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At least 181 records · Page 10

All sources NASA NTRS DOE OSTI

NASA NTRS2010

The Effect of Composition on the Surface Finish of PS400: A New High Temperature Solid Lubricant Coating

A new composite, multi-constituent, solid lubricant coating, NASA PS400, developed for high temperature tribological applications, exhibits a smoother surface finish after grinding and polishing than its predecessors PS200 and PS300. In this paper, the baseline composition of PS400 is modified to investigate each individual constituent s role on the achievable surface finish through a series of coating deposition, grinding, and polishing experiments. Furthermore, to explore the limits of compositional tailoring for improved tribological performance, several PS400 coatings were doped with additional solid lubricants (graphite, MoS2 and BN) and tribologically tested. The test results clearly showed that, compared to PS300 coatings, PS400 achieves a smoother surface finish via a reduced lubricant content. Coatings prepared with higher than the baseline level (10 wt%) of lubricants exhibited higher final surface roughness than the earlier generation PS300 coatings. Reducing or eliminating the one or both lubricants (fluorides or silver) did not further improve the surface finish suggesting that the current composition of PS400 is near optimal with respect to surface finish. Lastly, attempts to improve the poor initial room temperature tribological behavior of PS400 via the addition of traditional solid lubricants were unsuccessful. Based upon this work and earlier results it is expected that future research will concentrate on developing methods to produce a lubricious glaze on the rubbing surface during break in to ensure that low friction and wear are rapidly achieved.

DellaCorte, Christopher↗

NASA NTRS2016

Pulsed Plasma Lubrication Device and Method

Disclosed herein is a lubrication device comprising a solid lubricant disposed between and in contact with a first electrode and a second electrode dimensioned and arranged such that application of an electric potential between the first electrode and the second electrode sufficient to produce an electric arc between the first electrode and the second electrode to produce a plasma in an ambient atmosphere at an ambient pressure which vaporizes at least a portion of the solid lubricant to produce a vapor stream comprising the solid lubricant. Methods to lubricate a surface utilizing the lubrication device in-situ are also disclosed.

Hofer, Richard R.↗

DOE OSTI2018

Slippery self-lubricating polymer surfaces

The present disclosure describes a strategy to create self-healing, slippery self-lubricating polymers. Lubricating liquids with affinities to polymers can be utilized to get absorbed within the polymer and form a lubricant layer (of the lubricating liquid) on the polymer. The lubricant layer can repel a wide range of materials, including simple and complex fluids (water, hydrocarbons, crude oil and bodily fluids), restore liquid-repellency after physical damage, and resist ice, microorganisms and insects adhesion. Some exemplary applications where self-lubricating polymers will be useful include energy-efficient, friction-reduction fluid handling and transportation, medical devices, anti-icing, optical sensing, and as self-cleaning, and anti-fouling materials operating in extreme environments.

36 MATERIALS SCIENCE↗

DOE OSTI2021

Slippery self-lubricating polymer surfaces

Aizenberg, Joanna↗

NASA NTRS1950

Rise of Air Bubbles in Aircraft Lubricating Oils

Lubricating and antifoaming additives in aircraft lubricating oils may impede the escape of small bubbles from the oil by forming shells of liquid with a quasi-solid or gel structure around the bubbles. The rates of rise of small air bubbles, up to 2 millimeters in diameter, were measured at room temperature in an undoped oil, in the same oil containing foam inhibitors, and in an oil containing lubricating additives. The apparent diameter of the air bubbles was measured visually through an ocular micrometer on a traveling telescope. The bubbles in the undoped oil obeyed Stokes' Law, the rate of rise being proportional to the square of the apparent diameter and inversely proportional to the viscosity of the oil. The bubbles in the oils containing lubricating additives or foam inhibitors rose more slowly than the rate predicted by Stokes 1 Law from the apparent diameter, and the rate of rise decreased as the length of path the bubbles traveled increased. A method is derived to calculate the thickness of the liquid shell which would have to move with the bubbles in the doped oils to account for the abnoi'I!l8.lly slow velocity. The maximum thickness of this shell, calculated from the velocities observed, was equal to the bubble radius.

