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At least 181 records · Page 10

All sources NASA NTRS DOE OSTI

DOE OSTI2025

Microstructure, mechanical, and thermal properties of compositionally complex (Hf,Zr,Nb,Ti)B 2 ‒LaB 6 ceramics

Novel compositionally complex borides, (Hf,Zr,Nb,Ti)B 2 and (Hf,Zr,Nb,Ti)B 2 ‒LaB 6 , were fabricated using spark plasma sintering process. (Hf,Zr,Nb,Ti)B 2 ‒LaB 6 exhibits a dual-phase microstructure, in which (Hf,Zr,Nb,Ti)B 2 is a primary phase with the hexagonal structure and LaB 6 is a secondary phase with a cubic structure. The mechanical properties of both (Hf,Zr,Nb,Ti)B 2 and (Hf,Zr,Nb,Ti)B 2 ‒LaB 6 are comparable, with a combination of high hardness and moderate fracture toughness. Thermal diffusivity and conductivity of (Hf,Zr,Nb,Ti)B 2 are much lower than the individual transition metal borides but are significantly increased by the addition of LaB 6 . Herein, it is implied that the thermal properties of boride ceramics can be controlled through the appropriate design of principal metal element compositions.

borides↗

NASA NTRS1984

Advanced Gas Turbine (AGT) powertrain system development for automotive applications

Rotor dynamic instability investigations were conducted. Forward ball bearing hydraulic mount configurations were tested with little effect. Trial assembly of S/N 002 ceramic engine was initiated. Impeller design activities were completed on the straight line element (SLE) blade definition to address near-net-shape powder metal die forging. Performance characteristics of the Baseline Test 2A impeller were closely preserved. The modified blading design has been released for tooling procurement. Developmental testing of the diffusion flame combustor (DFC) for initial use in the S/N 002 2100 F ceramic structures engine was completed. A natural gas slave preheater was designed and fabricated. Preliminary regenerator static seal rig testing showed a significant reduction in leakage and sensitivity to stack height. Ceramic screening tests were completed and two complete sets of ceramic static structures were qualified for engine testing. Efforts on rotor dynamics development to resolve subsynchronous motion were continued.

Source record↗

NASA NTRS2005

Bringing Thunder and Lightning Indoors

Piezoelectric materials convert mechanical energy into electrical energy and electrical energy into mechanical energy. They generate electrical charges in response to mechanical stress and generate mechanical displacement and/or force when subjected to an electric current. Scientists at Langley Research Center have developed a piezoelectric device that is superior in many ways to those that used to be the only ones commercially available. It is tougher, has far greater displacement and greater mechanical load capacity for a comparative voltage operation, can be easily produced at a relatively low cost, and lends itself well to mass production. The NASA-developed piezoelectric device is also unique in that it is more efficient in extracting electrical energy from the mechanical energy that goes in. It works on a simple principle. A thin ceramic piezoelectric wafer is sandwiched between an aluminum sheet and a steel sheet and held together with LaRC-SI, an amorphous thermoplastic adhesive with special properties created by NASA at Langley. The sandwich is heated in an autoclave, and the adhesive melts. When the sandwich cools, the adhesive bonds the parts together into one piezoelectric element. While they cool, the components of the element contract at different rates, since they are made of different materials. This differential shrinkage causes the element to warp in either a convex or concave shape, depending on which way it is oriented. The shrinking of the outside metal layers places the inside piezoelectric ceramic under mechanical stress. If the element is cantilevered by clamping one side and then plucked, it reverberates like a diving board that has just ejected a diver. This way, a small amount of mechanical energy can result in a relatively long period of electrical generation. When the piezoelectric element is used for the creation of electricity, it is called Lightning. This same sandwiched piezoelectric wafer can also convert electrical energy into mechanical energy. Then, it is called Thunder. Electricity goes in, excites the element, and then, mechanical energy in the form of movement is generated.

Source record↗

DOE OSTI2021

Compositions and methods for thermoelectric ceramics

In one aspect, the disclosure relates to thermoelectric ceramic oxide compositions comprising a CaMnO 3 ceramic. In a further aspect, the disclosed thermoelectric ceramic oxide compositions can dramatically increase the energy conversion efficiency of thermoelectric through a combination of modifying the chemistry of precursor materials, and simultaneously introducing a metal oxide liquid phase during sintering. In a further aspect, the present disclosure pertains to thermoelectric ceramic oxide compositions comprising a metal doped CaMnO 3 having with a metal oxide grain boundary phase; wherein the metal is selected from group 13, group 14, group 15, group 16, or a rare earth element. In a still further aspect, the disclosure relates to methods for making the thermoelectric ceramic oxide materials. This abstract is intended as a scanning tool for purposes of searching in the particular art and is not intended to be limiting of the present disclosure.

