules on a graph of wavelength vs. intensity. OES was most useful in identifying species which may interact with other molecules in the plasma, such as atomic oxygen or hydroxide radicals. Extracting useful data from the MS is done by filtering out the peaks generated by expected molecules and looking for peaks caused by foreign ones leaving the plasma chamber. This paper describes the efforts at setting up and testing these methods in order to accurately and effectively characterize the plasma.

cold plasma characterization↗