The Certification of Standard Reference Material 1979: Powder Diffraction Line Profile Standard for Crystallite Size Analysis
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Engineering topics
Publications and source records attributed to Black, David.
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This report includes the results of monthly inspections and monitoring for January, February, and March 2020. Monthly inspections and monitoring were conducted on January 15, February 12, and March 17, 2020. Inspections include a visual assessment of the berms, ponding, water levels relative to the overflow pipes, tunneling or burrowing into the berms, soil conditions on and around the berms, erosion or sloughing of the slopes of the berms, seeps at the toe of the berms, deep-rooting botanicals on the berms, and fencing. Monthly monitoring includes measurements of the instantaneous flow rate, hydrogen ion activity (pH), and specific conductance of the E-Tunnel Wastewater Disposal System discharge.
This report includes the results of monthly inspections and monitoring for October, November, and December 2019. Monthly inspections and monitoring were conducted on October 15, November 26, and December 18, 2019. Inspections include a visual assessment of the berms, ponding, water levels relative to the overflow pipes, tunneling or burrowing into the berms, soil conditions on and around the berms, erosion or sloughing of the slopes of the berms, seeps at the toe of the berms, deep-rooting botanicals on the berms, and fencing. Monthly monitoring includes measurements of the instantaneous flow rate, hydrogen ion activity (pH), and specific conductance of the E-Tunnel Wastewater Disposal System (ETDS) discharge. Annual sample results of the effluent water from the ETDS are also included in this report. The effluent sample was collected on September 11, 2019, and analyzed for the parameters listed in Table 1-B of Permit NEV 96021. In addition, Permit NEV 96021 requires the collection and analysis of representative groundwater samples from Well ER 12-1 every 24 months. This summary report provides the information pertaining to the sampling and analysis of groundwater samples collected on April 10, 2019.
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Environmental monitoring data are collected at and around the Area 3 and Area 5 Radioactive Waste Management Sites (RWMSs) within the Nevada National Security Site. This report summarizes the 2018 environmental data to provide an overall evaluation of RWMS performance and to support environmental compliance and performance assessment activities.
This report is a compilation of the groundwater and waste cell leachate sampling results from the Area 5 Radioactive Waste Management Site (RWMS) at the Nevada National Security Site, Nye County, Nevada. Groundwater samples from the aquifer immediately below the Area 5 RWMS have been collected and analyzed and static water levels have been measured in this aquifer since 1993. These groundwater data are evaluated for evidence of effects on the aquifer related to the Area 5 RWMS. Leachate from one lined mixed waste cell at the Area 5 RWMS (Cell 18) has been sampled since the cell opened in 2011. These leachate data are analyzed for hazardous contaminants to determine appropriate leachate handling and disposal. A second lined mixed waste cell at the Area 5 RWMS (Cell 25) began receiving waste in August 2018, but no leachate samples were collected or analyzed during 2018. This report includes data from 2014 through 2018 but focuses on the 2018 data. During 2018, groundwater samples were collected and static water levels were measured at three wells surrounding the Area 5 RWMS. Groundwater samples were collected at wells UE5PW-1, UE5PW-2, and UE5PW-3 on March 6 and August 14, 2018. Static water levels were measured at each of these wells on March 5, June 4, August 13, and October 25, 2018. Groundwater monitoring at the Area 5 RWMS complies with Title 40 Code of Federal Regulations (CFR) Part 264.97, General ground-water monitoring requirements , and 40 CFR 264.98, Detection monitoring program. Groundwater samples were analyzed for indicators of contamination (pH, specific conductance [SC], total organic carbon, total organic halides, and tritium) and, beginning in 2017, toxicity characteristic metals (arsenic, barium, cadmium, chromium, lead, mercury, selenium, and silver). General water chemistry parameters (calcium, iron, magnesium, manganese, potassium, sodium, sulfate, chloride, fluoride, bicarbonate, and silicate) were also measured. Results from samples collected in 2018 are within the limits for each parameter established by the Nevada Division of Environmental Protection in Resource Conservation and Recovery Act (RCRA) Permit NEV HW0101, Revision 6. Data from the shallow aquifer indicate there has been no measurable impact to the uppermost aquifer from the Area 5 RWMS, and there were no significant changes in measured groundwater parameters compared to previous years. Leachate from lined mixed waste Cell 18 drains into a sump and is pumped into an above ground tank. Samples are collected from the tank when the leachate volume approaches the 3,000-gallon tank capacity. During 2018, leachate samples were collected on March 1, 2018 and August 1, 2018. All leachate analysis results are below the regulatory levels for toxicity characteristic contaminants (40 CFR 261.24) and below the investigation levels for polychlorinated biphenyls (PCBs), tritium, pH, and SC specified in RCRA Permit NEV HW0101, Revision 6. No quantifiable PCB levels were detected in any leachate sample. Based on the leachate analysis results, RCRA Permit NEV HW0101 allowed all leachate collected from Cell 18 to be pumped from the collection tank and used for dust control at Cell 18.
