A software system for emission spectrometry

Abstract

A computer system was developed for an emission spectrometry facility consisting of a direct current (DC) argon arc spectrograph optically coupled to an inductively coupled plasma multichannel spectrometer. Custom hardware and software were designed to control analytical functions and perform data acquisition. The software system was designed to make operation of the facility simple for routine operation and flexible for research and development. Special software was written to collect data under controlled conditions to characterize and monitor system response. One sequence collects intensity versus time data on all channels and displays the data graphically. These profiles are useful in studying the effects of operating parameters on measurement precision. Another special sequence performs calibration using a spline curve fit procedure. Routines were also written to measure dark currents and signals from a standard tungsten halogen lamp mounted in place of the DC arc. For quality control purposes, histories of these values are kept and monitored for excess scatter or drift.