Song, Xueyan↗

NASA NTRS2002

Design and Fabrication of Two-Dimensional Semiconducting Bolometer Arrays for the High Resolution Airborne Wideband Camera (HAWC) and the Submillimeter High Angular Resolution Camera II (SHARC-II)

The High resolution Airborne Wideband Camera (HAWC) and the Submillimeter High Angular Resolution Camera II (SHARC 11) will use almost identical versions of an ion-implanted silicon bolometer array developed at the National Aeronautics and Space Administration's Goddard Space Flight Center (GSFC). The GSFC "Pop-Up" Detectors (PUD's) use a unique folding technique to enable a 12 x 32-element close-packed array of bolometers with a filling factor greater than 95 percent. A kinematic Kevlar(Registered Trademark) suspension system isolates the 200 mK bolometers from the helium bath temperature, and GSFC - developed silicon bridge chips make electrical connection to the bolometers, while maintaining thermal isolation. The JFET preamps operate at 120 K. Providing good thermal heat sinking for these, and keeping their conduction and radiation from reaching the nearby bolometers, is one of the principal design challenges encountered. Another interesting challenge is the preparation of the silicon bolometers. They are manufactured in 32-element, planar rows using Micro Electro Mechanical Systems (MEMS) semiconductor etching techniques, and then cut and folded onto a ceramic bar. Optical alignment using specialized jigs ensures their uniformity and correct placement. The rows are then stacked to create the 12 x 32-element array. Engineering results from the first light run of SHARC II at the CalTech Submillimeter Observatory (CSO) are presented.

Voellmer, George M.↗

NASA NTRS2002

Design and Fabrication of Two-Dimensional Semiconducting Bolometer Arrays for the High Resolution Airborne Wideband Camera (HAWC) and the Submillimeter High Angular Resolution Camera II (SHARC-II)

The High resolution Airborne Wideband Camera (HAWC) and the Submillimeter High Angular Resolution Camera II (SHARC II) will use almost identical versions of an ion-implanted silicon bolometer array developed at the National Aeronautics and Space Administration's Goddard Space Flight Center (GSFC). The GSFC 'Pop-up' Detectors (PUD's) use a unique folding technique to enable a 12 x 32-element close-packed array of bolometers with a filling factor greater than 95 percent. A kinematic Kevlar(trademark) suspension system isolates the 200 mK bolometers from the helium bath temperature, and GSFC - developed silicon bridge chips make electrical connection to the bolometers, while maintaining thermal isolation. The JFET preamps operate at 120 K. Providing good thermal heat sinking for these, and keeping their conduction and radiation from reaching the nearby bolometers, is one of the principal design challenges encountered. Another interesting challenge is the preparation of the silicon bolometers. They are manufactured in 32-element, planar rows using Micro Electro Mechanical Systems (MEMS) semiconductor etching techniques, and then cut and folded onto a ceramic bar. Optical alignment using specialized jigs ensures their uniformity and correct placement. The rows are then stacked to create the 12 x 32-element array. Engineering results from the first light run of SHARC II at the Caltech Submillimeter Observatory (CSO) are presented.

Voellmer, George M.↗

NASA NTRS2004

A Hybrid Actuation System Demonstrating Significantly Enhanced Electromechanical Performance

A hybrid actuation system (HYBAS) utilizing advantages of a combination of electromechanical responses of an electroactive polymer (EAP), an electrostrictive copolymer, and an electroactive ceramic single crystal, PZN-PT single crystal, has been developed. The system employs the contribution of the actuation elements cooperatively and exhibits a significantly enhanced electromechanical performance compared to the performances of the device made of each constituting material, the electroactive polymer or the ceramic single crystal, individually. The theoretical modeling of the performances of the HYBAS is in good agreement with experimental observation. The consistence between the theoretical modeling and experimental test make the design concept an effective route for the development of high performance actuating devices for many applications. The theoretical modeling, fabrication of the HYBAS and the initial experimental results will be presented and discussed.

