Influence of microstructure and phase morphology on the stability of high temperature irradiation resistant thermocouples
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Riley, Scott (ORCID:000000027498065X)↗
Engineering topics
Skifton, Richard
Publications and source records attributed to Skifton, Richard.
High-temperature irradiation-resistant thermocouple instability model for in-pile reactor use
This article presents an instability model for the high-temperature irradiation-resistant thermocouple (HTIR-TC). Here the term instability defines the superposition of both drift and inhomogeneity of TC thermoelements occurring simultaneously. The HTIR-TC is an advanced thermocouple (TC) that uses the refractory metals niobium and molybdenum as sensing thermoelements for generating electromotive force (EMF) in a field of neutrons and at temperatures upward of 1,600°C. In the Advanced Gas Reactor (AGR) 5/6/7 tests conducted at Idaho National Laboratory’s Advanced Test Reactor (ATR), the HTIR-TCs showed low to moderate instability throughout the life of the test. The instability model reveals that HTIR-TCs can, when the operating temperature of the reactor fuel is normal, maintain performance throughout an 18-month refueling cycle typical of nuclear power plants, reflecting an instability of less than ±1%. The HTIR-TC is also qualified for incorporation into a test fixture during the testing of new fuels.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Integration Testing of Ultrasonic Deformation Sensor for TREAT Experiments
Fuel deformation (both axial and radial) information provides insights into fuel performance and failure limits. Traditionally, fuel deformation has been quantified using post-irradiation examinations due to the lack of an appropriate sensor for monitoring deformation in situ. Recent developments in sensor and instrumentation design have led to the use of linear variable differential transformers (LVDT) for monitoring axial strain in fuel during irradiation. Size and operational constraints limit the use of LVDT sensors for radial deformation monitoring, and alternatives are needed. One possible alternative to LVDT sensors is an ultrasonic sensor. Ultrasonic sensors monitor the interaction of high-frequency stress waves with the test object. The resulting response may be analyzed to determine the properties of the material, including stress, strain, microstructure, presence of defects, and the elastic constants. While ultrasonic measurements have been successfully applied for monitoring strain in a number of applications, their use for in-core measurements has been limited. Largely, the limitations are due to the challenges associated with designing sensors that can operate under typical in-core conditions. This report documents testing performed to confirm that the prototypic ultrasonic deformation sensor can be integrated into TREAT irradiation experiments using the SETH capsule.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
HOT R&D100
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HOT video presentation
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Design Requirements for Ultrasonic Deformation Sensor for TREAT Experiments
Ultrasonic measurements of deformation can provide nondestructive measurements of dimensional changes rapidly (within tens to hundreds of microseconds). Further these methods are sensitive to both microstructural changes due to damage (from thermal, mechanical, and irradiation environments) and gross structural changes (such as swelling). As a result, ultrasonic methods have been applied to address needs in the nondestructive evaluation of structural components in nuclear power plants (including fuel cladding) during periodic pre-service and in-service inspection inspections. Ultrasonic measurements have been successfully used for nondestructive materials characterization, including nondestructive evaluation (NDE) of degradation and damage, microstructure characterization, and process control. Ultrasonic NDE is a critical element of the nuclear power industry’s in-service inspection program for maintaining the integrity of the pressure boundary, and is being actively investigated for post-irradiation examination of fuels. Ultrasonic measurements, typically performed at 10 MHz or higher, performed post irradiation show that fuel microstructural parameters, such as porosity and grain size, can be correlated to ultrasonic velocity. Ultrasonic methods historically have seen limited applicability to environments with high temperatures and irradiation. Though some environmental factors (such as temperature) affect the measurement (sound speed, for instance), the limitation is primarily due to the probes themselves. Most commonly, lead-zirconate-titanate (PZT) is used as the piezoelectric sensor material for ultrasonic nondestructive measurements. PZT is limited in its applicability at elevated temperatures (approximately above 300C). However, recent tests (through DOE-NE’s NEET-ASI program) have identified a number of alternatives that can operate at elevated temperatures (in excess of 400C) and can survive irradiation. Certain grades of PZT have also been demonstrated for use in imaging under-sodium in sodium fast reactors.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Optimization of heat treatment and calibration procedures for high temperature irradiation resistant thermocouples [The development of calibration procedures for high temperature irradiation resistant thermocouples]
Here, a detailed description is provided for the optimization of heat treatment and calibrating procedure for Idaho National Laboratory’s high temperature irradiation resistant thermocouples (HTIR-TC). Also discussed is the implication of the procedures on the overall performance of the HTIR-TC finished product; in particular, for the case of long lead sections that are typical of sensors deployed in nuclear reactors. The effect on the measurement accuracy of fluctuations of the reference temperature and localized heating along the sensor lead is also investigated. A calibration graphical user interface (GUI) and accompanying script is presented for unifying the calibration process. A fifth-order polynomial function was found to be best for fitting HTIR-TC calibration data. The performance of the HTIR-TCs subject to the optimized heat treatment and calibration procedures is shown to be robust and consistent with other TC industry standards. Electromotive force curves versus length of the TC are presented to clarify positioning of TCs in general and how its effect on the calibrated temperatures.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
In-Pile Fuel Rod Deformation Measurements Using Miniaturized LVDT Technology
Different types of materials are being considered for fuel, cladding, and structures in existing and advanced nuclear reactors. These materials can undergo significant dimensional changes during irradiation. Currently in the US, such changes are measured with the ‘cook and look’ method (i.e. repeatedly irradiating a specimen for a specified period of time, and then removing it from the reactor for evaluation) – which leads to costly and time consuming experiments. In addition, such techniques provide limited data, and handling may disturb the phenomena of interest. Therefore, in-pile detection of geometric changes is needed to understand real-time behavior during irradiation testing of fuels and materials in high flux US Material and Test Reactors (MTRs). The developmental results of an advanced Linear Variable Differential Transformer (LVDT)-based test rig capable of detecting real-time changes in diameter or length of fuel rods or other material samples during irradiation in US MTRs are presented. The LVDT is being developed at the Idaho National Laboratory (INL), and will provide experimenters with the capability to measure dimensional changes associated with fuel and clad swelling, pellet-clad interaction, and crud buildup. The LVDT design utilizes the MTR’s loop pressure to drive the test specimen at a constant rate. This leads to a simplified construction which only requires three pressure boundary penetrations. Further, the LVDT pressure boundary is a leak tight hydraulic ram capable of actuating under low differential pressure (e.g. 1 psid), and is able to survive the high irradiation tests at Pressurized Water Reactor (PWR) conditions.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