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Kendall, B. R. F.

Publications and source records attributed to Kendall, B. R. F..

At least 19 records
All sourcesNASA NTRSDOE OSTI
NASA NTRS1986

Mass spectrometric studies of the electrical breakdown of thin polymer films

The composition of the neutral particles released during the electrical breakdown of 50-micron and 75-micron insulating films of the type used on spacecraft exteriors investigated experimentally using a time-of-flight mass spectrometer triggered by the breakdown event. The experimental apparatus is described in detail, and the results are presented in photographs. It is found that the particle flux from Teflon FEP and PFA films comprise mainly fluorocarbon fragments, some with mass 350 amu or greater, but the flux from Kapton oxygen-ion-beam treated Kapton, Tefzel, and Mylar comprises mainly molecules of mass 44 amu or less.

Kendall, B. R. F.↗
NASA NTRS1985

Mass analysis of neutral particles and ions released during electrical breakdowns on spacecraft surfaces

Charged-particle fluxes from breakdown events were studied. Methods to measure mass spectra and total emitted flux of neutral particles were developed. The design and construction of the specialized mass spectrometer was completed. Electrical breakdowns were initiated by a movable blunt contact touching the insulating surface. The contact discharge apparatus was used for final development of two different high-speed recording systems and for measurements of the composition of the materials given off by the discharge. It was shown that intense instantaneous fluxes of neutral particles were released from the sites of electrical breakdown events. A laser micropulse mass analyzer showed that visible discoloration at breakdown sites were correllated with the presence of iron on the polymer side of the film, presumably caused by punch-through to the Inconel backing. Kapton samples irradiated by an oxygen ion beam were tested. The irradiated samples were free of surface hydrocarbon contamination but otherwise behaved in the same way as the Kapton samples tested earlier. Only the two samples exposed to oxygen ion bombardment were relatively clean. This indicates an additional variable that should be considered when testing spacecraft materials in the laboratory.

Kendall, B. R. F.↗
NASA NTRS1985

Mass spectra of neutral particles released during electrical breakdown of thin polymer films

A special type of time-of-flight mass spectrometer triggered from the breakdown event was developed to study the composition of the neutral particle flux released during the electrical breakdown of polymer films problem. Charge is fed onto a metal-backed polymer surface by a movable smooth platinum contact. A slowly increasing potential from a high-impedance source is applied to the contact until breakdown occurs. The breakdown characteristics is made similar to those produced by an electron beam charging system operating at similar potentials. The apparatus showed that intense instantaneous fluxes of neutral particles are released from the sites of breakdown events. For Teflon FEP films of 50 and 75 microns thickness the material released consists almost entirely of fluorocarbon fragments, some of them having masses greater than 350 atomic mass units amu, while the material released from a 50 micron Kapton film consists mainly of light hydrocarbons with masses at or below 44 amu, with additional carbon monoxide and carbon dioxide. The apparatus is modified to allow electron beam charging of the samples.

Kendall, B. R. F.↗
NASA NTRS1983

The pressure multiplier revisited

Pressure multipliers, which were originally intended to continuously sample an unknown pressure and increase it by a known factor, so that measurements could be conducted at low pressures with liquid-in-gas gauges, may be usefully applied to the increasing number of components available for use in molecular flow networks. An intriguing possibility involves the electric control of pressure multiplier gain by means of a piezoelectric valve.

Kendall, B. R. F.↗
NASA NTRS1983

Mass analysis of neutral particles and ions released during electrical breakdowns on spacecraft surfaces

A specialized spectrometer was designed and developed to measure the mass and velocity distributions of neutral particles (molecules and molecular clusters) released from metal-backed Teflon and Kapton films. Promising results were obtained with an insulation breakdown initiation system based on a moveable contact touching the insulated surfaces. A variable energy, high voltage pulse is applied to the contact. The resulting surface damage sites can be made similar in size and shape to those produced by a high voltage electron beam system operating at similar discharge energies. The point discharge apparatus was used for final development of several high speed recording systems and for measurements of the composition of the materials given off by the discharge. Results with this apparatus show evolution of large amounts of fluorocarbon fragments from discharge through Teflon FEP, while discharges through Kapton produce mainly very light hydrocarbon fragments at masses below about 80 a.m.u.