LUBRICATING OILS - FOAMING↗

DOE OSTI2021

Synthetic Lubricants Derived from Plastic Waste and their Tribological Performance

The energy efficiency, mechanical durability, and environmental compatibility of all moving machine components rely heavily on advanced lubricants for smooth and safe operation. Herein an alternative family of high-quality liquid (HQL) lubricants was derived by the catalytic conversion of pre- and post-consumer polyolefin waste. The plastic-derived lubricants performed comparably to synthetic base oils such as polyalphaolefins (PAOs), both with a wear scar volume (WSV) of 7.5×10 -5 mm -3 . HQLs also performed superior to petroleum-based lubricants such as Group III mineral oil with a WSV of 1.7×10 -4 mm -3 , showcasing a 44% reduction in wear. Furthermore, a synergistic reduction in friction and wear was observed when combining the upcycled plastic lubricant with synthetic oils. Additionally, life cycle and techno-economic analyses also showed this process to be energetically efficient and economically feasible. This novel technology offers a cost-effective opportunity to reduce the harmful environmental impact of plastic waste on our planet and to save energy through reduction of friction and wear-related degradations in transportation applications akin to synthetic oils.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2017

Tribological performance of quaternary CrSiCN coatings under dry and lubricated conditions

This paper presents an experimental study of friction and wear performance of quaternary CrSiCN coatings deposited on a hardened H-13 steel substrate by a plasma enhanced magnetron sputtering (PEMS) technique. Friction and wear tests were conducted with a reciprocating line contact between a hardened 4370 steel roller and coated and uncoated flat specimens under dry and lubricated conditions. The effects of coating thickness (1, 3.5 and 7.5 μm) on the mechanical properties, friction and wear performance were also assessed. In dry sliding, the friction of coated surfaces was about the same as for uncoated surfaces, except for the 1-μm coating, which had higher friction. Friction for coated surfaces under lubricated contact was in general higher than for uncoated surfaces. There was no measurable wear on any of the coated surfaces, under either dry or lubricated conditions. However, wear was higher on the steel roller counterface sliding against the coated surfaces, with the amount of wear proportional to the mating coating thickness. The effectiveness of formulated lubricant additives was also modified by the coating, resulting in major effects on friction and wear behavior. Finally, this reduction in lubricant additive efficacy is due to the fact that the additives were designed and optimized for ferrous surfaces.

36 MATERIALS SCIENCE↗

DOE OSTI2017

Tribological behavior of N-doped ZnO thin films by metal organic chemical vapor deposition under lubricated contacts

N-doped ZnO thin films were deposited on 304L stainless steel through the pyrolysis of zinc acetate and ammonium acetate in different ratios at a temperature of 420 degrees C using metal organic chemical vapor deposition. Compositional and structural analyzes of the films were performed by using Rutherford backscattering spectroscopy and X-ray diffraction. The frictional behavior of the thin films and 304L stainless steel substrate was evaluated using a ball-on-flat configuration with reciprocating sliding under marginally lubricated and fully flooded conditions. Al alloy (2017) was used as ball counterface, while basestock synthetic polyalfaolefin oil (PAO10) without additives was used as lubricant. The flat and ball counterface surfaces were examined to assess the wear dimension and failure mechanism. Under marginally lubricated condition, N-doped ZnO thin films provided significant reduction in friction, whereas the films have minimal or no effect in friction under fully flooded condition. N-doped ZnO thin films showed a significant effect in protecting the ball counterface as wear volume was reduced compared with that of the substrate under the marginally lubricated condition. Under the fully flooded condition, with the exception of one of the films, the wear volume of the N-doped ZnO thin films ball reduced compared with that of the substrate. In all the ball counterfaces for N-doped ZnO thin films under both conditions, wear occurred through abrasive mechanism of various degrees or mild polishing. Thus, superfluous lubrication of N-doped ZnO thin films is not necessary to reduce friction and wear.

36 MATERIALS SCIENCE↗

DOE OSTI2014

Tribological properties of self-lubricating NiAl/Mo-based composites containing AgVO{sub 3} nanowires

Silver vanadate (AgVO{sub 3}) nanowires were synthesized by hydrothermal method and self-lubricating NiAl/Mo-AgVO{sub 3} composites were fabricated by powder metallurgy technique. The composition and microstructure of NiAl/Mo-based composites were characterized and the tribological properties were investigated from room temperature to 900 °C. The results showed that NiAl/Mo-based composites were consisted of nanocrystalline B2 ordered NiAl matrix, Al{sub 2}O{sub 3}, Mo{sub 2}C, metallic Ag and vanadium oxide phase. The appearance of metallic Ag and vanadium oxide phase can be attributed to the decomposition of AgVO{sub 3} during sintering. Wear testing results confirmed that NiAl/Mo-based composites have excellent tribological properties over a wide temperature range. For example, the friction coefficient and wear rate of NiAl/Mo-based composites containing AgVO{sub 3} were significantly lower than the composites containing only metallic Mo or AgVO{sub 3} lubricant when the temperature is above 300 °C, which can be attributed to the synergistic lubricating action of metallic Mo and AgVO{sub 3} lubricants. Furthermore, Raman results indicated that the composition on the worn surface of NiAl-based composites was self-adjusted after wear testing at different temperatures. For example, Ag{sub 3}VO{sub 4} and Fe{sub 3}O{sub 4} lubricants were responsible for the improvement of tribological properties at 500 °C, AgVO{sub 3}, Ag{sub 3}VO{sub 4} and molybdate for 700 °C, and AgVO{sub 3} and molybdate for 900 °C of NiAl-based composites with the addition of metallic Mo and AgVO{sub 3}. - Highlights: • NiAl/Mo-AgVO{sub 3} nanocomposites were prepared by mechanical alloying and sintering. • AgVO{sub 3} decomposed to metallic Ag and vanadium oxide during the sintering process. • NiAl/Mo-AgVO{sub 3} exhibited superior tribological properties at a board temperature range. • Phase composition on the worn surface was varied with temperatures. • Self-adjusted action was responsible for the improvement of tribological properties.

