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At least 181 records · Page 10

All sources NASA NTRS DOE OSTI

DOE OSTI2018

Equilibrium Properties of the Mixed State in Superconducting Niobium in a Transverse Magnetic Field: Experiment and Theoretical Model

Equilibrium magnetic properties of the mixed state in type II superconductors were studied on high-purity film and single-crystal niobium samples with different Ginzburg-Landau parameters in perpendicular and parallel magnetic fields using dc magnetometry and scanning Hall-probe microscopy. The magnetization curve for samples with unity demagnetizing factor (slabs in perpendicular field) was obtained for the first time. It was found that none of the existing theories is consistent with these new data. To address this problem, a theoretical model is developed and comprehensively validated. The new model describes the mixed state in an averaged limit, i.e., without detailing the samples’ magnetic structure and therefore ignoring the surface current and interactions between the structural units (vortices). At low values of the Ginzburg-Landau parameter, it converts to the model of Peierls and London for the intermediate state in type I superconductors. The model quantitatively describes the magnetization curve for the perpendicular field and provides new insights into the properties of the mixed state, including properties of individual vortices. In particular, it suggests that description of the vortex matter in superconductors of the transverse geometry as a “gas-like” system of non-interacting vortices is more appropriate than the frequently used solid-like scenarios.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2018

Calculation of AC Magnetizing Loss of ReBCO Superconducting Tapes Subjected to Applied Distorted Magnetic Fields

In recent years, there are fast-increasing concerns on the utilizations of superconducting rotating electrical machines in different application areas, such as ship propulsion systems, aircraft drivers, and wind turbine generators, since these machines exhibit the merits of high current density, compact design, high power density, light weight, high torque density as well as high efficiency. One of the main limitations in front of the vast use of superconducting tapes in the fabrication of electrical machineries is AC magnetizing loss when tapes are exposed to an external magnetic field, which can decrease the critical current density of wires, as well. In the literature, most of the research works have been done on calculation of the AC magnetizing loss under a pure external magnetic field, while in reality, magnetic flux lines in AC electrical machines are usually distorted with harmonics because of different reasons such as distorted leakage flux, distributed coils of a winding in several slots, cogging fields, mechanical faults, etc. Since these distorted fields contain harmonics, then in this paper, the AC magnetizing loss of superconducting tapes has been electromagnetically modeled and calculated when they are subjected to nonsinusoidally distorted external magnetic fields. The magnetic field dependency of critical current density has been considered in a proposed finite element model. The results have shown that the AC magnetizing loss increases significantly under a distorted applied field compared with a sinusoidal one. In addition, the loss increase depends on the harmonic content which would increases drastically with total harmonic distortion of the applied magnetic field.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2016

Tolerance analyses of a quadrupole magnet for advanced photon source upgrade

Given physics requirements, the mechanical fabrication and assembly tolerances for storage ring magnets can be calculated using analytical methods [1, 2]. However, this method is not easy for complicated magnet designs [1]. In this paper, a novel method is proposed to determine fabrication and assembly tolerances consistent with physics requirements, through a combination of magnetic and mechanical tolerance analyses. In this study, finite element analysis using OPERA is conducted to estimate the effect of fabrication and assembly errors on the magnetic field of a quadrupole magnet and to determine the allowable tolerances to achieve the specified magnetic performances. Based on the study, allowable fabrication and assembly tolerances for the quadrupole assembly are specified for the mechanical design of the quadrupole magnet. Next, to achieve the required assembly level tolerances, mechanical tolerance stackup analyses using a 3D tolerance analysis package are carried out to determine the part and subassembly level fabrication tolerances. This method can be used to determine the tolerances for design of other individual magnets and of magnet strings.

