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Lu, Ping

Publications and source records attributed to Lu, Ping.

At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Precipitation hardening of laser powder bed fusion Ti-6Al-4V

Here, the laser powder bed fusion (PBF-L) additive manufacturing (AM) community has dedicated significant efforts into process optimization and control for defect-free Ti-6Al-4V. As defects become less of an issue for PBF-L Ti-6Al-4V, the processing-structure-properties (PSP) relationships between AM microstructures can now be explored to optimize mechanical properties. Lower temperature aging treatments around 550 °C in wrought Ti-6A-4V have been historically understood to precipitation harden the α phase with an ordered, hexagonal close packed (HCP) α 2 phase. The α 2 phase existed as nanoscale Ti 3 Al precipitates coherent with the parent α phase. The goal of the present investigation was to implement a vacuum heat treatment of 545 °C for 100 hours on PBF-L Ti-6Al-4V. This vacuum heat treatment took place after an initial hot isostatic pressure (HIP) treatment that decomposed the as-built, martensitic microstructure. The vacuum aging successfully produced nanoscale precipitates of α 2 phase within α-laths, confirmed via atom probe tomography (APT). Microstructural-length scale and quasi-static mechanical properties were investigated by nanoindentation and uniaxial tensile tests of miniaturized test specimens. Given the sensitivity of Ti-6Al-4V mechanical properties to small changes in chemistry, all test specimens originated from the same build. The α 2 precipitation resulted in significantly harder α-laths (≈ 2 GPa) as measured via nanoindentation, as well as a relative yield and ultimate tensile strength increase of 60 MPa and 38 MPa, respectively. Analysis of Variance (ANOVA) of the datasets revealed no statistical differences in total elongation between the HIPed and HIPed + aged specimens, indicative of the aging treatment producing a net benefit of strength with no loss in ductility.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Engineering exchange bias at the interface of self-polarized ultrathin ferroelectric Ba⁢Ti⁢O 3 and ferromagnetic La 0.67⁢ Sr 0.33 ⁢Mn⁢O 3

We investigate the emergence and optimization of conventional exchange bias (EB) in ultrathin (<10 nm) ferroelectric (FE) Ba⁢Ti⁢O 3 (BTO)/ferromagnetic (FM) La 0.67 ⁢Sr 0.33⁢ Mn⁢O 3 (LSMO) epitaxial bilayers without an antiferromagnetic (AFM) material. The EB originates from the electronic orbital reconstruction at the FE-FM interface due to the ferroelectric polarization. We achieve maximum EB of approximately 42 Oe with single-domain polarization in nine-unit-cell-thick BTO, setting the BTO thickness above the critical threshold for ferroelectricity yet below the thickness of strain relaxation and multidomain breakdown. Furthermore, the LSMO layer needs to be thick enough to sustain both the FM layer and polarization-induced AFM spin configuration at the LSMO/BTO interface, yet as thin as possible to enable the EB loop shift. The temperature, training, field, and thickness dependence of the EB confirm that the LSMO/BTO interface exhibits conventional EB despite its unconventional origin. Using x-ray magnetic circular dichroism, scanning transmission electron microscopy, and density-functional-theory calculations, we confirm that the macroscopic EB effect originates from the interfacial AFM spin configuration in LSMO driven by FE-induced d-orbital modifications in interfacial Mn ions. Thus, we engineer strong interfacial EB coupling in artificial multiferroics without a conventional AFM material by controlling FE polarization, highlighting the potential for advanced spintronic applications.

exchange bias↗
DOE OSTI2024

Epitaxial Thin Film Growth on Recycled SrTiO 3 Substrates Toward Sustainable Processing of Complex Oxides

Complex oxide thin films cover a range of physical properties and multifunctionalities that are critical for logic, memory, and optical devices. Typically, the high‐quality epitaxial growth of these complex oxide thin films requires single crystalline oxide substrates such as SrTiO 3 (STO), MgO, LaAlO 3 , a‐Al 2 O 3, and many others. Recent successes in transferring these complex oxides as free‐standing films not only offer great opportunities in integrating complex oxides on other devices, but also present enormous opportunities in recycling the deposited substrates after transfer for cost‐effective and sustainable processing of complex oxide thin films. In this work, the surface modification effects introduced on the recycled STO are investigated, and their impacts on the microstructure and properties of subsequently grown epitaxial oxide thin films are assessed and compared with those grown on the pristine substrates. Detailed analyses using high‐resolution scanning transmission electron microscopy and geometric phase analysis demonstrate distinct strain states on the surfaces of the recycled STO versus the pristine substrates, suggesting a pre‐strain state in the recycled STO substrates due to the previous deposition layer. These findings offer opportunities in growing highly mismatched oxide films on the recycled STO substrates with enhanced physical properties. Specifically, yttrium iron garnet (Y 3 Fe 5 O 12 ) films grown on recycled STO present different ferromagnetic responses compared to that on the pristine substrates, underscoring the effects of surface modification. The study demonstrates the feasibility of reuse and redeposition using recycled substrates. Via careful handling and preparation, high‐quality epitaxial thin films can be grown on recycled substrates with comparable or even better structural and physical properties toward sustainable process of complex oxide devices.