36 MATERIALS SCIENCE↗

DOE OSTI2017

Novel Strategies for the Production of Fuels, Lubricants, and Chemicals from Biomass

Growing concern with the environmental impact of CO 2 emissions produced by combustion of fuels derived from fossil-based carbon resources has stimulated the search for renewable sources of carbon. Much of this focus has been on the development of methods for producing transportation fuels, the major source of CO 2 emissions today, and to a lesser extent on the production of lubricants and chemicals. First-generation biofuels such as bioethanol, produced by the fermentation of sugar cane- or corn-based sugars, and biodiesel, produced by the transesterification reaction of triglycerides with alcohols to form a mixture of long-chain fatty esters, can be blended with traditional fuels in limited amounts and also arise in food versus fuel debates. Producing molecules that can be drop-in solutions for fossil-derived products used in the transportation sector allows for efficient use of the existing infrastructure and is therefore particularly interesting. In this context, the most viable source of renewable carbon is abundantly available lignocellulosic biomass, a complex mixture of lignin, hemicellulose, and cellulose. Conversion of the carbohydrate portion of biomass (hemicellulose and cellulose) to fuels requires considerable chemical restructuring of the component sugars in order to achieve the energy density and combustion properties required for transportation fuels - gasoline, diesel, and jet. A different set of constraints must be met for the conversion of biomass-sourced sugars to lubricants and chemicals. This Account describes strategies developed by us to utilize aldehydes, ketones, alcohols, furfurals, and carboxylic acids derived from C 5 and C 6 sugars, acetone-butanol-ethanol (ABE) fermentation mixtures, and various biomass-derived carboxylic acids and fatty acids to produce fuels, lubricants, and chemicals. Oxygen removal from these synthons is achieved by dehydration, decarboxylation, hydrogenolysis, and hydrodeoxygenation, whereas reactions such as aldol condensation, etherification, alkylation, and ketonization are used to build up the number of carbon atoms in the final product. In this study, we show that our strategies lead to high-octane components that can be blended into gasoline, C 9 -C 22 compounds that possess energy densities and properties required for diesel and jet fuels, and lubricants that are equivalent or superior to current synthetic lubricants. Replacing a fraction of the crude-oil-derived products with such renewable sources can mitigate the negative impact of the transportation sector on overall anthropogenic greenhouse gas (GHG) emissions and climate change potential. While ethanol is a well-known fuel additive, there is significant interest in using ethanol as a platform molecule to manufacture a variety of valuable chemicals. We show that bioethanol can be converted with high selectivity to butanol or 1,3-butadiene, providing interesting alternatives to the current production from petroleum. Finally, we report that several of the strategies developed have the potential to reduce GHG emissions by 55-80% relative to those for petroleum-based processes.

Shylesh, Sankaranarayanapillai↗

DOE OSTI2013

Next Generation Refrigeration Lubricants for Low Global Warming Potential/Low Ozone Depleting Refrigeration and Air Conditioning Systems

The goal of this project is to develop and test new synthetic lubricants that possess high compatibility with new low ozone depleting (LOD) and low global warming potential (LGWP) refrigerants and offer improved lubricity and wear protection over current lubricant technologies. The improved compatibility of the lubricants with the refrigerants, along with improved lubricating properties, will resulted in lower energy consumption and longer service life of the refrigeration systems used in residential, commercial and industrial heating, ventilating and air-conditioning (HVAC) and refrigeration equipment.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

NASA NTRS1971

The pressure and deformation profile between two colliding lubricated cylinders

The pressure and deformation profiles between two colliding lubricated cylinders are obtained by solving the coupled, time-dependent elastohydrodynamic equations with an iterative procedure. The analysis includes effects which were not considered in a previous solution, namely, the effect of the lubricant compressibility and the effect of a lubricant with composite pressure-viscosity coefficients. It is found that the local approach velocity plays an important role during final stages of normal approach. It causes the lubricant to be entrapped within the contact region; neither the pressure nor the deformation profile converges to the Hertzian profile for a dry contact. The use of a smaller pressure-viscosity coefficient at high pressures reduces the sharp pressure gradient at the center of the contact and produces a much milder variation of load with respect to the film thickness. The effect of compressibility of the lubricant is found to be relatively small.

