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At least 181 records · Page 10

Investigations into the burning-out of organic substances in the ceramic body

Pressed compacts were made of spray dried alumina containing water soluble polyvinyl alcohol or cellulose derivative binder. The burning out of organic binder on gradual heating was investigated by visual and microscopic observations of the cross section and by thermogravimetry. Burning out proceeds inward from the peripheries, gradually reducing the size of the black core, which first consists of a dark boundary layer and later turns uniformly black with a sharp boundary. A detailed mechanism of the burning out process between and within the spray dried granules is observed under the microscope. Oxygen atmosphere accelerates the burning out process.

Locher, C.↗

Bioassay, isolation and studies on the mechanism of action of neurite extension factor

The identification and purification of molecules active in promoting neurite outgrowth requires a sensitive reproducible bioassay. A quantitative bioassay was utilized to purify a neurite extension factor (NEF) based on counting the number of phase bright neurons with processes at least equal to one cell body diameter after 20 hrs. in culture is defined, serum free medium. Using a combination of heat treatment DEAE cellulose chromatography and gel filtration, an acidic protein of M sub r = 75,000 was highly purified. Upon reduction, it yields subunits of M sub r = 37,000. Purified fractions are active half maximally at 100 ng/ml in inducing neurite outgrowth in this bioassay. Currently, monoclonal antibodies to NEF are being produced. Female Balb C mice were immunized with the antigen and fusions with mouse myeloma cells will be performed to yield hybridoma cells.

Kligman, D.↗

Feasibility of producing a range of food products from a limited range of undifferenitiated major food components

This report reviews current knowledge associated with producing safe, nutritious, and acceptable foods from a limited number of source independent macronutrients. The advantages, and disadvantages, of such an approach for use by space crews are discussed. The production of macronutrients from a variety of sources is covered in detail. The sources analyzed are: wheat, soybeans, algae (3 genera), glycerol, and digested cellulose. Fabrication of food from the above macronutrient sources is discussed and particular attention is addressed to nutrition, acceptability and reliability. The processes and concepts involved in food fabrication and macronutrient production are also considered for utilization in a space environment.

Karel, M.↗

Slip casting and nitridation of silicon powder

Powdered Silicon was slip-cast with a CaSO4 x 0.5H2O mold and nitrided in a N atm. containing 0 or 5 vol. % H at 1000 to 1420 deg. To remove the castings, the modeling faces were coated successively with an aq. salt soap and powdered cellulose containing Na alginate, and thus prevented the sticking problem.

Seiko, Y.↗

Gravitropism in Leafy Dicot Stems

A polarizing research microscope with rotating stage and associated camera equipment were ordered, and techniques of fixation and preparation of specimens were perfected for studying possible changes in orientation of cellulose microfibrils in cell walls of gravistimulated dicot stems. Acid ethephon solutions or acid without ethephon caused elongation of stem tissues where they were applied; stems bent away from the side of application. Acid solutions applied to the bottom of horizontal stems greatly delayed bending. Research in tissue sensitivity changes during gravitropic bending of soybean hypocotyls while immersed in auxin and in castor bean stems is also reported.

Salisbury, F. B.↗

Measurement of low energy cosmic rays aboard Spacelab-1

In December 1983 the first Spacelab mission was launched for a duration of 10 days. Aboard was the Kiel experiment Isotopic Stack designed for measurement of heavy cosmic ray nuclei with nuclear charge equal to or greater than 3 and energies up to some 100MeV/nuc. One part of the stack was rotated in well defined steps registered by an angle encoder to receive information on impact times of the nuclei. Using this time resolving system geomagnetically forbidden particles can be detected. The chemical composition and energy spectra of mainly CNO particles are examined using a rotated 300 microns m thick CR-39 foil beneath a fixed 100 microns m thick Kodak-Cellulose Nitrate foil. About 600 sq cm have been scanned yielding nearly 100 nuclear tracks within an energy range of approximately 8 to 30 MeV/nuc. The calibration is done by means of a postflight irradiation with 410 MeV/nuc Fe-56 at Berkeley Laboratory, California, USA. Relative abundances and energy spectra are presented.

Beaujean, R.↗

A poorly graphitised carbon contaminant in studies of extraterrestrial materials

Poorly-graphitized carbon particles are formed during manufacture of sample substrates (holey carbon films) for Analytical Electron Microscopy studies of small particles. The particles form during heat treatment of cellulose acetobutyrate at about 975 C and 1050 C. In AEM studies of fine-grained carbonaceous extraterrestrial materials, these particles are easily recognized.