Su, Ji↗

DOE OSTI2024

A general flame aerosol route to high-entropy nanoceramics

High-entropy ceramics are an emerging class of materials with fascinating characteristics. However, elemental immiscibility and crystal complexity limit the development of a general synthesis strategy, and common methods yield bulk materials. Here, we introduce a transformative non-equilibrium flame aerosol technique for synthesizing high-entropy nanoceramics. This scalable, one-step process enables the production of high-entropy oxide nanoceramics with an unprecedented diversity of crystal structures, including fluorite-phase materials that integrate up to 22 distinct cation elements. The method’s capacity for entropic stabilization and grain refinement significantly improves the thermal stability of these nanostructures. In a representative application, a Pt-(MgCoNiCuZn)O high-entropy single-atom catalyst showed superior activity and long-term stability, maintaining constant CO 2 conversion over 670 h and dramatically outperforming conventional catalysts. Finally, the general approach opens a vast composition and structure space for the creation of high-entropy oxide nanomaterials for application across diverse fields, including catalysis, energy storage, sensing, and thermal management.

36 MATERIALS SCIENCE↗

NASA NTRS1997

Dynamic Analysis of a Two Member Manipulator

Attenuating start-up and stopping vibrations when maneuvering large payloads attached to flexible manipulator systems is a great concern for many space missions. To address this concern, it was proposed that the use of smart materials, and their applications in smart structures, may provide an effective method of control for aerospace structures. In this paper, a modified finite element model has been developed to simulate the performance of piezoelectric ceramic actuators, and was applied to a flexible two-arm manipulator system. Connected to a control voltage, the piezoelectric actuators produce control moments based on the optimal control theory. The computer simulation modeled the end-effector vibration suppression of the NASA manipulator testbed for berthing operations of the Space Shuttle to the Space Station. The results of the simulation show that the bonded piezoelectric actuators can effectively suppress follow-up vibrations of the end-effector, stimulated by some external disturbance.

McGinley, W. Mark↗

NASA NTRS1997

Dynamic Analysis of a Two Member Manipulator Arm

McGinley, Mark↗

DOE OSTI2021

Nanoscale microstructure and chemistry of transparent gahnite glass-ceramics revealed by atom probe tomography

The nanoscale microstructure and chemistry of a transparent gahnite glass-ceramic and its precursor glass were investigated using atom probe tomography, transmission electron microscopy, and nuclear magnetic resonance spectroscopy. In the annealed precursor glass, statistically significant ZrO clustering was observed along with Si depletion within 2 nm of the ZrO clusters. This clustering is expected to be the first step in the nucleation and crystallization of the nucleating agent, ZrO 2 . In the glass-ceramic, gahnite (ZnAl 2 O 4 ) crystallites were found to exist in proximal locations to ZrO 2 and not in a core-shell arrangement. The residual glass composition was directly measured by atom probe, showing higher concentrations of Al, Zn, and Zr than previously expected. At the interfaces between the crystallites and residual glass, no enrichment or depletion zones were found. Our findings provide answers to outstanding questions surrounding the nucleation and elemental partitioning, microstructure, and the residual glass composition of transparent gahnite glass-ceramics.

36 MATERIALS SCIENCE↗

NASA NTRS2017

Multi-Functional BN-BN Composite

Multifunctional Boron Nitride nanotube-Boron Nitride (BN-BN) nanocomposites for energy transducers, thermal conductors, anti-penetrator/wear resistance coatings, and radiation hardened materials for harsh environments. An all boron-nitride structured BN-BN composite is synthesized. A boron nitride containing precursor is synthesized, then mixed with boron nitride nanotubes (BNNTs) to produce a composite solution which is used to make green bodies of different forms including, for example, fibers, mats, films, and plates. The green bodies are pyrolized to facilitate transformation into BN-BN composite ceramics. The pyrolysis temperature, pressure, atmosphere and time are controlled to produce a desired BN crystalline structure. The wholly BN structured materials exhibit excellent thermal stability, high thermal conductivity, piezoelectricity as well as enhanced toughness, hardness, and radiation shielding properties. By substituting with other elements into the original structure of the nanotubes and/or matrix, new nanocomposites (i.e., BCN, BCSiN ceramics) which possess excellent hardness, tailored photonic bandgap and photoluminescence, result.