Environmental monitoring data are collected at and around the Area 3 and Area 5 Radioactive Waste Management Sites (RWMSs) within the Nevada National Security Site (NNSS). These data include direct radiation exposure, as well as radiation from the air, groundwater, meteorology, and vadose zone. This report summarizes the 2016 environmental data to provide an overall evaluation of RWMS performance and to support environmental compliance and performance assessment (PA) activities. Some of these data (e.g., radiation exposure, air, and groundwater) are presented in other reports, developed by National Security Technologies, LLC Direct radiation monitoring data indicate exposure levels at the RWMSs are within the range of background levels measured at the NNSS. Slightly elevated exposure levels outside the Area 3 RWMS are attributed to nearby historical aboveground nuclear weapons tests. Air monitoring data show that tritium concentrations in water vapor and americium and plutonium concentrations in air particles are below Derived Concentration Standards for these radionuclides. Groundwater monitoring data indicate the groundwater in the uppermost aquifer beneath the Area 5 RWMS is not impacted by RWMS operations. Results of groundwater analysis from wells around the Area 5 RWMS were all below established investigation levels. Leachate samples collected from the leachate collection system at the mixed low-level waste cell were below established contaminant regulatory limits. During 2016, precipitation at the Area 3 RWMS was 8% below average, and precipitation at the Area 5 RWMS was 8% above average. Water balance measurements indicate that evapotranspiration from the vegetated weighing lysimeter dries the soil and prevents downward percolation of precipitation more effectively than evaporation as measured from the bare-soil weighing lysimeter. Vadose zone monitoring on Area 5 and Area 3 RWMS cell covers shows no evidence of precipitation percolating through the covers to the waste. Moisture from precipitation did not percolate below 150 centimeters (cm) (5 feet [ft]) in the vegetated final cover on the U-3ax/bl disposal unit at the Area 3 RWMS. During 2016, there was no drainage through 2.4 meters (8 ft) of soil as indicated from the Area 3 drainage lysimeters that received only natural precipitation. Forty-four percent of the applied precipitation and irrigation drained from the bare-soil drainage lysimeter, which received 3 times the natural precipitation. All 2016 monitoring data indicate that the Area 3 and Area 5 RWMSs are performing within expectations of the model and parameter assumptions for the facilities’ PAs
Environmental monitoring data are collected at and around the Area 3 and Area 5 Radioactive Waste Management Sites (RWMSs) within the Nevada National Security Site (NNSS). These data include direct radiation exposure, as well as radiation from the air, groundwater, meteorology, and vadose zone. This report summarizes the 2015 environmental data to provide an overall evaluation of RWMS performance and to support environmental compliance and performance assessment (PA) activities. Some of these data (e.g., radiation exposure, air, and groundwater) are presented in other reports developed by National Security Technologies, LLC. Direct radiation monitoring data indicate exposure levels at the RWMSs are within the range of background levels measured at the NNSS. Slightly elevated exposure levels outside the Area 3 RWMS are attributed to nearby historical aboveground nuclear weapons tests. Air monitoring data show that tritium concentrations in water vapor and americium and plutonium concentrations in air particles are below Derived Concentration Standards for these radionuclides. Groundwater monitoring data indicate the groundwater in the uppermost aquifer beneath the Area 5 RWMS is not impacted by RWMS operations. Results of groundwater analysis from wells around the Area 5 RWMS were all below established investigation levels. Leachate samples collected from the leachate collection system at the mixed low-level waste cell were below established contaminant regulatory limits. During 2015, precipitation at the Area 3 RWMS was 0.9% above average, and precipitation at the Area 5 RWMS was 25% above average. Water balance measurements indicate that evapotranspiration from the vegetated weighing lysimeter dries the soil and prevents downward percolation of precipitation more effectively than evaporation as measured from the bare-soil weighing lysimeter. The 1.8 inches of precipitation in September reached the lowest sensors at 180 cm on the Cell 5S and 5N covers, however the sensors on the floor do not indicate any signs of the precipitation percolating thru the waste to the floor. Moisture from precipitation did not percolate below 150 centimeters (cm) (5 feet [ft]) in the vegetated final cover on the U-3ax/bl disposal unit at the Area 3 RWMS. A second remedial revegetation trial was done on the southern portion of the North Cover. In March 2015 it was determined that germination occurred on both the mulched and non-mulched treatments that were irrigated, but that no germination occurred on the non-irrigated treatments. By June the seedlings observed in March were gone, possibly grazed by rabbits which were observed inside the rabbit-proof fence. In August the entire area was sprayed with the herbicide glyphosate in an attempt to minimize weed seed production. During 2015, there was no drainage through 2.4 meters (8 ft) of soil as indicated from the Area 3 drainage lysimeters that received only natural precipitation. Thirty-one percent of the applied precipitation and irrigation drained from the bare-soil drainage lysimeter, which received 3 times the natural precipitation. All 2015 monitoring data indicate that the Area 3 and Area 5 RWMSs are performing within expectations of the model and parameter assumptions for the facilities’ PAs.