Rietmeijer, F. J. M.↗

Solid Surface Combustion at Reduced Gravity

The spread of a flame in the gas over the surface of a solid combustible involves in an essential way the transfer of heat from the flame to the solid fuel immediately ahead of it. This heat transfer is affected by the character of the gas phase flame, and so the phenomenon of flame spreading under reduced gravity, in which the flow is generated by gasification of the solid combustible, is apt to be different from what occurs under the Earth's normal gravitational acceleration where the flow is largely buoyancy driven. An experiment is being designed for the Middeck of the Space Shuttle to aid us in understanding the process of flame spreading in the absence of a buoyancy driven flow. A chamber approximately 0.35 cu.m. in volume is to contain either a thin sample of a cellulosic material or a thick sample of polymethyl-methacrylate and an oxidizing environment of O2 and N2. Samples will be ignited at one end, and the ensuing flame spread will be filmed. The spread rate can be determined from the films, and surface and gas-phase temperatures just above the surface will also be recorded. These data will help to clarify the mechanism of forward heat transfer in the low gravity flames.

Altenkirch, R. A.↗

Manufacture of high-density ceramic sinters

High density ceramic sinters are manufactured by coating premolded or presintered porous ceramics with a sealing material of high SiO2 porous glass or nitride glass and then sintering by hot isostatic pressing. The ceramics have excellent abrasion and corrosion resistances. Thus LC-10 (Si3N2 powder) and Y2O3-Al2O3 type sintering were mixed and molded to give a premolded porous ceramic (porosity 37%, relative bulk density 63%). The ceramic was dipped in a slurry containing high SiO2 porous glass and an alcohol solution of cellulose acetate and dried. The coated ceramic was treated in a nitrogen atmosphere and then sintered by hot isostatic pressing to give a dense ceramic sinter.

Hibata, Y.↗

Volcanic impact on stratospheric aerosol chemistry

Samples collected by the National Center for Atmospheric Research (NCAR) using the multiple-filter sampler on the U-2 were analyzed. The sampler is capable of exposing a number of 110 mm filters in sequence to ram air flow. Two types of filters, IPC cellulose and polystrene, were used, both of which have high blank levels for the trace elements determined. The levels of most trace elements in the stratosphere are so low under normal circumstances that none can be seen. Results from the eruption of Mt. St. Helens, a mystery cloud (probably volcanic in origin) in 1982, and the El Chichonal eruption in 1983 are discussed. To improve the collection of particles for chemical analysis, a new sampling system was developed for use on the U-2. The sampler consisted of an electrostatic collection of particles between 1 and 0.001 micron diameter dierectly onto electron microscopic grids, followed by a thermal precipitation for the smaller particles. The system was built and tested in the laboratory, but never flown on the U-2.

Zoller, W. H.↗

Buoyancy effects on smoldering combustion

The effect of buoyancy on the rate of spread of a concurrent smolder reaction through a porous combustible material is investigated theoretically and experimentally. In the experiments, buoyant forces are controlled by varying the density difference, and the smolder rate spread through porous alpha cellulose (0.83 void fraction) is measured as a function of the ambient air pressure. The smolder velocity is found to increase with the ambient pressure; extinction occurs when the buoyancy forces cannot overcome the drag forces, indicating that diffusion by itself cannot support the spread of a smolder reaction. Theoretical predictions are found to be in good qualitative agreement with the experimental results.

Dosanjh, S.↗

Catalytic processes for space station waste conversion

Catalytic techniques for processing waste products onboard space vehicles were evaluated. The goal of the study was the conversion of waste to carbon, wash water, oxygen and nitrogen. However, the ultimate goal is conversion to plant nutrients and other materials useful in closure of an ecological life support system for extended planetary missions. The resulting process studied involves hydrolysis at 250 C and 600 psia to break down and compact cellulose material, distillation at 100 C to remove water, coking at 450 C and atmospheric pressure, and catalytic oxidation at 450 to 600 C and atmospheric pressure. Tests were conducted with a model waste to characterize the hydrolysis and coking processes. An oxidizer reactor was sized based on automotive catalytic conversion experience. Products obtained from the hydrolysis and coking steps included a solid residue, gases, water condensate streams, and a volatile coker oil. Based on the data obtained, sufficient component sizing was performed to make a preliminary comparison of the catalytic technique with oxidation for processing waste for a six-man spacecraft. Wet oxidation seems to be the preferred technique from the standpoint of both component simplicity and power consumption.

Schoonover, M. W.↗

A review of recent activities in the NASA CELSS program

A CELSS (Controlled Ecological Life Support System) is a device that utilizes photosynthetic organisms and light energy to regenerate waste materials into oxygen and food for a crew in space. The results of studies with the CELSS program suggest that a bioregenerative life support system is a useful and effective method of regenerating consumable materials for crew sustenance. The data suggests that the operation of a CELSS in space is practical if plants can be made to behave predictably in the space environment. Much of the work centers on the biological components of the CELSS system. Ways of achieving high efficiency and long term stability of all components of the system are examined. Included are explorations of the conversion of nonedible cellulose to edible materials, nitrogen fixation by biological and chemical methods, and methods of waste processing. A description is provided of the extent to which a bioregenerative life support system can meet the constraints of the space environment, and the degree is assessed to which system efficiency and stability can be increased during the next decade.