43 PARTICLE ACCELERATORS↗

DOE OSTI2022

Spontaneous Asymmetry of Chiral Magnetic Domains Within a Magnetic Field

Abstract Chiral magnetic domains are topological spin textures in which the Dzyaloshinskii–Moriya interaction assigns a given chirality to the domain walls. Notably, despite rapid progress in chiral magnetic research, one fundamental issue that remains unclear is how the chirality of chiral magnetic domains change as a magnetic field deforms the spin texture. Using spin‐polarized low energy electron microscopy, the evolution of Fe/Ni chiral magnetic stripe domains are investigated in single‐crystalline Fe/Ni/Cu/Co/Cu(001) multilayers in which the interlayer magnetic coupling between the Co and Fe/Ni films serves as an in‐plane magnetic field. Contrary to theoretical works, it is found that the chirality of the Néel walls results in a parallel alignment of the magnetic stripes with the in‐plane magnetic field direction. The transformation of chiral Néel walls into achiral Bloch walls can be precisely controlled by tuning the Cu spacer layer thickness. In addition, the domain wall exhibits a spontaneous asymmetry within the in‐plane magnetic field, leading to an unbalanced chirality between the left‐handed and right‐handed Bloch walls. These new results foster a better understanding of the chiral domain properties within a magnetic field.

Li, Qian↗

DOE OSTI2022

The role of microstructural evolution during spark plasma sintering on the soft magnetic and electronic properties of a CoFe–Al2O3 soft magnetic composite

Abstract For transformers and inductors to meet the world’s growing demand for electrical power, more efficient soft magnetic materials with high saturation magnetic polarization and high electrical resistivity are needed. This work aimed at the development of a soft magnetic composite synthesized via spark plasma sintering with both high saturation magnetic polarization and high electrical resistivity for efficient soft magnetic cores. CoFe powder particles coated with an insulating layer of Al 2 O 3 were used as feedstock material to improve the electrical resistivity while retaining high saturation magnetic polarization. By maintaining a continuous non-magnetic Al 2 O 3 phase throughout the material, both a high saturation magnetic polarization, above 1.5 T, and high electrical resistivity, above 100 μΩ·m, were achieved. Through microstructural characterization of samples consolidated at various temperatures, the role of microstructural evolution on the magnetic and electronic properties of the composite was elucidated. Upon consolidation at relatively high temperature, the CoFe was to found plastically deform and flow into the Al 2 O 3 phase at the particle boundaries and this phenomenon was attributed to low resistivity in the composite. In contrast, at lower consolidation temperatures, perforation of the Al 2 O 3 phase was not observed and a high electrical resistivity was achieved, while maintaining a high magnetic polarization, ideal for more efficient soft magnetic materials for transformers and inductors.

36 MATERIALS SCIENCE↗

DOE OSTI2019

Magnetic Ground State Crossover in a Series of Glaserite Systems with Triangular Magnetic Lattices

The magnetic properties are reported for three members of the glaserite series of compounds, Na 2 BaM(VO 4 ) 2 , M = Mn, Mn 0.6 Co 0.4 , and Co. Large single crystals are grown using a high-temperature hydrothermal synthesis method. This structure type exhibits a triangular magnetic lattice in which M 2+ O 6 octahedra are interconnected with nonmagnetic (VO 4 ) 3– groups. All the structures crystallize at room temperature with rigid trigonal symmetry (space group $P\bar{3m}1$); however, at lower temperatures both Na 2 BaMn(VO 4 ) 2 and Na 2 BaMn 0.6 Co 0.4 (VO 4 ) 2 undergo a structural transition to lower symmetry (monoclinic, C2/c). The bulk magnetic measurements indicate that Mn- and Co-structures are antiferromagnetic and ferromagnetic, respectively. Na 2 BaMn 0.6 Co 0.4 (VO 4 ) 2 does not show any long-range ordering down to 0.5 K, although a broad heat capacity anomaly near 1.2 K suggests short-range magnetic order or freezing into a spin-glass-like state related to the chemical disorder and resulting competing magnetic interactions. The magnetic structures of Na 2 BaMn(VO 4 ) 2 and Na 2 BaCo(VO 4 ) 2 were determined using neutron powder diffraction. At zero magnetic field, Na 2 BaMn(VO 4 ) 2 possesses an antiferromagnetic structure with the moments ordered in a Néel-type arrangement and aligned along the C 4 axis of the octahedra. Under applied magnetic field at 0.3 K, the evolution of the magnetic structure toward a fully polarized state is observed. Na 2 BaCo(VO 4 ) 2 represents a ferromagnetic (FM) magnetic structure with Co moments aligned parallel to the c-axis direction. Finally, the relationships between these structures and magnetic properties are discussed.

