Engineering Papers⌕ Search

Engineering topics

Johnson, S. M.

Publications and source records attributed to Johnson, S. M..

At least 19 records
All sourcesNASA NTRSDOE OSTI
NASA NTRS2001

Ultrahigh Temperature Ceramics for Thermal Protection of Next Generation Space Vehicles

Materials with improved properties are needed for thermal protection of next generation space vehicles. Sharp leading edges on these vehicles will have to withstand exposure to high temperatures (> 2200 C or 4000 F) and severe thermal cycling in both neutral and oxidizing environments. These extreme conditions will require materials that possess superior oxidation resistance, low creep, and excellent thermal shock properties. This presentation will first discuss the system requirements for thermal protection of advanced space vehicles and then show how they are driving development of new materials systems. The presentation will focus on ultrahigh temperature ceramics (UHTCs) that are promising candidates for such applications. ZrB2 and HfB2 and composites of those ceramics with SiC are two particular families of UHTCs that are currently under development for sharp leading edges. These ceramics are appealing because their melting temperatures are 3245 C (5873 F) for ZrB2 and 3380 C (6116 F) for HfB2 and because they may form protective, oxidation resistant coatings in use. The mechanical properties of the UHTCs are strongly dependent on phase purity and the processing route used to make them, both of which factors are being actively investigated. For example, oxide impurities could form glassy grain boundary phases that soften at high temperatures and make the ceramic susceptible to creep deformation. Results from scanning and transmission electron microscopic studies of the UHTCs have shown how their processing can be improved to give better properties. This presentation will discuss the UHTC characterization results in some detail, focusing particularly on the structure and composition of the ceramic grain boundaries. The presentation will conclude with some remarks on how the properties of these promising UHTCs can be further improved and how they might be made more economically.

Loehman, R. E.↗
NASA NTRS2001

Mechanical Properties and Microstructural Characterization of Particulate Reinforced Diboride Composites for High Temperature Leading Edge Applications

Previous work on refractory diboride composites has shown that these systems have the potential for use in high temperature leading edge applications for reusable reentry vehicles. Experiments in reentry environments have shown that these materials have multiple use temperatures greater than 1900 C. The work to be discussed focuses on three compositions: HfB2/SiC, ZrB2/SiC, and ZrB2/C/SiC. These composites have been hot pressed and their mechanical properties measured at room and elevated temperatures. Extensive microstructural characterization has been conducted on polished cross sections and the fracture surfaces have been examined to determine their failure origins.

Ellerby, Donald T.↗
NASA NTRS2001

Composites: Processing and Fabrication Methodologies of Nonoxide Ceramic Composites. Processing HfB2 Composites for Use in Extreme Environments

HfB2 and ZrB2 composites containing SiC are known to have good thermal shock and configurational stability at elevated temperatures. These are promising ultra-high temperature ceramics (UHTCs) for use on the sharp leading edges of next generation space vehicles. Sharp leading edges on these vehicles will need to: withstand repeated exposures to temperatures > 2200 C in oxidizing environments; have good thermal shock and ablation resistance; and withstand the mechanical stress of launch and reentry. The HfB2/SiC composite is currently undergoing processing improvements in an effort to better the performance of a material that has been studied for approx. 35 years. The potential for HfB2/SiC composites to meet the requirements of hypersonic flight depends on controlling processing techniques. This presentation will focus on understanding processing steps now being undertaken to optimize the material properties of HfB2/SiC composites at NASA Ames Research Center. Correlation between processing techniques and microstructure will be shown. Preliminary oxidation studies will also be discussed.

Gusman, Michael I.↗
NASA NTRS2001

Processing and Properties Of Refractory Zirconium Diboride Composites For Use In High Temperature Applications

The Thermal Protection Materials and Systems Branch at NASA Ames Research Center is involved in the development of a class of refractory oxidation-resistant diboride composites termed Ultra High Temperature Ceramics or UHTCs. These composites have good high temperature properties making them candidate materials for thermal protection system (TPS) applications. The current research focuses on improving processing methods to develop more reliable composites with enhanced thermal and mechanical properties. This presentation will concentrate on the processing of ZrB2/SiC composites. Some preliminary mechanical properties and oxidation data will also be presented.

Stackpoole, Margaret↗
NASA NTRS2001

Fractographic Analysis of HfB2-SiC and ZrB2-SiC Composites

Hafnium diboride-silicon carbide and zirconium diboride-silicon carbide composites are potential materials for high temperature leading edge applications on reusable launch vehicles. In order to establish material constants necessary for evaluation of in-situ fracture, bars fractured in four point flexure were examined using fractographic principles. The fracture toughness was determined from measurements of the critical crack sizes and the strength values, and the crack branching constants were established to use in forensic fractography of materials for future flight applications. The fracture toughnesses range from about 13 MPam (sup 1/2) at room temperature to about 6 MPam (sup 1/2) at 1400 C for ZrB2-SiC composites and from about 11 MPam (sup 1/2) at room temperature to about 4 MPam (sup 1/2) at 1400 C for HfB2-SiC composites.