Kendall, B. R. F.↗
NASA NTRS1982

Pressure pulsations above turbomolecular pumps

Lange and Singleton (1978) have observed pressure pulses above a turbomolecular pump. They reported that the mean pulse frequency increased with the temperature of the pump cooling water and that the evolved gas was mainly hydrogen. The present investigation takes into account tests conducted with a similar pumping system. The pumping system was equipped with additional pressure-monitoring equipment in order to study these pulsations in more detail. It was found that at least two distinct types of pressure pulsations may be present in a turbomolecular-pumped ultrahigh vacuum system. The random hydrogen pulses are easily eliminated for period of days by changing the cooling water temperature. The cyclic pulses consisting mainly of water vapor are not likely to be a problem in normal experiments.

Danziger, S.↗
NASA NTRS1982

Anaerobic polymers as high vacuum leak sealants

Anaerobic polymers are useful as solventless leak sealants with good vacuum properties at moderate temperatures. Loctite 290 can seal leaks in a range generally encountered in carefully constructed ultrahigh vacuum and high vacuum systems. It was found that small leaks are sealed best under vacuum, whereas large leaks should be sealed at atmospheric pressure. The high-temperature behavior of Loctite 290 is limited by its fast cure, which prevents deep penetration into small leaks; cracking eventually occurs at the entrance to the leak. Repeated thermal cycling to about 300 C is possible, however, provided viscosity, curing time, and leak size are properly matched to ensure penetration into the body of the leak. This may require special formulations for high temperature vacuum applications.

Kendall, B. R. F.↗
NASA NTRS1980

Vacuum applications of metal foams

Several vacuum applications of copper foams in the density range 2-5% and pore sizes of 0.5-0.7 mm are discussed, such as a foreline hydrocarbon trap in a mechanical vacuum pump, a molecular-flow resistor, a diffuser, and a water injector. Other suggested applications include the use of foam copper in the form of an externally heated plug to remove traces of oxygen from inert gases bled into a vacuum system through a stainless steel line and the use of the porous surface for minimizing release of secondary electrons from electrodes in the path of charged particle beams.

Kendall, B. R. F.↗
NASA NTRS1980

Production of pulsed electric fields using capacitively coupled electrodes

It is shown that pulsed electric fields can be produced over extended volumes by taking advantage of the internal capacitances in a stacked array of electrodes. The design, construction, and performance of practical arrays are discussed. The prototype arrays involved fields of 100-1000 V/cm extending over several centimeters. Scaling to larger physical dimensions is straightforward.

Kendall, B. R. F.↗
NASA NTRS1975

Bonded electrodes for use on the external surface of spacecraft

A new bonding process is described which is suitable for applying electrodes to the external surfaces of spacecraft and sounding rockets. A polyimide material containing small, uniform glass spheres provides the necessary insulation and mechanical strength. The bonded electrodes are simple to construct and are shown to have good electrical, vacuum, and thermal properties.

Kendall, B. R. F.↗
NASA NTRS1974

Three-terminal shielded resistors for fast electrometers

The design of electrometer feedback resistors for use at frequencies up to the kilohertz range is discussed. It is shown experimentally that the addition of capacitive coupling between the electrometer output and the center of the feedback resistor, combined with suitable shielding, gives substantially better performance at high frequencies than is obtainable with more conventional designs.

Kendall, B. R. F.↗
NASA NTRS1974

Transient desorption of water vapor - A potential source of error in upper atmosphere rocket experiments

Results of measurements of the outgassing rates of samples of materials and surface finishes used on the outer skins of rocket-borne experiment packages in simulated rocket ascents. The results showed outgassing rates for anodized aluminum in the second minute of flight which are two to three orders of magnitude higher than those given in typical tables of outgassing rates. The measured rates for aluminum with chromate conversion surface coatings were also abnormally high. These abnormally high initial rates fell quickly after about five to ten minutes to values comparable with those in the published literature. It is concluded that anodized and chromate conversion coatings on the aluminum outer surfaces of a sounding rocket experiment package will cause gross distortion of the true water vapor environment.

Kendall, B. R. F.↗