36 MATERIALS SCIENCE↗

DOE OSTI2017

Measurement of magnetic field fluctuations and diamagnetic currents within a laser ablation plasma interacting with an axial magnetic field

Here, the guiding of laser ablation plasmas with axial magnetic fields has been used for many applications, since its effectiveness has been proven empirically. For more sophisticated and complicated manipulations of the plasma flow, the behavior of the magnetic field during the interaction and the induced diamagnetic current in the plasma plume needs to be clearly understood. To achieve the first milestone for establishing magnetic plasma manipulation, we measured the spatial and temporal fluctuations of the magnetic field caused by the diamagnetic current. We showed that the small fluctuations of the magnetic field can be detected by using a simple magnetic probe. We observed that the field penetrates to the core of the plasma plume. The diamagnetic current estimated from the magnetic field had temporal and spatial distributions which were confirmed to be correlated with the transformation of the plasma plume. Our results show that the measurement by the magnetic probe is an effective method to observe the temporal and spatial distributions of the magnetic field and diamagnetic current. The systematic measurement of the magnetic field variations is a valuable method to establish the magnetic field manipulation of the laser ablation plasma.

43 PARTICLE ACCELERATORS↗

DOE OSTI2019

Creation of nanoscale magnetic fields using nano-magnet arrays

In this paper, we present the fabrication of nano-magnet arrays, comprised of two sets of interleaving SmCo 5 and Co nano-magnets, and the subsequent development and implementation of a protocol to program the array to create a one-dimensional rotating magnetic field. We designed the array based on the microstructural and magnetic properties of SmCo 5 films annealed under different conditions, also presented here. Leveraging the extremely high contrast in coercivity between SmCo 5 and Co, we applied a sequence of external magnetic fields to program the nano-magnet arrays into a configuration with alternating polarization, which based on simulations creates a rotating magnetic field in the vicinity of nano-magnets. Our proof-of-concept demonstration shows that complex, nanoscale magnetic fields can be synthesized through coercivity contrast of constituent magnetic materials and carefully designed sequences of programming magnetic fields.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

DOE OSTI2020

Cooperative response of magnetism and superconductivity in the magnetic superconductor RbEuFe 4 As 4

Herein, we present a study of the magnetic-flux evolution in the magnetic superconductor RbEuFe 4 As 4 performed using magneto-optical imaging and magnetization measurements during field cooling and warming and magnetic field cycling at temperatures above and below the magnetic transition point, T$_m$. The vortex patterns emerging at T ≲ T$_m$ reveal that the Eu-spin subsystem serves as an internal pump of the magnetic flux while the superconducting critical current controls the delivery of magnetic-flux quanta into the bulk. The interplay of magnetic susceptibility amplifying the magnetic induction and vortex pinning attenuating the magnetic-flux entry results in a field- and temperature-dependent critical state that emulates a paramagnetic Meissner effect. The observed vortex dynamics corresponds to a nontrivial spatial current distribution and yields a self-consistent inhomogeneous enhancement of the sample magnetization.

36 MATERIALS SCIENCE↗

DOE OSTI2017

Magnetic Measurements of Storage Ring Magnets for the APS Upgrade Project

Extensive prototyping of storage ring magnets is ongoing at the Advanced Photon Source (APS) in support of the APS Multi-Bend Achromat (MBA) upgrade project (APS-U) [1]. As part of the R&D activities four quadrupole magnets with slightly different geometries and pole tip materials, and one sextupole magnet with vanadium permendur (VP) pole tips were designed, built and tested. Magnets were measured individually using a rotating coil and a Hall probe for detailed mapping of the magnetic field. Magnets were then assembled and aligned relative to each other on a steel support plate and concrete plinth using precision machined surfaces to gain experience with the alignment method chosen for the APS-U storage ring magnets. The required alignment of magnets on a common support structure is 30 μm rms. Measurements of magnetic field quality, strength and magnet alignment after subjecting the magnets and assemblies to different tests are presented.