Mecholsky, J.J., Jr.↗
NASA NTRS1985

High Efficiency Large Area Polysilicon Solar Cells

Large area (100 sq cm) polysilicon solar cells having efficiencies of up to 14.1% (100 mW/sq cm, 25 C) were fabricated and a detailed analysis was performed to identify the efficiency loss mechanisms. The 1-5 characteristics of the best cell were dominated by recombination in the quasi-neutral base due to the combination of minority carrier diffusion length and base resistivity. An analysis of the microstructural defects present in the material and their effect on the electrical properties is presented.

Johnson, S. M.↗
NASA NTRS1984

Preliminary investigation of a two-zone swirl flow combustor

The effect of full-annular swirling-flow on a flow-zone combustor design is investigated. Swirl flow angles of 25, 35, and 45 degrees were investigated in a combustor design envelope typical of those used in modern engines. The two-zone combustor had 24 pilot-zone fuel injectors and 24 main-fuel injectors located in the centerbody between the pilot and swirl passage. Combustor performance was determined at idle, and two parametric 589 K inlet temperature conditions. Combustor performance was highest with the 45 degree swirl vane design; at the idle condition, combustion efficiency was 99.5 percent. The 45 degree swirl vane also produced the lowest pattern factor of the three angles and showed a combustor lean blowout limit below a 0.001 fuel-air ratio. Combustor total pressure drop varied from a low of 4.6 percent for the 25 degree swirl to a high of 4.9 percent for the 45 degree swirl. Previously announced in STAR as N84-22565

Biaglow, J. A.↗
NASA NTRS1984

Experimental investigation of the low NOx vortex airblast annular combustor

A low oxides of nitrogen vortex airblast annular combustor was evaluated which has attained the goal of 1 gm NO2/kg fuel or less during operation. The experimental combustor test conditions were a nominal inlet-air temperature of 703 K, inlet total pressures between 0.52 to 0.83 MPa, and a constant inlet Mach number of 0.26. Exit temperature pattern factors for all test points were between 0.16 and 0.20 and exit swirl flow angles were 47 degrees at isothermal conditions and 23 degrees during combustion. Oxides of nitrogen did not exceed 1.05 gm NO2/kg fuel at the highest inlet pressure and exhaust temperature tested. Previous correlations have related NOx proportionally to the combustor inlet pressure raised to some exponent. In this experiment, a band of exponents between 0.5 and 1.0 resulted for fuel-air ratios from 0.023 to 0.027 and inlet pressures from 0.52 to 0.83 MPa. Previously announced in STAR as N84-22567

Johnson, S. M.↗
NASA NTRS1984

Effects of Non-equilibrium Solidification on the Material Properties of Brick Silicon for Photovoltaics

Silicon ingot growth technologies like the Ubiquitous Crystallization Process (UCP) are solidified within a shaping crucible. The rate at which heat can be lost from this crucible minus the rate at which heat is input from an external source determines the rate at which crystallization will occur. Occasionally, when the process parameters for solidification are exceeded, the normally large multi-centimeter grain size material assocated with the UCP will break down into regions containing extremely small, millimeter or less, grain size material. Accompanying this breakdown in grain growth is the development of so called sinuous grain boundaries. The breakdown in grain growth which results in this type of small grain structure with sinuous boundaries is usually associated with the rapid crystallization that would accompany a system failure. This suggests that there are limits to the growth velocity that one can obtain and still expect to produce material that would possess good photovoltaic properties. It is the purpose to determine the causes behind the breakdown of this material and what parameters will determine the best rates of solidification.

Regnault, W. F.↗
NASA NTRS1984

Preliminary investigation of a two-zone swirl flow combustor

The effect of full-annular swirling-flow on a flow-zone combustor design is investigated. Swirl flow angles of 25, 35, and 45 degrees were investigated in a combustor design envelope typical of those used in modern engines. The two-zone combustor had 24 pilot-zone fuel injectors and 24 main-fuel injectors located in the centerbody between the pilot and swirl passage. Combustor performance was determined at idle, and two parametric 589 K inlet temperature conditions. Combustor performance was highest with the 45 degree swirl vane design; at the idle condition, combustion efficiency was 99.5 percent. The 45 degree swirl vane also produced the lowest pattern factor of the three angles and showed a combustor lean blowout limit below a 0.001 fuel-air ratio. Combustor total pressure drop varied from a low of 4.6 percent for the 25 degree swirl to a high of 4.9 percent for the 45 degree swirl.