pre-strained STO surfaces↗
DOE OSTI2024

Effect of crystallite size on lithium storage performance of high entropy oxide (Cr 0.2 Mn 0.2 Co 0.2 Ni 0.2 Zn 0.2 ) 3 O 4 nanoparticles

High-entropy oxides (HEOs), known for their high theoretical capacity and structural stability, are considered promising anode materials for next-generation lithium-ion batteries (LIBs). In this research, we synthesized a novel spinel-type HEO, (Cr 0.2 Mn 0.2 Co 0.2 Ni 0.2 Zn 0.2 ) 3 O 4 , using a solution combustion method. By adjusting the quantity of the combustion agent, we produced samples with varying crystallite sizes. The crystallite size of the HEOs initially enlarges with an increased combustion agent, then diminishes. The enhancement of crystallite size correlates with improved electrochemical performance for lithium storage. Notably, the (Cr 0.2 Mn 0.2 Co 0.2 Ni 0.2 Zn 0.2 ) 3 O 4 nanoparticles, with the largest crystallite size of 36.3 nm, demonstrated a reversible capacity of 343 mA h g -1 after 100 cycles at 100 mA g -1 , a capacity retention to 319 mA h g -1 after 1000 cycles at 1 A g -1 , and a commendable rate capability of 260 mA h g -1 at 2 A g -1 . Furthermore, this study underscores the pivotal role of crystallite size in LIB performance and presents a viable strategy to enhance the lithium storage capabilities of HEOs and other metal oxides.

25 ENERGY STORAGE↗
DOE OSTI2024

Advancing the Understanding of Manufacturing Tools for Hardware Security

This project’s goal was to explore new methods and tools to evaluate the focused ion beam (FIB) effect on active electrical devices, which is becoming increasingly challenged by the continual decrease in transistor geometry. Novel hole transfer methods leveraging FIB patterning were demonstrated utilizing selective area atomic layer deposition (ALD) and metal assisted chemical etching. A FIB damage electrical tester device was fabricated, and the effects of FIB beams were characterized by examining change in performance of damaged transistors. Detailed characterization of end-of-range damage for common FIB ions were correlated to modeling methods. Finally, undamaged and damaged devices were simulated by Charon to begin understanding the FIB effects on active devices. This test platform along with modeling methods give a powerful way to assess FIB damage in materials and devices, and with more development can help establish methods to predict FIB damage effects on electrical devices.

42 ENGINEERING↗
DOE OSTI2024

Atomic-Scale Characterization of Dilute Dopants in Topological Insulators via STEM–EDS Using Registration and Cell Averaging Techniques

Magnetic dopants in three-dimensional topological insulators (TIs) offer a promising avenue for realizing the quantum anomalous Hall effect (QAHE) without the necessity for an external magnetic field. Understanding the relationship between site occupancy of magnetic dopant elements and their effect on macroscopic property is crucial for controlling the QAHE. By combining atomic-scale energy-dispersive X-ray spectroscopy (EDS) maps obtained by aberration-corrected scanning transmission electron microscopy (AC-STEM) and novel data processing methodologies, including semi-automatic lattice averaging and frame registration, we have determined the substitutional sites of Mn atoms within the 1.2% Mn-doped Sb 2 Te 3 crystal. More importantly, the methodology developed in this study extends beyond Mn-doped Sb 2 Te 3 to other quantum materials, traditional semiconductors, and even electron irradiation sensitive materials.

36 MATERIALS SCIENCE↗
NASA NTRS2020

Pterodactyl: The Development and Performance of Guidance Algorithms for a Mechanically Deployed Entry Vehicle

Pterodactyl is a NASA Space Technology Mission Directorate (STMD) project focused on developing a design capability for optimal, scalable, Guidance and Control (G&C) solutions that enable precision targeting for Deployable Entry Vehicles (DEVs). This feasibility study is unique in that it focuses on the rapid integration of targeting performance analysis with structural & packaging analysis, which is especially challenging for new vehicle and mission designs. This paper will detail the guidance development and trajectory design process for a lunar return mission, selected to stress the vehicle designs and encourage future scalability. For the five G&C configurations considered, the Fully Numerical Predictor-Corrector Entry Guidance (FNPEG) was selected for configurations requiring bank angle guidance and FNPEG with Uncoupled Range Control (URC) was developed for configurations requiring angle of attack and sideslip angle guidance. Successful G&C configurations are defined as those that can deliver payloads to the intended descent and landing initiation point, while abiding by trajectory constraints for nominal and dispersed trajectories.