Lee, K.↗

NASA NTRS1972

Lubricating characteristics of polyimide bonded graphite fluoride and polyimide thin films

A friction and wear life study was conducted on the use of a polyimide (PI) varnish as a binder for the solid lubricant, graphite fluoride (CF(1.1))N. Also studied were the lubricating properties of PI thin films with no solid lubricant additives. For comparison, similar experiments on PI-bonded MoS2 and burnished films of MoS2 or (CF(li))N were conducted. The best results were obtained with the PI-bonded (CF(1.1))N films. The polyimide thin films (with no solid lubricant additives) did not lubricate well at 25 C; however, when heated to 100 C, low friction and long wear lives were obtained.

Fusaro, R. L.↗

NASA NTRS1973

Friction losses in a lubricated thrust-loaded cageless angular-contract bearing

The NASA spinning torque apparatus was modified to measure the spinning torque on a cageless ball thrust bearing. Friction torque was measured for thrust loads varying from 44.5 to 403 newtons (10 to 90 lb) at speeds of 1000, 2000, and 3000 rpm. Tests were conducted with di-2-ethylhexyl sebacate and a synthetic paraffinic oil. These tests were run with either oil jet lubrication or with a thin surface film of lubricant only. An analytical model which included rolling resistance was developed and extended from previous models for spinning torque and lubricant rheology. The model was extended by the inclusion of rolling resistance. The computed values were in fair agreement with the experimental results and confirmed previous hypotheses that a thin lubricant film gives minimum bearing torque and an oil jet flow of a viscous lubricant will result in considerable rolling torque in addition to the torque due to ball spin.

Townsend, D. P.↗

NASA NTRS1973

Study of ball bearing torque under elastohydrodynamic lubrication

Spinning and rolling torques were measured in an angular-contact ball bearing with and without a cage under several lubrication regimes in a modified NASA spinning torque apparatus. Two lubricants were used, a di-2 ethylhexyl sebacate and a synthetic paraffinic oil, at shaft speeds of 1000, 2000, and 3000 rpm and bearing loads from 10 lbs to 90 lbs. An analytical model was developed from previous spinning friction models to include rolling with spinning under lubrication regimes from thin film to flooded conditions. The bearing torque values have a wide variation, under any condition of speed and load, depending on the amount of lubricant present in the bearing. The analytical model compared favorably with experimental results under several lubrication regimes.

Townsend, D. P.↗

NASA NTRS1972

Lubricating characteristics of polyimide bonded graphite fluoride and polyimide thin films.

A friction and wear life study was conducted on the use of a polyimide (PI) varnish as a binder for the solid lubricant, graphite fluoride (CF sub 1.1) sub n. Also studied were the lubricating properties of PI thin films with no solid lubricant additives. For comparison, similar experiments on PI-bonded MoS2 and burnished films of MoS2 or (CF sub 1.1) sub n were conducted. The best results were obtained with the PI-bonded (CF sub 1.1) sub n films. The polyimide thin films (with no solid lubricant additives) did not lubricate well at 25 C; however, when heated to 100 C, low friction and long wear lives were obtained.

Fusaro, R. L.↗

NASA NTRS1973

KSC lubricant testing program

A program was conducted to evaluate the performance of various lubricants in use and considered for use at Kennedy Space Center (KSC). The overall objectives of the program were to: (1) determine the lubrication characteristics and relative corrosion resistance of lubricants in use and proposed for use at KSC; (2) identify materials which may be equivalent to or better than KELF-90 and Krytox 240 AC greases; and (3) identify or develop an improved lubricating oil suitable for use in liquid oxygen (LOX) pumps at KSC. It was concluded that: (1) earth gel thickened greases are very poor corrosion preventive materials in the KSC environment; (2) Halocarbon 25-5S and Braycote 656 were suitable substiutes for KELF-90 and Krytox 240 AC respectively; and (3) none of the oils evaluated possessed the necessary inertness, lubricity, and corrosion prevention characteristics for the KSC LOX pumping systems in their present configuration.

Lockhart, B. J.↗

NASA NTRS1973

Microfog lubricant application system for advanced turbine engine components, phase 3

The wetting characteristics and deposit forming tendencies of a series of lubricants were evaluated using a microfog jet delivery system to wet a flat heated rotating disc. The performances of the nine lubricants are discussed in terms of the various testing parameters which include temperature, disc speed and lubricant gas flow rates. Also discussed are the heat transfer characteristics of two of the lubricants on that same plane disc specimen. The wetting characteristics and heat transfer characteristics of one of the lubricants on a complex disc simulating bearing geometry are also discussed.

Petrucco, R. J.↗