Kang, Jin Ho↗

NASA NTRS2014

Development and Testing of a Refractory Millimeter-Wave Absorbent Heat Exchanger

Central to the Millimeter-Wave Thermal Launch System (MTLS) is the millimeter-wave absorbent heat exchanger. We have developed metallic and ceramic variants, with the key challenge being the millimeter-wave absorbent coatings for each. The ceramic heat exchanger came to fruition first, demonstrating for the first time 1800 K peak surface temperatures under illumination by a 110 GHz Gaussian beam. Absorption efficiencies of up to 80 are calculated for mullite heat exchanger tubes and up to 50 are calculated for alumina tubes. These are compared with estimates based on stratified layer and finite element analyses. The problem of how to connect the 1800 K end of the ceramic tubes to a graphite outlet manifold and nozzle is solved by press fitting, or by threading the ends of the ceramic tubes and screwing them into place. The problem of how to connect the ceramic tubes to a metallic or nylon inlet pipe is solved by using soft compliant PTFE and PVC tubes that accommodate thermal deformations of the ceramic tubes during startup and operation. We show the resulting heat exchangers in static tests using argon and helium as propellants.

propulsion↗

DOE OSTI2026

INL CRMO XRF Special Report No. 3: INL CRMO XRF Calibration Methods for the Analysis of Ceramics and Brick

This report details the analytical methods used by the Idaho National Laboratory Cultural Resource Management Office to characterize ceramic and brick artifacts using X-ray fluorescence spectrometry. More specifically, this report provides details on instrumentation, analysis times, and matrix-specific calibration protocols for ceramic materials. Calibration curves were developed to adjust raw instrumental output for 13 elements using a suite of reference standards made from historic brick borrowed from the Yale Peabody Museum. Calibration curves were validated by plotting predicted values against published reference values for the calibration set as well as a certified soil reference standard (SRM 2711a).

36 MATERIALS SCIENCE↗

DOE OSTI2023

Protecting People and Planet

To produce energy, civilian nuclear power plants require fuel. The majority of existing plants rely on solid ceramic fuels that contain concentrations of about 3 to 5% of the element uranium-235. This specific isotope is well suited to sustaining the type of chain reaction required for a nuclear reactor to harness the heat produced by nuclear fission. Title I of the United States Atomic Energy Act of 1954 defines “special nuclear material” as plutonium, uranium-233, or uranium enriched in the isotopes uranium-233 or uranium-235. This label identifies materials that at high concentrations can be used to produce nuclear weapons. The United States and broader international community are fully committed to ensuring the peaceful use of nuclear energy by committing to practices known as safeguards.

99 GENERAL AND MISCELLANEOUS↗

NASA NTRS1972

Investigation of biowaste resistojets for space station application

The feasibility of using electrically conducting ceramics to heat biowaste propellants to 2000 K in resistojet thrustors was demonstrated. These thrustors are being developed for use on the space station. Among the candidate ceramic heater materials, zirconia and thoria are chemically resistant to the biopropellants, and they are also sufficiently conductive at high temperatures to make them suitable for the heater elements in these thrustors. A proof of concept thrustor design is presented, incorporating a multiple passage cylindrical heater made of zirconia ceramic which is capable of operating at 2000 K wall temperature with CO2 and H2O biopropellants. For the 25 mlb size thrustor, specific impulses of 200 seconds for CO2 and 275 seconds for H2O biopropellants are predicted.

Halbach, C. R.↗

NASA NTRS1985

Thermal stress analysis of a new turbine shroud seal concept

The thermal stress field of a two piece turbine shroud seal concept was analyzed and results compared to one piece designs by finite element analysis. The two piece seal has independently formed structure (substrate) and ceramic components that are assembled at ambient conditions. The boundary conditions used for analysis were hot gas surface temperatures of 1370 and 1650 C (2500 and 3000 F) and cooled surface temperature of 700 C (1285 F). The resulting thermal stress field, of the two piece seal when compared to the one piece seals in the region of all ceramic material, was reduced substantially.

Handschuh, R. F.↗

NASA NTRS1985

Design of a flight qualified long-life cryocooler

A second generation Stirling cycle cryogenic refrigerator with a linear drive, magnetic bearings, and clearance seals; designed to produce 5 watts of cooling at 65 Kelvin and to meet Space Shuttle mission requirements is described. The first generation refrigerator met all performance specifications, and operated with no failure for over 12,030 hours. Meeting launch requirements necessitated improvements in the electromagnetic bearings, the radial position sensors, and in the structural design of the moving elements. Organic contamination was eliminated by the use of all metal and ceramic construction. Reductions in system input power are attained by an integral magnetic spring/motor for the displacer and by more efficient linear motors and drive electronics.

Knox, L.↗