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Harris, J. M.

Publications and source records attributed to Harris, J. M..

27 records · Page 2

Purification of biomaterials by phase partitioning

A technique which is particularly suited to microgravity environments and which is potentially more powerful than electrophoresis is phase partitioning. Phase partitioning is purification by partitioning between the two immiscible aqueous layers formed by solution of the polymers poly(ethylene glycol) and dextran in water. This technique proved to be very useful for separations in one-g but is limited for cells because the cells are more dense than the phase solutions thus tend to sediment to the bottom of the container before reaching equilibrium with the preferred phase. There are three phases to work in this area: synthesis of new polymers for affinity phase partitioning; development of automated apparatus for ground-based separations; and design of apparatus for performing simple phase partitioning space experiments, including examination of mechanisms for separating phases in the absence of gravity.

Harris, J. M.

New polymers for low-gravity purification of cells by phase partitioning

A potentially powerful technique for separating different biological cell types is based on the partitioning of these cells between the immiscible aqueous phases formed by solution of certain polymers in water. This process is gravity-limited because cells sediment rather than associate with the phase most favored on the basis of cell-phase interactions. In the present contract we have been involved in the synthesis of new polymers both to aid in understanding the partitioning process and to improve the quality of separations. The prime driving force behind the design of these polymers is to produce materials which will aid in space experiments to separate important cell types and to study the partitioning process in the absence of gravity (i.e., in an equilibrium state).

Harris, J. M.

New polymers for phase partitioning

The synthesizing of several polyethylene glycols having crown ethers attached is reported. This work led to the identification of three new polymer types which promise to be more effective at selectively binding specific cell types. Work was completed on identification of chemical properties of the new polymer crowns and on development of new techniques for determination of polymer-phase composition.

Harris, J. M.

Precipitation attenuation studies based on measurements of ATS-6 20/30-GHz beacon signals at Clarksburg, MD.

COMSAT Laboratories participated in the millimeter wavelength propagation experiment, performing measurements of the 20/30-GHz ATS-6 satellite beacon signals and auxiliary measurements such as radiometric sky temperature and minute precipitation at Clarksburg, MD. These measurements were intended to broaden the data base required to advance satellite path at frequencies over 10 GHz. A correlation is established between direct measurement of attenuation of the signal radiated from the satellite and the indirect measurement of attenuation by auxiliary ground-based equipment. The indirectly derived statistics agreed reasonably well or can be reconciled with earlier published results and may therefore be used as a basis for estimating long-term cumulative attenuation statistics.

Fang, D. J.

Detecting contamination on a metal surface

Thin layers of contaminant on metal surface are detected by measuring surface-potential difference between reference electrode and surface of interest. Procedure does not require mechanical contact with surface under examination.

Harris, J. M.

Precipitation-attenuation studies based on measurements of ATS-6 20/30-GHz beacon signals at Clarksburg, Maryland

Radiometric sky temperature and minute precipitation measurements were intended to broaden the data base required to advance the understanding of the propagation characteristics of the earth-satellite path at frequencies over 10 GHz. Analyses of the data collected from the measurement program have established a detailed correlation between the satellite signal and the signals from auxiliary ground-based measurements. The indirectly derived statistics agreed reasonably well (or can be reconciled) with the earlier published results. The correlations may therefore be used for indirectly estimating long term cumulative attenuation statistics in the absence of direct satellite signal measurements.

Fang, D. J.

Studies on the Al2O3-Ti-Mo-Au metallization system

The behavior of Ti-Mo-Au metallization on Al2O3 and C has been investigated by backscattering spectrometry. Results show that Mo-Au bimetal films typically mix during deposition. Diffusion of Ti in Mo film occurs at 600 C, but is inhibited by the presence of oxygen in the Ti film. Even 1000 A of Mo is not a barrier against interdiffusion of Ti and Au during 20-min anneals at 600 C. The amount of mixing observed also depends on the nature of the substrate which supports the Ti-Mo-Au metallization.

Harris, J. M.

Auger spectroscopy of fracture surfaces of ceramics

Results of Auger electron spectroscopy (AES) studies of fracture surfaces in a series of ceramic materials, including Al2O3, MgO, and Si3N4, which were formed using different processing techniques. AES on the fractured surface of a lunar sample is also discussed. Scanning electron micrograph fractography is used to relate the surface chemistry to the failure mode. Combined argon ion sputtering and AES studies demonstrate the local variations in chemistry near the fracture surface. The problems associated with doing AES in insulators are also discussed, and the experimental techniques directed toward solving them are described.

Marcus, H. L.