DOE OSTI · 2584545
Radiation Damage Mitigation in FeCrAl Alloy at Sub-Recrystallization Temperatures
Abstract
Traditional defect recovery methods rely on high-temperature annealing, often exceeding 750 °C for FeCrAl. In this study, we introduce electron wind force (EWF)-assisted annealing as an alternative approach to mitigate irradiation-induced defects at significantly lower temperatures. FeCrAl samples irradiated with 5 MeV Zr 2+ ions at a dose of 10 14 cm −2 were annealed using EWF at 250 °C for 60 s. We demonstrate a remarkable transformation in the irradiated microstructure, where significant increases in kernel average misorientation (KAM) and low-angle grain boundaries (LAGBs) typically indicate heightened defect density; the use of EWF annealing reversed these effects. X-ray diffraction (XRD) confirmed these findings, showing substantial reductions in full width at half maximum (FWHM) values and a realignment of peak positions toward their original states, indicative of stress and defect recovery. To compare the effectiveness of EWF, we also conducted traditional thermal annealing at 250 °C for 7 h, which proved less effective in defect recovery as evidenced by less pronounced improvements in XRD FWHM values.
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Rahman, Md Hafijur [The Pennsylvania State University, University Park, PA (United States)] (ORCID:0000000214401839), Rasel, Md Abu Jafar [The Pennsylvania State University, University Park, PA (United States)] (ORCID:0009000318666767), Smyth, Christopher M. [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)] (ORCID:0000000346689555), Waryoba, Daudi [The Pennsylvania State University, DuBois, PA (United States)] (ORCID:0000000211903665), Haque, Aman [The Pennsylvania State University, University Park, PA (United States)] (ORCID:0000000165355484). 2024-12-31. Radiation Damage Mitigation in FeCrAl Alloy at Sub-Recrystallization Temperatures. https://doi.org/10.3390/ma18010124
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