Engineering Papers⌕ Search

Engineering topics

Kazmierczak, Michael

Publications and source records attributed to Kazmierczak, Michael.

Thermal Imaging Applied to Cryocrystallography: Cryocooling and Beam Heating (Part I)

Thermal imaging provides a non-invasive method to study both the cryocooling process and the heating due to the X-ray beam interaction with a sample. The method has been used successfully to image cryocooling in a number of experimental situations, i.e. cooling as a function of sample volume and as a function of cryostream orientation. Although there are experimental limitations to the method, it has proved a powerful technique to aid cryocrystallography development. Due to the rapid spatial temperature information provided about the sample it is also a powerful tool in the testing of mathematical models. Recently thermal imaging has been used to measure the temperature distribution on both a model and typical crystal samples illuminated with an X-ray beam produced by an undulator. A brief overview of thermal imaging and previous results will be presented. In addition, a detailed description of the calibration and experimental aspects of the beam heating measurements will be described. This will complement the following talk on the mathematical modeling and analysis of the results.

Snell, Edward↗

Beam Heating of Samples: Modeling and Verification

Energy absorbed from the X-ray beam by the sample requires cooling by forced convection (i.e. cryostream) to minimize temperature increase and the damage caused to the sample by the X-ray heating. In this presentation we will first review the current theoretical models and recent studies in the literature, which predict the sample temperature rise for a given set of beam parameters. It should be noted that a common weakness of these previous studies is that none of them provide actual experimental confirmation. This situation is now remedied in our investigation where the problem of x-ray sample heating is taken up once more. We have theoretically investigated, and at the same time, in addition to the numerical computations, performed experiments to validate the predictions. We have modeled, analyzed and experimentally tested the temperature rise of a 1 mm diameter glass sphere (sample surrogate) exposed to an intense synchrotron X-ray beam, while it is being cooled in a uniform flow of nitrogen gas. The heat transfer, including external convection and internal heat conduction was theoretically modeled using CFD to predict the temperature variation in the sphere during cooling and while it was subjected to an undulator (ID sector 19) X-ray beam at the APS. The surface temperature of the sphere during the X-ray beam heating was measured using the infrared camera measurement technique described in a previous talk. The temperatures from the numerical predictions and experimental measurements are compared and discussed. Additional results are reported for the two different sphere sizes and for two different supporting pin orientations.

Kazmierczak, Michael↗

Deterministic multi-zone ice accretion modeling

The focus here is on a deterministic model of the surface roughness transition behavior of glaze ice. The initial smooth/rough transition location, bead formation, and the propagation of the transition location are analyzed. Based on the hypothesis that the smooth/rough transition location coincides with the laminar/turbulent boundary layer transition location, a multizone model is implemented in the LEWICE code. In order to verify the effectiveness of the model, ice accretion predictions for simple cylinders calculated by the multizone LEWICE are compared to experimental ice shapes. The glaze ice shapes are found to be sensitive to the laminar surface roughness and bead thickness parameters controlling the transition location, while the ice shapes are found to be insensitive to the turbulent surface roughness.

Yamaguchi, K.↗