Johnson, Breanna J.↗
NASA NTRS2020

Mid Lift-to-Drag Ratio Rigid Vehicle 6-DoF Performance for Human Mars Entry, Descent, and Landing: A Fractional Polynomial Powered Descent Guidance Approach

Defining a feasible vehicle design and mission architecture capable of reliably delivering apayload of 20 metric tons (mt) or more is a great challenge for landing humans on Mars. TheMid Lift-to-Drag Rigid Vehicle (MRV), a rigid decelerator studied in NASA’s Entry, Descent,and Landing Architecture Study (EDLAS), has shown to be a viable vehicle candidate forfuture human Mars missions. As the vehicle concept matures, models of increasing fidelity areadded to the six-degree-of-freedom (6DoF) EDL simulation. This paper presents 6DoFsimulation results using model updates for vehicle mass properties, fineness ratio, andaerodynamic-propulsive interactions. Additionally, an assessment of the Fractional-Polynomial Powered Descent Guidance (FP2DG) performance is presented, and the vehicleperformance is compared with the Tunable Apollo Powered Descent Guidance (TAPDG).Finally, Monte Carlo results of the vehicle design trades are presented.

Johnson, Breanna J.↗
NASA NTRS2019

Mid-Lift-To-Drag Ratio Rigid Vehicle 6-DOF EDL Performance Using Tunable Apollo Powered Guidance

The Mid-Lift-to-Drag ratio Rigid Vehicle (MRV) is a candidate in the NASA multi-center effort to determine the most cost effective vehicle to deliver a large-mass payload to the surface of Mars for a human mission. Products of this effort include six-degree-of-freedom (6DoF) entry-to-landing trajectory performance studies for each candidate vehicle. These high fidelity analyses help determine the best guidance and control (G&C) strategies for a feasible, robust trajectory. This paper presents an analysis of the MRV's G&C design by applying common entry and descent associated uncertainties using a Fully Numerical Predictor-corrector Entry Guidance (FNPEG) and tunable Apollo powered descent guidance.

Johnson, Breanna J.↗
NASA NTRS2019

Mid-Lift-to-Drag Ratio Rigid Vehicle 6-DOF EDL Performance Using Tunable Apollo Powered Guidance

The Mid-Lift-to-Drag ratio Rigid Vehicle (MRV) is a candidate in the NASA multi-center effort to determine the most cost effective vehicle to deliver a large-mass payload to the surface of Mars for a human mission. Products of this effort include six-degree-of-freedom (6DoF) entry-to-descent trajectory performance studies for each candidate vehicle. These high fidelity analyses help determine the best guidance and control (G&C) strategies for a feasible, robust trajectory. This paper presents an analysis of the MRV's G&C design by applying common entry and descent associated uncertainties using a Fully Numerical Predictor-corrector Entry Guidance (FNPEG) and tunable Apollo powered descent guidance.

human↗
NASA NTRS2018

Entry, Descent, and Landing Performance for a Mid-Lift-to-Drag Ratio Vehicle at Mars

In an effort to mature the design of the Mid-Lift-to-Drag ratio Rigid Vehicle (MRV) candidate of the NASA Evolvable Mars Campaign (EMC) architecture study, end-to-end six-degree-of-freedom (6DOF) simulations are needed to ensure a successful entry, descent, and landing (EDL) design. The EMC study is assessing different vehicle and mission architectures to determine which candidate would be best to deliver a 20 metric ton payload to the surface of Mars. Due to the large mass payload and the relatively low atmospheric density of Mars, all candidates of the EMC study propose to use Supersonic Retro-Propulsion (SRP) throughout the descent and landing phase, as opposed to parachutes, in order to decelerate to a subsonic touchdown. This paper presents a 6DOF entry-to-landing performance and controllability study with sensitivities to dispersions, particularly in the powered descent and landing phases.

mars↗
NASA NTRS2018

Nguyen Xuan Vinh - A Life In Hypersonic Flight

Nguyễn Xuân Vinh (born January 1930 in Yên Bái, Vietnam) is a noted Vietnamese-American aerospace scientist and educator whose seminal work on the guidance, dynamics and optimal control of space vehicles and their interaction with the atmosphere has played a fundamental role in space exploration. Vinh is Professor Emeritus of Aerospace Engineering at the University of Michigan, where he taught for nearly thirty years. Among his many publications was "Hypersonic and Planetary Entry Flight Mechanics” (1980. Vinh, N. X.; Busemann, A.; Culp, R. D. University of Michigan Press) which contains equations for hypersonic flight that came to be known as “the Vinh equations”.

Lu, Ping↗
NASA NTRS2018

Mid-Lift-to-Drag Ratio Rigid Vehicle Control System Design and Simulation for Human Mars Entry

The Mid-Lift-to-Drag Ratio Rigid Vehicle (MRV) is a proposed candidate in the NASA Evolvable Mars Campaign's (EMC) Pathfinder Entry, Descent, and Landing (EDL) architecture study. The purpose of the study is to design a mission and vehicle capable of transporting a 20mt payload to the surface of Mars. The MRV is unique in its rigid, asymmetrical lifting-body shape which enables a higher lift-to-drag ratio (L/D) than the typical robotic Mars entry capsule vehicles that carry much less mass. This paper presents the formulation and six-degree-of-freedom (6DOF) performance of the MRV's control system, which uses both aerosurfaces and a propulsive reaction control system (RCS) to affect longitudinal and lateral directional behavior.

mars↗