Macelroy, R. D.↗

The Effect of Microgravity on Flame Spread over a Thin Fuel

A flame spreading over a thermally thin cellulose fuel was studied in a quiescent microgravity environment. Flame spread over two different fuel thicknesses was studied in ambient oxygen-nitrogen environments from the limiting oxygen concentration to 100 percent oxygen at 1 atm pressure. Comparative normal-gravity tests were also conducted. Gravity was found to play an important role in the mechanism of flame spread. In lower oxygen environments, the buoyant flow induced in normal gravity was found to accelerate the flame spread rate as compared to the microgravity flame spread rates. It was also found to stabilize the flame in oxidizer environments, where microgravity flames in a quiescent environment extinguish. In oxygen-rich environments, however, it was determined that gravity does not play an important role in the flame spread mechanism. Fuel thickness influences the flame spread rate in both normal gravity and microgravity. The flame spread rate varies inversely with fuel thickness in both normal gravity and in an oxygen-rich microgravity environment. In lower oxygen microgravity environments, however, the inverse relationship breaks down because finite-rate kinetics and heat losses become important. Two different extinction limits were found in microgravity for the two thicknesses of fuel. This is in contrast to the normal-gravity extinction limit, which was found to be independent of fuel thickness. In microgravity the flame is quenched because of excessive thermal losses, whereas in normal gravity the flame is extinguished by blowoff.

Olson, Sandra L.↗

A review of recent activities in the NASA CELSS program

A CELSS (Controlled Ecological Life Support System) is a device that utilizes photosynthetic organisms and light energy to regenerate waste materials into oxygen and food for a crew in space. The results of theoretical and practical studies conducted by investigators within the CELSS program suggest that a bioregenerative life support system can be a useful and effective method of regenerating consumable materials for crew sustenance. Experimental data suggests that the operation of a CELSS in space will be practical if plants can be made to behave predictably in the space environment. Much of the work currently conducted within the CELSS program centers on the biological components of the CELSS system. The work is particularly directed at ways of achieving high efficiency and long term stability of all components of the system. Included are explorations of the conversion of nonedible cellulose to edible materials, nitrogen fixation by biological and chemical methods, and methods of waste processing. It is the intent of the presentation to provide a description of the extent to which a bioregenerative life support system can meet the constraints of the space environment, and to assess the degree to which system efficiency and stability can be increased during the next decade.

Macelroy, R. D.↗

Glass Coats For Hot Isostatic Pressing

Surface voids sealed from pressurizing gas. Coating technique enables healing of surface defects by hot isostatic pressing (HIP). Internal pores readily closed by HIP, but surface voids like cracks and pores in contact with pressurizing gas not healed. Applied to casting or weldment as thick slurry of two glass powders: one melts at temperature slightly lower than used for HIP, and another melts at higher temperature. For example, powder is glass of 75 percent SiO2 and 25 percent Na2O, while other powder SiO2. Liquid component of slurry fugitive organic binder; for example, mixture of cellulose acetate and acetone. Easy to apply, separates voids from surrounding gas, would not react with metal part under treatment, and easy to remove after pressing.

Ecer, Gunes M.↗

Results of inphase axial-torsional fatigue experiments on 304 stainless steel

A series of axial-torsional, inphase, strain-controlled, low-cycle fatigue tests were performed at room temperature on tubular specimens of 304 stainless steel. The program was conducted in cooperation with the task group on multiaxial fatigue research of ASTM committee E-09. The objective was to quantify the variability in multiaxial test results among several laboratories. Only included is data which was generated at the NASA Lewis Research Center's High Temperature Fatigue and Structures Laboratory. The experimental equipment and procedures used are described. The tubular specimens were polished on the outer surface to aid in the use of a cellulose film surface replication technique for crack detection. However, cracking initiated predominantly on the internal surface for all specimens. Honing of the bore of the tubular specimens lessened but did not entirely eliminate this problem. The observed fatigue lives are compared with lives calculated from three multiaxial life models. Constants for the life prediction models were obtained from uniaxial and torsional tests performed on the same heat of material. The observed fatigue lives agreed with calculated lives to within a factor of two for all but one of the life prediction models.

Bonacuse, Peter J.↗

AVIRIS performance during the 1987 flight season: An AVIRIS project assessment and summary of the NASA-sponsored performance evaluation

Results are presented of the assessment of AVIRIS performance during the 1987 flight season by the AVIRIS project and the earth scientists who were chartered by NASA to conduct an independent data quality and sensor performance evaluation. The AVIRIS evaluation program began in late June 1987 with the sensor meeting most of its design requirements except for signal-to-noise ratio in the fourth spectrometer, which was about half of the required level. Several events related to parts failures and design flaws further reduced sensor performance over the flight season. Substantial agreement was found between the assessments by the project and the independent investigators of the effects of these various factors. A summary of the engineering work that is being done to raise AVIRIS performance to its required level is given. In spite of degrading data quality over the flight season, several exciting scientific results were obtained from the data. These include the mapping of the spatial variation of atmospheric precipitable water, detection of environmentally-induced shifts in the spectral red edge of stressed vegetation, detection of spectral features related to pigment, leaf water and ligno-cellulose absorptions in plants, and the identification of many diagnostic mineral absorption features in a variety of geological settings.

Vane, Gregg↗