Doose, C.↗

DOE OSTI2020

Laminated magnetic materials for on-chip magnetic inductors/transformers

A technique relates to a method of forming a laminated multilayer magnetic structure. An adhesion layer is deposited on a substrate. A magnetic seed layer is deposited on top of the adhesion layer. Magnetic layers and non-magnetic spacer layers are alternatingly deposited such that an even number of the magnetic layers is deposited while an odd number of the non-magnetic spacer layers is deposited. The odd number is one less than the even number. Every two of the magnetic layers is separated by one of the non-magnetic spacer layers. The first of the magnetic layers is deposited on the magnetic seed layer, and the magnetic layers each have a thickness less than 500 nanometers.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Laminated magnetic materials for on-chip magnetic inductors/transformers

36 MATERIALS SCIENCE↗

DOE OSTI2022

Superconducting Magnet System Concept with a Mechanical Energy Transfer in the Magnetic Field

There is an interest to design superconducting magnet systems working in a persistent current mode. These systems continuously generate magnetic field with disconnected power source working like permanent magnet devices. In this paper proposed a magnet system concept based on the direct mechanical energy transfer in the magnetic field. Short circuited superconducting coils do not have current leads and power source. To pump the mechanical energy in the superconducting coil used a magnetizer which magnetically coupled with the coil. The mechanical removing the magnetizer from the magnet induces a persistent current in the superconducting coil which generates the magnetic field. Iron dominated magnet system concept was investigated using OPERA3d code which confirmed a visibility of proposed approach.

43 PARTICLE ACCELERATORS↗

DOE OSTI2015

Oxygen trapped by rare earth tetrahedral clusters in Nd{sub 4}FeOS{sub 6}: Crystal structure, electronic structure, and magnetic properties

Single crystals of Nd{sub 4}FeOS{sub 6} were grown from an Fe–S eutectic solution. Single crystal X-ray diffraction analysis revealed a Nd{sub 4}MnOSe{sub 6}-type structure (P6{sub 3}mc, a=9.2693(1) Å, c=6.6650(1)Å, V=495.94(1) Å{sup 3}, Z=2), featuring parallel chains of face-sharing [FeS{sub 6×1/2}]{sup 4−} trigonal antiprisms and interlinked [Nd{sub 4}OS{sub 3}]{sup 4+} cubane-like clusters. Oxygen atoms were found to be trapped by Nd{sub 4} clusters in the [Nd{sub 4}OS{sub 3}]{sup 4{sub +}} chains. Structural differences among Nd{sub 4}MnOSe{sub 6}-type Nd{sub 4}FeOS{sub 6} and the related La{sub 3}CuSiS{sub 7}− and Pr{sub 8}CoGa{sub 3}-type structures have been described. Magnetic susceptibility measurements on Nd{sub 4}FeOS{sub 6} suggested the dominance of antiferromagnetic interactions at low temperature, but no magnetic ordering down to 2 K was observed. Spin-polarized electronic structure calculations revealed magnetic frustration with dominant antiferromagnetic interactions. - Graphical abstract: Trapping of oxygen in Nd{sub 4} tetrahedral clusters results in the formation of the Nd{sub 4}MnOSe{sub 6}-type Nd{sub 4}FeOS{sub 6}, in contrast to the La{sub 3}CuSiS{sub 7}-type oxygen-free Nd{sub 4}FeS{sub 7} and related Pr{sub 8}CoGa{sub 3}-type structures. Complex magnetic frustration inhibits magnetic ordering at low temperature. - Highlights: • Single crystals of Nd{sub 4}FeOS{sub 6} were grown using self-flux method. • Oxygen was found trapped by Nd{sub 4} tetrahedral clusters. • Comparison with two closely related structural types were discussed. • Magnetic measurements revealed antiferromagnetic (AFM) interaction. • VASP calculations confirmed strong magnetic frustration in AFM model.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2018

Relationship between laser energy input, microstructures and magnetic properties of selective laser melted Fe-6.9%wt Si soft magnets

Highlights: • Effect of laser energy input on magnetic properties of SLM Fe-6.9%wt.Si is described; • Magnetic properties can be described as function of as-built microstructure after stress-relief post-treatment; • Samples with density >99% and strong crystallographic texture along BD have the best magnetic properties; • At very high laser energy, a strong cube texture forms that deteriorates the magnetic properties. - Abstract: Selective Laser Melting (SLM), a powder-bed Additive Manufacturing technology, can be used in combination with high temperature post-annealing to produce high-silicon steel parts characterised by quasi-static magnetic properties comparable to those of commercial electrical steel. However, the role of the as-built microstructure on the magnetic properties is still unexplored. Therefore, in this study the effect of the energy input of the processing laser on the magnetic properties of the material is investigated. The magnetic properties are determined for 4 mm-high rings obtained using three laser energy input values that provide a good compromise in terms of porosity and crack formation. The best magnetic properties are obtained for the rings built using a value of energy input that produces a strong fibrous crystallographic texture, in which one of the crystallographic <001> axes is preferentially aligned along the build direction. Whether the magnetic properties change with sample direction as a result of the crystallographic texture will be the subject of future research.

