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Rohatgi, N.

Publications and source records attributed to Rohatgi, N..

Cross contamination of Martian rock samples

This paper presents the results of theoretical analyses conducted to investigate potential of various particle removal techniques.

contamination particle removal techniques

Evaluation of sample preservation methods for space mission

For interplanetary spacecraft that will travel to destinations where future life detection experiments may be conducted or samples are to be returned to earth, we should archive and preserve relevant samples from the spacecraft and cleanrooms for evaluation at a future date.

ATP endotoxin archiving planetary protection sampl

Development of vapor phase hydrogen peroxide sterilization process for spacecraft applications

This paper will present test data and discussion on the work we are conducting at JPL to address the following issues: 1) efficacy of sterilization process; 2) diffusion of hydrogen peroxide under sterilization process conditions into hard to reach places; 3) materials and components compatibility with the sterilization process and 4) development of methodology to protect sensitive components from hydrogen peroxide vapor.

hydrogen peroxide sterilization spacecraft

Planetary protection technologies at the Jet Propulsion Laboratory

This paper presents a summary of the planetary protection technology development efforts currently being conducted at the Jet Propulsion Laboratory (JPL). This is a multidisciplinary effort involving JPL and NASA expertise in microbiology, material science, and analytical chemistry, in conjunction with outside, industrial academic collaborators.

planetary

Fluidized-Bed Particles Scavenge Silicon Fines

Waste reduced, and silicon production rate improved. In new process silicon formed by thermal decomposition of SiH4. Part of silicon formed on silicon seed particles as result of surface chemical reaction. However, silicon formed by homogeneous reaction in gas phase tends to form aggregates of silicon atoms, which appear as fine particles (like dust). Believed that scavenging action of seed particles enables large fraction fines to be incorporated onto seed surface. This mode of growth confirmed by electron microscopy photographs.

Hsu, G. C.

Fines in fluidized bed silane pyrolysis

Silicon deposition on silicon seed particles by silane pyrolysis in a fluidized-bed reactor is investigated as a low-cost, high-throughput method to produce high-purity polysilicon for solar-cell applications. Studies of fines, particles 0.1-10 microns diam, initiated from homogeneous decomposition in the reactor were conducted using 2 and 6-in-diam fluidized beds. The studies show functional dependences of fines elutriation on silane feed concentration, temperature, gas velocity, and bubble size. The observation that the fines elutriation is generally below 10 percent of the silicon-in-silane feed is attributed to scavenging by large particles in an environment of less free space for homogeneous nucleation. Preliminary results suggest that, with proper conditions and distributor design, high-silane-concentration (over 50 percent SiH4 in H2) feed may be used.

Hsu, G.

Fluidized bed silicon deposition

The growth of silicon on seed particles from the pyrolysis of silane in a fluidized bed reactor (FBR) was studied. The grown particles were shown to be crystalline and to have a structure which has been interpreted to indicate growth by chemical vapor deposition as well as by the collection (scavenging) of silicon clusters on seed particle surfaces. Scanning electron microscopy was used to study the product morphology.

Hsu, G.

Coal desulfurization by low temperature chlorinolysis, phase 2

An engineering scale reactor system was constructed and operated for the evaluation of five high sulfur bituminous coals obtained from Kentucky, Ohio, and Illinois. Forty-four test runs were conducted under conditions of 100 by 200 mesh coal,solvents - methlychloroform and water, 60 to 130 C, 0 to 60 psig, 45 to 90 minutes, and gaseous chlorine flow rate of up to 24 SCFH. Sulfur removals demonstrated for the five coals were: maximum total sulfur removal of 46 to 89% (4 of 5 coals with methylchloroform) and 0 to 24% with water. In addition, an integrated continuous flow mini-pilot plant was designed and constructed for a nominal coal rate of 2 kilograms/hour which will be operated as part of the follow-on program. Equipment flow sheets and design drawings are included for both the batch and continuous flow mini-pilot plants.

Kalvinskas, J. J.