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Gluyas, R. E.

Publications and source records attributed to Gluyas, R. E..

Resin char oxidation retardant for composites

Boron powder stabilizes char, so burned substances are shiny, smooth, and free of loose graphite fibers. Resin weight loss of laminates during burning in air is identical for the first three minutes for unfilled and boron-filled samples, then boron samples stabilize.

Bowles, K. J.

Improved fiber retention by the use of fillers in graphite fiber/resin matrix composites

A variety of matrix fillers were tested for their ability to prevent loss of fiber from graphite fiber/PMR polyimide and graphite fiber/epoxy composites in a fire. The fillers tested included powders of boron, boron carbide lime glass, lead glass, and aluminum. Boron was the most effective and prevented any loss of graphite fiber during burning. Mechanical properties of composites containing boron filler were measured and compared to those of composites containing no filler.

Gluyas, R. E.

Improved fiber retention by the use of fillers in graphite fiber/resin matrix composites

A potential problem in the use of graphite fiber reinforced resin matrix composites is the dispersal of graphite fiber during accidental fires. Airborne electrically conductive fibers originating from burning composites could enter and cause shorting in electrical equipment located in surrounding areas. A variety of matrix fillers have been tested for their ability to prevent loss of fiber from graphite fiber/PMR polyimide and graphite fiber/epoxy composites in a fire. The fillers tested included powders of boron, boron carbide (B4C), lime glass, lead glass, and aluminum. Of these fillers, boron was the most effective and prevented any loss of graphite fiber during burning. Mechanical properties of composites containing boron filler were measured and compared to those of composite containing no filler.

Gluyas, R. E.

Thermal analysis of PMR-polyimides by dielectrometry

A preliminary study was conducted to determine the dielectric properties of glass fabric reinforced composites as influenced by the reactions occurring during the preparation of crosslinked polyimides by the PMR process. The variables studied included: formulated molecular weight, staging temperature and time; rate of temperature increase to cure temperature; and cure temperature and time. The changes of capacitance and, particularly, of dissipation factor were found to be strongly dependent on each of the variables studied.

Gluyas, R. E.

Evaluation of refractory-metal-clad uranium nitride and uranium dioxide fuel pins after irradiation for times up to 10 450 hours at 990 C

The effects of some materials variables on the irradiation performance of fuel pins for a lithium-cooled space power reactor design concept were examined. The variables studied were UN fuel density, fuel composition, and cladding alloy. All pins were irradiated at about 990 C in a thermal neutron environment to the design fuel burnup. An 85-percent dense UN fuel gave the best overall results in meeting the operational goals. The T-111 cladding on all specimens was embrittled, possibly by hydrogen in the case of the UN fuel and by uranium and oxygen in the case of the UO2 fuel. Tests with Cb-1Zr cladding indicate potential use of this cladding material. The UO2 fueled specimens met the operational goals of less than 1 percent cladding strain, but other factors make UO2 less attractive than low-density UN for the contemplated space power reactor use.

Bowles, K. J.

Materials technology for an advanced space power nuclear reactor concept: Program summary

The results of a materials technology program for a long-life (50,000 hr), high-temperature (950 C coolant outlet), lithium-cooled, nuclear space power reactor concept are reviewed and discussed. Fabrication methods and compatibility and property data were developed for candidate materials for fuel pins and, to a lesser extent, for potential control systems, reflectors, reactor vessel and piping, and other reactor structural materials. The effects of selected materials variables on fuel pin irradiation performance were determined. The most promising materials for fuel pins were found to be 85 percent dense uranium mononitride (UN) fuel clad with tungsten-lined T-111 (Ta-8W-2Hf).

Gluyas, R. E.