36 MATERIALS SCIENCE↗

DOE OSTI2021

Magnetic Texture in Insulating Single Crystal High Entropy Oxide Spinel Films

Magnetic insulators are important materials for a range of next-generation memory and spintronic applications. Structural constraints in this class of devices generally require a clean heterointerface that allows effective magnetic coupling between the insulating layer and the conducting layer. However, there are relatively few examples of magnetic insulators that can be synthesized with surface qualities that would allow these smooth interfaces and precisely tuned interfacial magnetic exchange coupling, which might be applicable at room temperature. In this work, we demonstrate an example of how the configurational complexity in the magnetic insulator layer can be used to realize these properties. The entropy-assisted synthesis is used to create single-crystal (Mg 0.2 Ni 0.2 Fe 0.2 Co 0.2 Cu 0.2 )Fe 2 O 4 films on substrates spanning a range of strain states. These films show smooth surfaces, high resistivity, and strong magnetic responses at room temperature. Furthermore, local and global magnetic measurements further demonstrate how strain can be used to manipulate the magnetic texture and anisotropy. These findings provide insight into how precise magnetic responses can be designed using compositionally complex materials that may find application in next-generation magnetic devices.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2015

Magnetic tweezers with high permeability electromagnets for fast actuation of magnetic beads

As a powerful and versatile scientific instrument, magnetic tweezers have been widely used in biophysical research areas, such as mechanical cell properties and single molecule manipulation. If one wants to steer bead position, the nonlinearity of magnetic properties and the strong position dependence of the magnetic field in most magnetic tweezers lead to quite a challenge in their control. In this article, we report multi-pole electromagnetic tweezers with high permeability cores yielding high force output, good maneuverability, and flexible design. For modeling, we adopted a piece-wise linear dependence of magnetization on field to characterize the magnetic beads. We implemented a bi-linear interpolation of magnetic field in the work space, based on a lookup table obtained from finite element simulation. The electronics and software were custom-made to achieve high performance. In addition, the effects of dimension and defect on structure of magnetic tips also were inspected. In a workspace with size of 0.1 × 0.1 mm{sup 2}, a force of up to 400 pN can be applied on a 2.8 μm superparamagnetic bead in any direction within the plane. Because the magnetic particle is always pulled towards a tip, the pulling forces from the pole tips have to be well balanced in order to achieve control of the particle’s position. Active video tracking based feedback control is implemented, which is able to work at a speed of up to 1 kHz, yielding good maneuverability of the magnetic beads.

36 MATERIALS SCIENCE↗

DOE OSTI2016

Alternate current magnetic property characterization of nonstoichiometric zinc ferrite nanocrystals for inductor fabrication via a solution based process

We investigate the ac magnetic behavior of solution processable, non-stoichiometric zinc ferrite nanocrystals with a series of sizes and zinc concentrations. Nearly monodisperse Zn{sub x}Fe{sub 3−x}O{sub 4} nanocrystals (x = 0–0.25) with an average size ranging from 7.4 nm to 13.8 nm are synthesized by using a solvothermal method. All the nanocrystals are in a superparamagnetic state at 300 K, which is confirmed by Superconductive Quantum Interference Device magnetometry. Due to the doping of non-magnetic Zn{sup 2+} into A site of ferrite, the saturation magnetization of nanocrystals increases as the size and Zn concentration increases. The ac magnetic permeability measurements at radio frequencies reveal that the real part of the magnetic permeability of similarly sized ferrite nanocrystals can be enhanced by almost twofold as the Zn{sup 2+} doping level increases from 0 to 0.25. The integration of 12.3 nm Zn{sub 0.25}Fe{sub 2.75}O{sub 4} nanocrystals into a toroidal inductor and a solenoid inductor prepared via a simple solution cast process yields a higher quality factors than air core inductors with the same geometries up to 5 MHz and 9 MHz, respectively, which is in the regime of the switching frequencies for the advanced integrated power converters.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