This report describes research undertaken by USRA scientists working in the NASA Space Science Directorate laboratories at Goddard Space Flight Center.
The mission of this activity, know as the Cooperative Program in Space Sciences (CPSS), is to conduct space science research and leading-edge instrumentation and technology development, enable research by the space sciences communities, and to expedite the effective dissemination of space science research, technology, data, and information to the educational community and the general public. To fulfill this mission, USRA recruits and maintains a staff of scientific researchers, operates a series of guest investigator facilities, organizes scientific meetings and workshops, and encourages various interactions with students and university faculty members.
The mission of this activity, known as the Cooperative Program in Space Sciences (CPSS), is to conduct space science research and leading-edge instrumentation and technology development, enable research by the space sciences communities, and to expedite the effective dissemination of space science research, technology, data, and information to the educational community and the general public. To fulfill this mission, the Universities Space Research Association (USRA) recruits and maintains a staff of scientific researchers, operates a series of guest investigator facilities, organizes scientific meetings and workshops, and encourages various interactions with students and university faculty members. This paper is the final report from this now completed Cooperative Agreement.
The Universities Space Research Association received an award of Cooperative Agreement NCC5-356 on September 29, 1998. The mission of this activity, known as the Cooperative Program in Space Sciences (CPSS), is to conduct space science research and leading-edge instrumentation and technology development, enable research by the space sciences communities, and to expedite the effective dissemination of space science research, technology, data, and information to the educational community and the general public. To fulfill this mission, USRA recruits and maintains a staff of scientific researchers, operates a series of guest investigator facilities, organizes scientific meetings and workshops, and encourages various interactions with students and university faculty members.
High resolution X-ray diffraction images of two directly comparable crystals of lead tin telluride, one Bridgman-grown on Space Shuttle STS 61A and the other terrestrially Bridgman-grown under similar conditions from identical material, present different subgrain structure. In the terrestrial, sample 1 the appearance of an elaborate array of subgrains is closely associated with the intrusion of regions that are out of diffraction in all of the various images. The formation of this elaborate subgrain structure is inhibited by growth in microgravity.
Irregularities in three crystals grown in space and in four terrestrial crystals grown under otherwise comparable conditions have been observed in high resolution diffraction imaging. The images provide important new clues to the nature and origins of irregularities in each crystal. For two of the materials, mercuric iodide and lead tin telluride, more than one phase (an array of non-diffracting inclusions) was observed in terrestrial samples; but the formation of these multiple phases appears to have been suppressed in directly comparable crystals grown in microgravity. The terrestrial seed crystal of triglycine sulfate displayed an unexpected layered structure, which propagated during directly comparable space growth. Terrestrial Bridgman regrowth of gallium arsenide revealed a mesoscopic structure substantially different from that of the original Czochralski material. A directly comparable crystal is to be grown shortly in space.
The evolution of the Astrometric Telescope Facility (ATF) proposed for use on NASA's Space Station is traced and its design characteristics are presented. With a focal plane scale of 12.7 arcsec/mm, the strawman design has a field size of 10 sq arcmin and a limiting visual magnitude fainter than 16. Output from an observation includes the X and Y coordinates of each star and its relative brightness.
The authors profile the field of astronomy, identify some of the key scientific questions that can be addressed during the decade of the 1990's, and recommend several facilities that are critically important for answering these questions. Scientific opportunities for the 1990' are discussed. Areas discussed include protoplanetary disks, an inventory of the solar system, primitive material in the solar system, the dynamics of planetary atmospheres, planetary rings and ring dynamics, the composition and structure of the atmospheres of giant planets, the volcanoes of IO, and the mineralogy of the Martian surface. Critical technology developments, proposed projects and facilities, and recommendations for research and facilities are discussed.