Biaglow, J. A.↗
NASA NTRS1984

Experimental investigation of the low NO/sub x vortex airblast annular combustor

A low oxides of nitrogen vortex airblast annular combustor was evaluated which has attained the goal of 1 gm NO2/kg fuel or less during operation. The experimental combustor test conditions were a nominal inlet-air temperature of 703 K, inlet total pressures between 0.52 to 0.83 MPa, and a constant inlet Mach number of 0.26. Exit temperature pattern factors for all test points were between 0.16 and 0.20 and exit swirl flow angles were 47 degrees at isothermal conditions and 23 degrees during combustion. Oxides of nitrogen did not exceed 1.05 gm NO2/kg fuel at the highest inlet pressure and exhaust temperature tested. Previous correlations have related NOx proportionally to the combustor inlet pressure raised to some exponent. In this experiment, a band of exponents between 0.5 and 1.0 resulted for fuel-air ratios from 0.023 to 0.027 and inlet pressures from 0.52 to 0.83 MPa.

Johnson, S. M.↗
NASA NTRS1982

Venturi nozzle effects on fuel drop size and nitrogen oxide emissions

The effect of a venturi nozzle on the Sauter mean diameter of a water spray produced by a simplex pressure atomizing injector in a swirling airflow was determined. A Malvern particle and droplet size distribution analyzer, Type S.T. 1800, was used to measure D sub 32 of the water sprays. The water spray was studied at ambient temperature (293 K) and atmospheric pressure. The venturi reduced D sub 32 by an average of 30 percent when installed with a simplex injector and air swirler. The venturi primarily improved atomization of the injector spray by increasing relative air velocity. The small drop size enhanced vaporization and therefore decreased oxides of nitrogen in a combustor. The decrease in drop size provided by the addition of a venturi explains the results obtained in a previous small scale research combustor wherein NOx emission indices decreased as a result of this hardware modification.

Johnson, S. M.↗
NASA NTRS1977

Baseline performance of solar collectors for NASA Langley solar building test facility

The solar collector field contains seven collector designs. Before operation in the field, the experimental performances (thermal efficiencies) of the seven collector designs were measured in an indoor solar simulator. The resulting data provided a baseline for later comparison with actual field test data. The simulator test results are presented for the collectors as received, and after several weeks of outdoor exposure with no coolant (dry operation). Six of the seven collector designs tested showed substantial reductions in thermal efficiency after dry operation.

Knoll, R. H.↗
NASA NTRS1976

Evaluation of flat-plate collector efficiency under controlled conditions in a solar simulator

The measured thermal efficiencies of 35 collectors tested with a solar simulator, along with the correlation equations used to generalize the data, are presented in this report. The single correlation used is shown to apply to all the different types of collectors tested, including one with black paint and one cover, one with a selective surface coating and two covers, and an evacuated-tube collector. The test and correlation technique is also modified by using a shield so that collectors larger than the simulator test area can also be tested. This technique was verified experimentally for a shielded collector for which the collector shielded area was 31% of the solar simulator radiation area. A table lists all the collectors tested, the collector areas, and the experimental constants used to correlate the data for each collector.

Johnson, S. M.↗
NASA NTRS1976

Evaluation of flat-plate collector efficiency under controlled conditions in a solar simulator

The measured thermal efficiencies of 35 collectors tested with a solar simulator, along with the correlation equations used to generalize the data, are presented. The single correlation used is shown to apply to all the different types of collectors tested, including one with black paint and one cover, one with a selective surface coating and two covers, and an evacuated-tube collector. The test and correlation technique is also modified by using a shield so that collectors larger than the simulator test area can also be tested. This technique was verified experimentally for a shielded collector for which the collector shielded area was 31% of the solar simulator radiation area. A table lists all the collectors tested, the collector areas, and the experimental constants used to correlate the data for each collector.

Johnson, S. M.↗
NASA NTRS1972

Thermogravimetric-quadrupole mass-spectrometric analysis of geochemical samples.

Thermogravimetric-quadrupole mass-spectrometric-analysis techniques can be used to study a wide variety of problems involving decomposition processes and identification of released volatile components. A recording vacuum thermoanalyzer has been coupled with a quadrupole mass spectrometer. The rapid scan capabilities of the quadrupole mass spectrometer are used to identify the gaseous components released. The capability of the thermogravimetric-quadrupole mass spectrometer to provide analytical data for identification of the released volatile components, for determination of their sequence of release and for correlation of thermal-decomposition studies is illustrated by an analysis of the Orgueil carbonaceous chondrite.

Gibson, E. K., Jr.↗